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    VERFAHREN ZUR HERSTELLUNG VON CYCLOHEXAN MIT AUS EINEM STEAMCRACKVERFAHREN STAMMENDEN AUSGANGSMATERIALIEN
    5.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON CYCLOHEXAN MIT AUS EINEM STEAMCRACKVERFAHREN STAMMENDEN AUSGANGSMATERIALIEN 有权
    用于生产用蒸汽CYCLOHEXANE从裂缝过程中获得起始物

    公开(公告)号：EP2909159A2

    公开(公告)日：2015-08-26

    申请号：EP13776829.7

    申请日：2013-10-16

    申请人： BASF SE

    发明人： TSCHIRSCHWITZ, Steffen ,  WISSEL-STOLL, Kathrin ,  BÜRKLE, Jochen ,  KOSTOVA, Albena ,  SCHMITT, Markus ,  WLOKA, Veronika ,  DEUERLEIN, Stephan ,  BOSCH, Marco ,  OEHLENSCHLÄGER, Steffen ,  SCHREIBER, Michael ,  AVERLANT, Gauthier Luc Maurice ,  JONI, Joni ,  PROCHAZKA, Roman ,  BOCK, Martin ,  KINDLER, Alois ,  MALKOWSKY, Daniela ,  SPUHL, Katharina ,  BITTERLICH, Stefan ,  PFEIFFER, Daniel

    IPC分类号： C07C5/29 ,  C07C13/18

    CPC分类号： C07C5/10 ,  C07C5/29 ,  C07C2523/755 ,  C07C2527/125 ,  C07C2601/14 ,  C07C13/18

    摘要： The invention relates to a method for producing cyclohexane by isomerizing a hydrocarbon mixture (KG1) containing methylcyclopentane (MCP) in the presence of a catalyst. The catalyst is preferably an acidic ionic liquid. A flow (S1) originating from a steam cracking process is used as a starting material. The hydrocarbon mixture (KG1) is obtained from said stream (S1) in a device for removing aromatics. The hydrocarbon mixture has a reduced aromatic content in comparison with the flow (S1). (KG1) can also be (nearly) free of aromatics. In dependence on the type and amount of the aromatics remaining in the hydrocarbon mixture (KG1), in particular if benzene is present, a hydrogenation of (KG1) additionally can be performed before the isomerization. Furthermore, additional purification steps can optionally be performed before or after the isomerization or hydrogenation in dependence on the presence of other components of (KG1). Preferably high-purity cyclohexane (in accordance with specifications) is isolated from the hydrocarbon mixture (KG2) arising during the isomerization, wherein the specifications are given, for example, by the use of the cyclohexane for the production of caprolactam known to the person skilled in the art.

    摘要翻译： 本发明涉及一种通过含异构化在催化剂的存在下的烃混合物（KG1）甲基环戊烷（MCP）生产环己烷。 催化剂较好是在酸性离子液体。 从蒸汽裂解过程的流程（S1）源自被用作起始材料。 烃混合物（KG1）从所述流（S1）在一个设备中获得用于除去芳族化合物。 烃混合物具有与所述流（S1）相比较减少的芳族含量。 因此（KG1）可以（几乎）不含芳香烃。 在剩余在烃混合物（KG1）的芳族化合物的类型和量的依赖性，特别是如果是苯存在的（KG1）氢化另外可在异构化之前进行。 进一步，另外的纯化步骤可任选的异构化或氢化之前或之后执行。在依赖（KG1）的其它组分的存在。 优选高纯度的环己烷（与规格雅舞蹈）从烃混合物（KG 2）的异构化，worin规格中给出，对于实施例中所产生，通过使用环己烷为已知的本领域技术人员生产己内酰胺的分离 的技术人员。

    VERFAHREN ZUR HERSTELLUNG VON ISOPROPANOL UND 2-BUTANOL AUS DEN ENTSPRECHENDEN ALKANEN
    6.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON ISOPROPANOL UND 2-BUTANOL AUS DEN ENTSPRECHENDEN ALKANEN 审中-公开
    用于从相应的烷烃产生异丙醇和2-丁醇

