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    PROCESS FOR MAKING PHENOL AND/OR CYCLOHEXANONE
    1.
    发明公开
    PROCESS FOR MAKING PHENOL AND/OR CYCLOHEXANONE 审中-公开
    制备苯酚和/或环己酮的方法

    公开(公告)号：EP3071540A2

    公开(公告)日：2016-09-28

    申请号：EP14790970.9

    申请日：2014-10-17

    申请人： ExxonMobil Chemical Patents Inc.

    发明人： DAKKA, Jihad M. ,  PATEL, Bryan A.

    IPC分类号： C07C37/08 ,  C07C37/72 ,  C07C45/53 ,  C07C407/00 ,  C07C49/403 ,  C07C409/14 ,  C07C7/10

    CPC分类号： C07C37/08 ,  B01J31/0247 ,  C07C7/10 ,  C07C37/72 ,  C07C45/53 ,  C07C407/00 ,  C07C407/003 ,  C07C2601/14 ,  C07C2601/16 ,  Y02P20/52 ,  C07C39/04 ,  C07C409/14 ,  C07C49/403 ,  C07C13/28

    摘要： A process for making phenol and/or cyclohexanone comprises: (A) oxidizing a cyclohexylbenzene feed to obtain an oxidation product comprising cyclohexylbenzene, cyclohexyl-1-phenyl-1-hydroperoxide and phenol; (B) separating at least a portion of the oxidation product to obtain a first fraction comprising cyclohexyl-1-phenyl-1-hydroperoxide and a second fraction comprising cyclohexylbenzene and phenol; (C) removing at least a portion of the phenol from at least a portion of the second fraction to obtain a third fraction; (D) recycling at least a portion of the cyclohexylbenzene in the third fraction to the oxidizing step (A); and (E) contacting at least a portion of the cyclohexyl-1-phenyl-1-hydroperoxide in the first fraction with an acid catalyst in a cleavage reactor under cleavage conditions to obtain a cleavage product comprising phenol and cyclohexanone.

    摘要翻译： 制备苯酚和/或环己酮的方法包括：（A）氧化环己基苯进料以获得包含环己基苯，环己基-1-苯基-1-氢过氧化物和苯酚的氧化产物; （B）分离至少一部分氧化产物以获得包含环己基-1-苯基-1-氢过氧化物的第一馏分和包含环己基苯和苯酚的第二馏分; （C）从所述第二馏分的至少一部分除去至少一部分所述酚以获得第三馏分; （D）将第三馏分中的至少一部分环己基苯循环至氧化步骤（A）; 和（E）在裂解反应条件下，在裂解反应器中使第一馏分中的至少一部分环己基-1-苯基-1-氢过氧化物与酸催化剂接触以获得包含苯酚和环己酮的裂解产物。

    PROCESS FOR PRODUCING CYCLOHEXANONE
    4.
    发明公开
    PROCESS FOR PRODUCING CYCLOHEXANONE 审中-公开
    VERFAHREN ZUR HERSTELLUNG VON CYCLOHEXANON

    公开(公告)号：EP2303822A1

    公开(公告)日：2011-04-06

    申请号：EP09739316.9

    申请日：2009-02-19

    申请人： ExxonMobil Chemical Patents Inc.

    发明人： DAKKA, Jihad M. ,  BUCHANAN, John Scott ,  LATTNER, James R. ,  MIZRAHI, Sadi

    IPC分类号： C07C45/53 ,  C07C45/00 ,  C07C49/403

    CPC分类号： C07C409/14 ,  C07C37/07 ,  C07C37/08 ,  C07C45/006 ,  C07C45/53 ,  C07C407/00 ,  C07C2601/14 ,  C07C49/403 ,  C07C39/04

    摘要： In a process for producing cyclohexanone, cyclohexylbenzene is oxidized to produce cyclohexylbenzene hydroperoxide and then the resultant cyclohexylbenzene hydroperoxide is cleaved to produce an effluent stream comprising phenol and cyclohexanone. At least a portion of the effluent stream is then fed to at least one hydrogenation reaction zone, where the effluent stream portion is contacted with hydrogen in the presence of a hydrogenation catalyst under conditions effective to convert at least part of the phenol in the effluent portion into cyclohexanone.

