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    VERFAHREN ZUR HERSTELLUNG VON N,N-SUBSTITUIERTEN 3-AMINOPROPAN-1-OLEN
    59.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON N,N-SUBSTITUIERTEN 3-AMINOPROPAN-1-OLEN 有权
    用于生产N，N-二取代的3-氨基-1- OLAND

    公开(公告)号：EP2352719A2

    公开(公告)日：2011-08-10

    申请号：EP09744155.4

    申请日：2009-11-02

    Applicant: BASF SE

    Inventor： WIGBERS, Christof Wilhelm ,  MELDER, Johann-Peter ,  ERNST, Martin

    IPC: C07C213/00 ,  C07C215/08

    CPC classification number: C07C213/02 ,  C07C227/08 ,  Y02P20/582 ,  C07C215/08 ,  C07C229/12

    Abstract: The present invention relates to a method for producing N,N-substituted-3-aminopropan-1-ols by a) converting secondary amine with acrolein at a temperature of (-50) to 100°C and a pressure of 0.01 to 300 bar, and b) converting the reaction mixture obtained in step a) with hydrogen and ammonia in the presence of a hydrogenation catalyst at a pressure of 1 to 400 bar, characterized in that in step a) the molar ratio of secondary amine to acrolein is 1:1 or more and the temperature in step b) is in the range of (-50) to 70°C. In a preferred embodiment, an acrolein that was obtained from glycerine based on renewable raw materials is used. The invention further relates to the use of an N,N-dimethyl-3-aminopropan-1-ol (DMAPOL) based on renewable raw materials as a catalyst for producing polyurethane, as a scrubbing liquid in gas scrubbing, in the field of electronics chemicals and electroplating, as a feed material in organic synthesis, and as an intermediate product in the production of pharmaceuticals and plant protection agents.

    VERFAHREN ZUR HERSTELLUNG VON N,N-SUBSTITUIERTEN-1,3-PROPANDIAMINEN
    60.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON N,N-SUBSTITUIERTEN-1,3-PROPANDIAMINEN 有权
    用于生产N，N-取代的1,3-丙二胺

    公开(公告)号：EP2279164A2

    公开(公告)日：2011-02-02

    申请号：EP09745709.7

    申请日：2009-05-11

    Applicant: BASF SE

    Inventor： ERNST, Martin ,  MELDER, Johann-Peter ,  WIGBERS, Christof Wilhelm

    IPC: C07C209/26 ,  C07C209/60

    CPC classification number: C07C211/11 ,  C07C209/60 ,  Y02P20/582

    Abstract: The invention relates to a method for producing N,N-substituted- 1,3-propandiamine by a) reacting secondary amines with acrolein at a temperature between (-50) - 100°C and at a pressure between 0,01 - 300 bar, and b) reacting the reaction mixture obtained in step a) with hydrogen and ammonia in the presence of a hydrogenation catalyst at a temperature between 40 - 400°C and at a pressure of 1 - 400 bar. The invention is characterised in that in step a) the molar ratio of secondary amines to acrolein is 2:1 or more and the hydrogenation catalyst used in step b) contains cobalt. In a preferred embodiment, acrolein that is obtained from glycerin based on renewable raw material is used. The invention also relates to the use of a N,N-dimethyl-1,3-propandiamine (DMAPA) based on renewable raw material as charge material for soft soaps and other detergents, coagulation agents, polymers and comb polymers. In another preferred embodiment, step b) takes place in the presence of water.

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