    公开(公告)号：EP2046706A1

    公开(公告)日：2009-04-15

    申请号：EP07787557.3

    申请日：2007-07-16

    申请人： BASF SE

    发明人： DEGEN, Georg ,  CRONE, Sven ,  BOEHLING, Ralf ,  ALTENHOFF, Ansgar Gereon ,  ROHDE, Wolfgang ,  BUERKLE, Jochen ,  SCHINDLER, Goetz-Peter ,  HOLTMANN, Thomas ,  SCHMITT, Markus

    IPC分类号： C07C29/09 ,  C07C31/10 ,  C07C31/12 ,  C07C5/333 ,  C07C11/06 ,  C07C11/08 ,  C07C67/04 ,  C07C69/06 ,  C07C69/14 ,  C07C51/09 ,  C07C53/02 ,  C07C53/08

    CPC分类号： C07C67/04 ,  C07C29/095 ,  Y02P20/127 ,  C07C31/10 ,  C07C31/12 ,  C07C69/06 ,  C07C69/14

    摘要： A process for preparing alkanols (I) selected from the group consisting of isopropanol and 2-butanol from the corresponding alkanes (II) selected from the group consisting of propane and n-butane, comprising the steps of: A) a use gas stream a comprising the alkane (II) is provided; B) use gas stream a comprising the alkane (II) is fed into a dehydrogenation zone and the alkane (II) is subjected to a dehydrogenation to the alkene (III), to obtain a product gas stream b comprising the alkene (III), unconverted alkane (II), with or without high boilers, steam, hydrogen and low boilers; C) product gas stream b is at least compressed, and product gas stream b is optionally separated into an aqueous phase c1, a phase c2 which comprises the alkene (III) and the alkane (II), with or without high boilers, and a gas phase c3 comprising hydrogen and low boilers; D) product gas stream b or the phase c2 comprising alkene (III) and alkane (II) is reacted in an esterification zone with an organic acid (IV) to obtain a product mixture d comprising the corresponding alkyl ester (V) of the organic acid and the unconverted alkane (II); E) a gas stream e1 comprising alkane (II) is removed from the product mixture d and is optionally recycled into the dehydrogenation zone, and a product mixture e2 comprising the alkyl ester is obtained; F) product mixture e2 comprising the alkyl ester is reacted in a deesterification zone with water to give a product mixture f comprising the alkanol (I) and the organic acid (IV); G) the alkanol (I) and the organic acid (IV) are removed from the product mixture f, and the organic acid is optionally recycled into the esterification zone.

    VERFAHREN ZUR HERSTELLUNG VON CYCLOHEXAN MIT EINER VORABTRENNUNG VON DIMETHYLPENTANEN
    7.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON CYCLOHEXAN MIT EINER VORABTRENNUNG VON DIMETHYLPENTANEN 审中-公开

    公开(公告)号：EP2909158A1

    公开(公告)日：2015-08-26

    申请号：EP13779553.0

    申请日：2013-10-16

    申请人： BASF SE

    发明人： SCHMITT, Markus ,  SPUHL, Katharina ,  BÜRKLE, Jochen ,  BITTERLICH, Stefan ,  TSCHIRSCHWITZ, Steffen ,  HÜBNER, Michael ,  CZAJKA, Pawel

    IPC分类号： C07C5/10 ,  C07C5/29

    CPC分类号： C07C5/10 ,  C07C5/29 ,  C07C7/08 ,  C07C2523/755 ,  C07C2601/14 ,  C07C13/18

    摘要： The present invention relates to a method for producing cyclohexane from benzene and/or methylcyclopentane (MCP) by hydrogenation or isomerisation. Prior to cyclohexane production, the dimethylpentanes (DMP) are separated in a distillation device (D1) from a hydrocarbon mixture (KG1) which contains DMP in addition to benzene and/or MCP. If cyclohexane is already present in the hydrocarbon mixture (KG1), the cyclohexane is separated initially with DMP in conjunction with benzene and/or MCP. The already present cyclohexane can be re-separated from DMP in a subsequent distillation step and can be recycled into the process in order to produce cyclohexane.

