VERFAHREN ZUR HERSTELLUNG VON SEHR REINEM 1,4-BUTANDIOL
    71.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON SEHR REINEM 1,4-BUTANDIOL 有权
    用于生产非常纯的1,4-丁二醇

    公开(公告)号:EP2118044A1

    公开(公告)日:2009-11-18

    申请号:EP07726909.0

    申请日:2007-03-14

    Applicant: BASF SE

    CPC classification number: C07C29/80 C07C31/207

    Abstract: The object of the present invention is a method for the purifying distillation of raw, aqueous 1,4-butanediol (1), in which 1,4-butanediol (5) freed of components boiling at a lower point than 1,4-butanediol and water is conducted through three distillation columns (III, IV, V), components boiling at a higher point than 1,4-butanediol are drawn from the bottom of the first column and conducted to the third (7), 1,4-butanediol is conducted from the top of the first column (6) into the second, the bottom product of the second column (9) is conducted into the third, the top product of the third column (11) is returned at least partially to the first column, characterized in that the pure 1,4-butanediol is removed from the side outlet of the second column.

    VERFAHREN ZUR HERSTELLUNG VON POLYTETRAHYDROFURAN ODER TETRAHYDROFURAN-COPOLYMEREN
    72.
    发明授权
    VERFAHREN ZUR HERSTELLUNG VON POLYTETRAHYDROFURAN ODER TETRAHYDROFURAN-COPOLYMEREN 有权
    VERFAHREN ZUR HERSTELLUNG VON聚四氢呋喃ODER四氢呋喃 - 共聚物

    公开(公告)号:EP2032626B1

    公开(公告)日:2009-08-26

    申请号:EP07729532.7

    申请日:2007-05-25

    Applicant: BASF SE

    CPC classification number: C08G65/20

    Abstract: The subject matter of the present invention is a method for the production of polytetrahydrofurane or tetrahydrofurane copolymers by means of the polymerization of tetrahydrofurane, in the presence of a telogen and/or a comonomer, on an acidic fixed-bed catalyst, in which the temperature of the polymerization mixture increases in the flow direction of the catalyst bed.

    Abstract translation: 本发明的主题是通过在调聚体和/或共聚单体存在下在酸性固定床催化剂上聚合四氢呋喃生产聚四氢呋喃或四氢呋喃共聚物的方法,其中温度 的聚合混合物在催化剂床的流动方向上增加。

    VERFAHREN ZUR REINIGUNG VON CYCLISCHEN KETONEN
    73.
    发明公开
    VERFAHREN ZUR REINIGUNG VON CYCLISCHEN KETONEN 有权
    通过热处理环十二酮纯化

    公开(公告)号:EP2041061A1

    公开(公告)日:2009-04-01

    申请号:EP07765650.2

    申请日:2007-06-27

    Applicant: BASF SE

    Abstract: The invention relates to a method for purifying a composition (I) containing at least one cyclic ketone having 7 to 16 C atoms. The method encompasses the thermal treatment of the composition (I) with a catalyst containing at least one transition metal and the further purification by a method selected from the group consisting of destillation, extraction and crystallization. The invention also relates to a method for producing cyclododecanone, which includes a purification of this type, and to the use of at least one catalyst containing at least one transition metal for purifying a composition (I) containing at least one cyclic ketone having 7 to 16 C atoms by thermal treatment of the composition (I) with a catalyst that contains at least one transition metal.

    VERFAHREN ZUR ABTRENNUNG VON POLYMEREN NEBENPRODUKTEN AUS 1,4-BUTINDIOL
    76.
    发明公开
    VERFAHREN ZUR ABTRENNUNG VON POLYMEREN NEBENPRODUKTEN AUS 1,4-BUTINDIOL 有权
    VERFAHREN ZUR ABTRENNUNG VON POLYMEREN NEBENPRODUKTEN AUS 1,4-BUTINDOL

    公开(公告)号:EP1926696A1

    公开(公告)日:2008-06-04

    申请号:EP06792973.7

    申请日:2006-08-23

    Applicant: BASF SE

    Abstract: The invention relates to a method for purifying 1,4-butynediol, in which 1,4-butynediol is processed in a dynamic mixing device in an inert gas atmosphere at 25 to 150 °C at a velocity gradient exceeding 100,000 sec-1 in the radial play between the rotor and the stator, one waits for the phases to separate at temperatures ranging from 25 to 150 °C, and the bottom phase is eliminated. Also disclosed is a method for hydrogenating 1,4-butynediol into 1,4-butenediol and 1,4-butanediol with the aid of the purified 1,4-butynediol.

    Abstract translation: 纯化1,4-丁炔二醇的方法本发明涉及一种纯化1,4-丁炔二醇的方法,其中1,4-丁炔二醇在动态混合装置中在25至150℃的惰性气体气氛中以超过100,000秒-1的速度梯度 在转子和定子之间的径向间隙,等待在25至150℃的温度范围内相分离,并且消除底部阶段。 还公开了借助于纯化的1,4-丁炔二醇将1,4-丁炔二醇氢化成1,4-丁烯二醇和1,4-丁二醇的方法。

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