VERFAHREN ZUR AUFREINIGUNG VON 4,4'-METHYLENDIPHENYLDIISOCYANAT ENTHALTENDEN MISCHUNGEN

    公开(公告)号:EP2640696A1

    公开(公告)日:2013-09-25

    申请号:EP11787657.3

    申请日:2011-11-15

    Applicant: BASF SE

    CPC classification number: C07C263/20 C07C265/14

    Abstract: The invention relates to a process for purifying mixtures comprising 4,4'-methylene diphenyl diisocyanate, comprising the distillative purification of a mixture I comprising 4,4'-methylene diphenyl diisocyanate by means of a column K1, wherein the gaseous stream consisting of mixture I is contacted in column K1 with at least one liquid compound A which has a boiling point which is the same as or higher than 4,4'-methylene diphenyl diisocyanate, and wherein the gaseous stream O which is obtained at the top of the column and comprises 4,4'-methylene diphenyl diisocyanate is cooled to a temperature of 20°C to 60°C within not more than 5 seconds.

    Abstract translation: 本发明涉及一种纯化包含4,4'-亚甲基二苯基二异氰酸酯的混合物的方法,该方法包括通过塔K1蒸馏纯化包含4,4'-亚甲基二苯基二异氰酸酯的混合物I,其中由混合物 I在塔K1中与至少一种液体化合物A接触,所述液体化合物A具有与4,4'-亚甲基二苯基二异氰酸酯相同或更高的沸点,并且其中在塔顶获得的气态流O 并且包含4,4'-亚甲基二苯基二异氰酸酯在不超过5秒内冷却至20℃至60℃的温度。

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