    摘要翻译： 本发明涉及通过氢化或异构化从苯和/或甲基环戊烷（MCP）生产环己烷的方法。 在环己烷生产之前，二甲基戊烷（DMP）在蒸馏装置（D1）中除与苯和/或MCP以外含有DMP的烃混合物（KG1）分离。 如果烃混合物（KG1）中已经存在环己烷，则首先用DMP和苯和/或MCP分离环己烷。 已经存在的环己烷可以在随后的蒸馏步骤中从DMP中重新分离，并且可以再循环到该方法中以产生环己烷。

    VERFAHREN ZUR HERSTELLUNG VON ISOPROPANOL UND 2-BUTANOL AUS DEN ENTSPRECHENDEN ALKANEN
    9.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON ISOPROPANOL UND 2-BUTANOL AUS DEN ENTSPRECHENDEN ALKANEN 审中-公开
    用于从相应的烷烃产生异丙醇和2-丁醇

    公开(公告)号：EP2220016A1

    公开(公告)日：2010-08-25

    申请号：EP08859972.5

    申请日：2008-12-09

    申请人： BASF SE

    发明人： ROHDE, Wolfgang ,  SCHMITT, Markus ,  HOLTMANN, Thomas ,  ALTENHOFF, Ansgar Gereon ,  DEGEN, Georg ,  BÜRKLE, Jochen ,  CRONE, Sven

    IPC分类号： C07C29/09 ,  C07C31/10 ,  C07C31/12 ,  C07C5/333 ,  C07C11/06 ,  C07C11/08 ,  C07C67/04 ,  C07C69/06 ,  C07C69/14 ,  C07C51/09 ,  C07C53/02 ,  C07C53/08

    CPC分类号： C07C29/095 ,  C07C5/333 ,  C07C5/48 ,  C07C67/04 ,  Y02P20/127 ,  C07C11/06 ,  C07C11/08 ,  C07C31/10 ,  C07C31/12 ,  C07C69/24

    摘要： The invention relates to a method for producing alcohols (I), selected from isopropanol and 2-butanol, from the corresponding alkanes (II), selected from propane and n-butane, comprising the steps: A) a feed stream a, comprising the alkane (II) is prepared, B) the feed stream a, comprising the alkane (II) is introduced into a dehydrogenation zone and the alkane (II) subjected to a dehydrogenation to give the alkene (III), wherein a product gas stream b containing the alkene (III), unreacted alkane (II), optional high-boilers, steam, hydrogen and low-boilers is obtained, C) the product gas stream b is at least compressed, the product gas stream b is optionally separated into an aqueous phase c1, a phase c2, comprising the alkene (III), the alkane (II) and optionally high-boilers and a gas phase c3, comprising hydrogen and low-boilers, D) the product gas stream b and/or the phase c2, comprising the alkene (III) and alkane (II) is reacted in an esterification zone with an alkanoic acid (IV) having 3 or more carbon atoms, wherein a product mixture d, comprising the corresponding alkyl ester (V) of the alkanoic acid and the unreacted alkane (II) is obtained, E) a gas stream e1 comprising an alkane (II) is separated off from the product mixture d, optionally recycled back to the dehydrogenation zone and a product mixture e2, comprising the alkyl ester (V) is obtained; F) the product mixture e2, comprising the alkyl ester (V) is reacted with water in an ester cleavage zone to give a product mixture f containing the alcohol (I) and the alkanoic acid (IV), G) the alcohol (I) and the alkanoic acid (IV) are separated off from the product mixture f and the alkanoic acid optionally recycled to the esterification zone.