HIGH PURITY TUNGSTEN HEXACHLORIDE AND METHOD FOR MAKING SAME
    101.
    发明公开
    HIGH PURITY TUNGSTEN HEXACHLORIDE AND METHOD FOR MAKING SAME 审中-公开
    赫尔辛基·沃尔夫哈佛·哈佛大使馆(VERFAHREN ZUR HERSTELLUNG DAVON)

    公开(公告)号:EP3081667A2

    公开(公告)日:2016-10-19

    申请号:EP16165675.6

    申请日:2016-04-15

    IPC分类号: C23C16/08 C23C16/44

    摘要: Condensable metal halide materials, such as but not limited to tungsten chloride (WCl 6 ), can be used deposit films metal or metal containing films in a chemical vapor deposition (CVD) or atomic layer deposition process. Described herein are high purity compositions comprising condensable materials and methods to purify condensable materials. In one aspect, there is provided a composition comprising: tungsten hexachloride which is substantially free of at least one impurity and wherein the tungsten hexachloride comprises at least 90%, preferably 95 % and more preferably 99 % by weight or greater of a β- WCl 6 and 5% by weight or less of the α- WCl 6 as measured by X-ray diffraction.

    摘要翻译: 可以在化学气相沉积(CVD)或原子层沉积工艺中使用可冷凝金属卤化物材料,例如但不限于氯化钨(WCl 6))沉积膜金属或含金属的膜。 本文描述的是包含可冷凝材料的高纯度组合物和用于纯化可冷凝材料的方法。 一方面,提供了一种组合物,其包含:基本上不含至少一种杂质的六氯化铬,其中六氯化钨包含至少90%,优选95%,更优选99重量%以上的2 -WCl 6和5重量%以下的± - WCl 6,通过X射线衍射测定。

    ALKALI METAL SALT OF FLUOROSULFONYL IMIDE, AND PRODUCTION METHOD THEREFOR
    103.
    发明公开
    ALKALI METAL SALT OF FLUOROSULFONYL IMIDE, AND PRODUCTION METHOD THEREFOR 审中-公开
    ALKALIMETALLSALZ AUS FLUORSULFONYLIMID UND HERSTELLUNGSVERFAHRENDAFÜR

    公开(公告)号:EP2578533A4

    公开(公告)日:2013-11-06

    申请号:EP11786792

    申请日:2011-05-27

    摘要: The present invention provides an alkali metal salt of fluorosulfonyl imide having favorable heat resistance and a reduced content of specific impurities and a water content, and provides a method for producing an alkali metal salt of fluorosulfonyl imide, which is capable of easily removing a solvent from a reaction solution. An alkali metal salt of fluorosulfonyl imide of the present invention is represented by the following general formula (I) and has a mass loss rate of 2% or less when the alkali metal salt of fuluorosulufonyl imide is kept at 100°C for 8 hours under an air current. A method for producing an alkali metal salt of fluorosulfonyl imide of the present invention comprises a step of concentrating a solution of the alkali metal salt of fulorosulfonyl imide by bubbling a gas into a reaction solution containing the alkali metal salt of fulorosulfonyl imide, and/or concentrating a solution of the alkali metal salt of fulorosulfonyl imide by thin layer distillation.

    摘要翻译: 本发明提供一种氟磺酰亚胺的碱金属盐,其具有良好的耐热性并且降低了特定杂质和水含量,并且提供了一种氟磺酰亚胺碱金属盐的制备方法,该方法能够容易地从 反应溶液。 本发明的氟磺酰亚胺的碱金属盐由下述通式(I)表示,并且当将氟代磺酰基酰亚胺的碱金属盐在100℃下保持8小时时,质量损失率为2%或更低 气流。 本发明的氟磺酰亚胺的碱金属盐的制造方法,其特征在于,包括:向含有氟磺酰亚胺的碱金属盐的反应溶液中鼓入气体,浓缩富勒烯磺酰亚胺的碱金属盐的溶液和/或 通过薄层蒸馏浓缩富勒烯磺酰亚胺的碱金属盐溶液。

    MIKROWELLEN-BASIERTES VERFAHREN UND VORRICHTUNG ZUM HERSTELLEN HOCHREINER FLÜSSIGKEITEN
    104.
    发明公开
    MIKROWELLEN-BASIERTES VERFAHREN UND VORRICHTUNG ZUM HERSTELLEN HOCHREINER FLÜSSIGKEITEN 审中-公开
    生产高纯液体微波为基础的方法和装置

    公开(公告)号:EP2635358A1

    公开(公告)日:2013-09-11

    申请号:EP11773448.3

    申请日:2011-10-18

    摘要: The invention relates to a method for producing high-purity liquids by means of distillation, particularly liquid chemicals, said method having the following steps: supplying a liquid to be purified (1) from a reservoir (41) to a sample container (3) arranged in a sample chamber (4); heating and evaporating the uppermost layers of the liquid to be purified (1); condensing the sample vapour (18) obtained from the liquid to the purified (1) in a condensation device (70) outside the sample chamber (4); and collecting the distillate (76) in a collection container (77) which is connected to the reservoir (41) by means of a return conduit (80) for the non-condensed sample vapour (18), and which forms a chamber, sealed off from the surroundings, between the chamber above the surface (14) of the liquid to be purified (1) in the sample chamber (4), and the reservoir (41).