    摘要翻译： 在制备环己酮的方法中，将环己基苯氧化生产环己基苯氢过氧化物，然后将所得环己基苯氢过氧化物切割，以产生包含苯酚和环己酮的流出料流。 然后将至少一部分流出物流进料至至少一个氢化反应区，其中流出物流部分在氢化催化剂存在下与氢气接触，在有效地将至少部分苯酚在流出物部分 加入环己酮。

    PROCESS FOR PRODUCING PHENOL AND METHYL ETHYL KETONE
    8.
    发明公开
    PROCESS FOR PRODUCING PHENOL AND METHYL ETHYL KETONE 审中-公开
    生产苯酚和甲基乙基酮的方法

    公开(公告)号：EP1984315A1

    公开(公告)日：2008-10-29

    申请号：EP07711514.5

    申请日：2007-02-08

    申请人： ExxonMobil Chemical Patents Inc. ,  Exxonmobil Chemical Limited

    发明人： DAKKA, Jihad M. ,  STANAT, Jon E. ,  BENITEZ, Francisco M. ,  BUCHANAN, John S. ,  CHENG, Jane C. ,  ELKS, Jeffrey T.

    IPC分类号： C07C37/08 ,  C07C39/04 ,  C07C45/53 ,  C07C49/10 ,  C07C2/66 ,  C07C15/02 ,  C07C409/08

    CPC分类号： C07C409/08 ,  C07C37/08 ,  C07C45/53 ,  C07C407/00 ,  C07C49/10 ,  C07C39/04

    摘要： A process for producing phenol and methyl ethyl ketone comprises contacting benzene and a C4 alkylating agent under alkylation conditions and in the presence of an alkylation catalyst comprising at least one molecular sieve of the MCM-22 family to produce an alkylation effluent comprising secbutylbenzene; wherein the contacting is conducted in a plurality of reaction zones and the C4 alkylating agent is supplied to each of the reaction zones. A secbutylbenzene fraction is recovered from the alkylation effluent and comprises at least 95 wt% sec-butylbenzene, less than 100 wt ppm of C8+ olefins, and less than 0.5 wt% of isobutylbenzene and tert-butylbenzene. The sec-butylbenzene fraction is then oxidized to produce sec-butylbenzene hydroperoxide and the hydroperoxide is cleaved to produce phenol and methyl ethyl ketone.

    摘要翻译： 生产苯酚和甲基乙基酮的方法包括在烷基化条件下并且在包含至少一种MCM-22家族的分子筛的烷基化催化剂的存在下使苯和C4烷基化剂接触以产生包含仲丁基苯的烷基化流出物; 其中所述接触在多个反应区中进行，并且所述C4烷基化剂被供应至每个反应区。 从烷基化流出物中回收仲丁基苯馏分，并包含至少95重量％的仲丁基苯，小于100重量ppm的C8 +烯烃和小于0.5重量％的异丁基苯和叔丁基苯。 然后将仲丁基苯馏分氧化生成仲丁基苯氢过氧化物，并将氢过氧化物裂解生成苯酚和甲基乙基酮。

    PRODUCTION OF BIPHENYL COMPOUNDS
    10.
    发明公开
    PRODUCTION OF BIPHENYL COMPOUNDS 审中-公开
    联苯基化合物的生产

    公开(公告)号：EP3274318A1

    公开(公告)日：2018-01-31

    申请号：EP15823117.5

    申请日：2015-12-21

    申请人： ExxonMobil Chemical Patents Inc.

    发明人： SALCICCIOLI, Michael ,  DAKKA, Jihad M. ,  SANGAR, Neeraj ,  DECAUL, Lorenzo C. ,  KHEIR, Ali A.

    IPC分类号： C07C2/74 ,  C07C5/367 ,  C07C13/28 ,  C07C15/14

    摘要： In a process for producing biphenyl compounds, a Cn aromatic hydrocarbon may be hydroalkylated to give C2n cycloalkylaromatic compounds and byproduct Cn saturated cyclic hydrocarbons. The C2n cycloalkylaromatic compounds are dehydrogenated to provide the biphenyl compounds. The Cn saturated cyclic hydrocarbons may also be dehydrogenated back to the corresponding Cn aromatic hydrocarbon, which may be recycled to provide additional feed. Although both the intermediate C2n cycloalkylaromatic compounds and the byproduct Cn saturated cyclic hydrocarbons should be dehydrogenated, at least part of the dehydrogenation of the Cn saturated cyclic hydrocarbons should take place in the absence of C2n or greater hydrocarbons. Thus, dehydrogenation of the byproduct Cn saturated cyclic hydrocarbons should take place at least in part separately from dehydrogenation of the C2n cycloalkylaromatic compounds.