    ALKALI METAL SALT OF FLUOROSULFONYL IMIDE, AND PRODUCTION METHOD THEREFOR
    105.
    发明公开
    ALKALI METAL SALT OF FLUOROSULFONYL IMIDE, AND PRODUCTION METHOD THEREFOR 审中-公开
    ALKALIMETALLSALZ AUS FLUORSULFONYLIMID UND HERSTELLUNGSVERFAHRENDAFÜR

    公开(公告)号:EP2578533A1

    公开(公告)日:2013-04-10

    申请号:EP11786792.9

    申请日:2011-05-27

    IPC分类号: C01B21/093

    摘要: The present invention provides an alkali metal salt of fluorosulfonyl imide having favorable heat resistance and a reduced content of specific impurities and a water content, and provides a method for producing an alkali metal salt of fluorosulfonyl imide, which is capable of easily removing a solvent from a reaction solution. An alkali metal salt of fluorosulfonyl imide of the present invention is represented by the following general formula (I) and has a mass loss rate of 2% or less when the alkali metal salt of fuluorosulufonyl imide is kept at 100°C for 8 hours under an air current. A method for producing an alkali metal salt of fluorosulfonyl imide of the present invention comprises a step of concentrating a solution of the alkali metal salt of fulorosulfonyl imide by bubbling a gas into a reaction solution containing the alkali metal salt of fulorosulfonyl imide, and/or concentrating a solution of the alkali metal salt of fulorosulfonyl imide by thin layer distillation.

    摘要翻译: 本发明提供了具有良好的耐热性和特定杂质含量以及含水量的氟磺酰亚胺的碱金属盐,并提供了能够容易地除去溶剂的氟磺酰亚胺的碱金属盐的方法 反应溶液。 本发明的氟代磺酰亚胺的碱金属盐由以下通式(I)表示,当将富氟磺酰基酰亚胺的碱金属盐在100℃保持8小时时,其质量损失率为2%以下 气流。 制备本发明的氟磺酰亚胺的碱金属盐的方法包括通过将气体鼓泡到含有有机磺酰亚胺的碱金属盐的反应溶液中来浓缩富马酰亚胺的碱金属盐的溶液和/或 通过薄层蒸馏浓缩富磺酰亚胺的碱金属盐的溶液。

    Process for stripping polymer dispersions
    108.
    发明公开
    Process for stripping polymer dispersions 审中-公开
    一种用于聚合物分散体的分离处理

    公开(公告)号:EP1920808A3

    公开(公告)日:2010-05-12

    申请号:EP07254265.7

    申请日:2007-10-29

    IPC分类号: B01D1/14 B01D3/34

    摘要: A process for continuously stripping polymer dispersions with volatile substances comprising:
    providing a polymer dispersion (10) and steam (20) wherein the dispersion comprises aqueous emulsion polymer and volatile organic compounds;
    feeding the polymer dispersion (10) and steam (20) into a stripper (30);
    removing at least a portion of the volatile organic compounds from the dispersion (10);
    transferring the portion of the volatile organic compounds to the steam (20); and
    separating the steam from the aqueous emulsion polymer in a separator vessel (40) wherein the stripper (30) has a ratio of surface area to volume of at least 10:1 1/m; and
    is comprised of one or more heat exchangers in parallel or series wherein the heat exchanger is a shell and tube or spiral heat exchanger.

    METHOD AND DEVICE FOR STRIPPING AMMONIA FROM LIQUIDS
    109.
    发明授权
    METHOD AND DEVICE FOR STRIPPING AMMONIA FROM LIQUIDS 有权
    用于从液体中去除氨的方法和装置

    公开(公告)号:EP1528953B8

    公开(公告)日:2009-06-10

    申请号:EP03740122.1

    申请日:2003-08-01

    申请人: GFE Patent A/S

    发明人: BONDE, Torben, A.

    IPC分类号: B01D3/38 C02F1/58

    摘要: The present invention in a first aspect provides a method and a system for stripping volatile compounds such as ammonia from e.g. fermentation liquids. Part of the ammonia is stripped form the liquid in a stripper system comprising a shunt through which liquid such as e.g. fermentation medium comprising a biomass can be diverted in the form of a side stream in liquid contact with a main fermentor(s). The stripper system is connected to an evaporator. In the evaporator aqueous liquid is heated at a pressure below atmospheric pressure whereby vapour is developed at a temperature below 100°C. The vapour from the evaporator is directed to the liquid medium comprising ammonia and this results in ammonia being stripped from the liquid and transferred to the vapour phase. The vapour phase is condensed in first condenser at a low pressure, e.g. a pressure well below 1 bar, and the liquid thus obtained is further treated in a stripper unit at a higher pressure, such as e.g. a pressure at or above 1 bar, to obtain a more concentrated solution of ammonia. When stripped for at least part of the ammonia the liquid initially obtained from the biogas reactor and diverted to the shunt can be returned to the reactor.

    摘要翻译: 本发明的第一方面提供了用于从例如乙醇中汽提挥发性化合物如氨的方法和系统。 发酵液。 部分氨在包含分流器的汽提系统中从液体中汽提出来, 包含生物质的发酵培养基可以以与主发酵罐液体接触的侧流形式转向。 汽提塔系统连接到蒸发器。 在蒸发器中,含水液体在低于大气压的压力下加热,由此在低于100℃的温度下形成蒸气。 来自蒸发器的蒸汽被引导至包含氨的液体介质,这导致氨从液体中汽提并转移至汽相。 汽相在第一冷凝器中在低压下冷凝, 压力远低于1巴,并且由此获得的液体在更高压力下的汽提单元中进一步处理,例如, 压力等于或高于1巴,以获得更浓的氨溶液。 当汽提至少一部分氨时,最初从沼气反应器获得并转移到分流器的液体可返回反应器。