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1.发明公开PROCESSES FOR PREPARING COLOR STABLE MANGANESE-DOPED COMPLEX FLUORIDE PHOSPHORS 有权VERFAHREN ZUR HERSTELLUNG VON FARBSTABILEN MANGANDOTIERTEN KOMPLEXEN FLUORIDLEUCHTSTOFFEN
公开(公告)号：EP3080230A1
公开(公告)日：2016-10-19
申请号：EP14821427.3
申请日：2014-12-12
IPC分类号： C09K11/61
CPC分类号： C09K11/616 , H01L33/502 , H01L33/507 , H01L2224/48247 , H01L2224/48257 , H01L2924/181 , H01L2924/00012
摘要： A process for preparing a color stable Mn
4+ doped complex fluoride phosphor of formula (I) includes: A
x (M
(1-m) , Mn
m ) F
y ; contacting a first aqueous HF solution comprising (1-m) parts of a compound of formula H
x MF
y , and a second aqueous HF solution comprising m*n parts of a compound of formula A
x [MnF
y ], with a third aqueous HF solution comprising (1 -n) parts of the compound of formula A
x [MnF
y ] and a compound of formula A
a X, to yield a precipitate comprising the color stable Mn
4+ doped complex fluoride phosphor; wherein A is Li, Na, K, Rb, Cs, NR
4 or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; R is H, lower alkyl, or a combination thereof; X is an anion; a is the absolute value of the charge of the X anion; x is the absolute value of the charge of the [MF
y ] ion; y is 5, 6 or 7; 0摘要翻译： 制备式I的颜色稳定的Mn4 +掺杂复合氟化物荧光体的方法包括与包含（1-m）份式H x M F y的化合物的第一HF水溶液接触的M 1（M（1-m），M nm） 和包含m * n个分子式Ax [MnFy]化合物的第二HF水溶液与包含（1-n）份式Ax [MnF y]化合物和式AaX化合物的第三HF水溶液 以产生包含颜色稳定的Mn4 +掺杂的复合氟化物荧光体的沉淀物; 其中A为Li，Na，K，Rb，Cs，NR4或其组合; M是Si，Ge，Sn，Ti，Zr，Al，Ga，In，Sc，Hf，Y，La，Nb，Ta，Bi，Gd或它们的组合; R为H，低级烷基或其组合; X是阴离子; a是X阴离子电荷的绝对值; x是[MFy]离子的电荷的绝对值; y为5,6或7; 0
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公开(公告)号：EP3303516A1
公开(公告)日：2018-04-11
申请号：EP16723922.7
申请日：2016-05-11
发明人： DU, Fangming , BEERS, William Winder , COHEN, William Erwin , NELSON, Clark David , NOVAK, Jenna Marie , ROOT, John Matthew , MURPHY, James Edward , SISTA, Sriniva Prasad
IPC分类号： C09K11/61
CPC分类号： C09K11/616 , C09K11/617
摘要： A process for preparing a Mn+4 doped phosphor of formula: Ax [MFy]:Mn+4, includes gradually adding a first solution to a second solution and periodically discharging the product liquor from the reactor while volume of the product liquor in the reactor remains constant; wherein A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7. The first solution includes a source of M and HF and the second solution includes a source of Mn to a reactor in the presence of a source of A.
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公开(公告)号：EP3230405A1
公开(公告)日：2017-10-18
申请号：EP15816931.8
申请日：2015-11-24
发明人： SRIVASTAVA, Alok, Mani , COMANZO, Holly, Ann , BEERS, William, Winder , CAMARDELLO, Samuel, Joseph , DU, Fangming , COHEN, William, Erwin
CPC分类号： H01L33/504 , C04B35/5152 , C04B35/6262 , C04B35/6268 , C04B2235/3206 , C04B2235/3208 , C04B2235/3213 , C04B2235/3215 , C04B2235/3224 , C04B2235/3284 , C04B2235/3287 , C04B2235/3418 , C09K11/7733 , C09K11/7734 , C09K11/7735 , H01L33/50 , H01L33/502 , H01L33/505 , Y02B20/181
摘要： A phosphor composition is disclosed. A phosphor composition, comprises at least 10 atomic % bromine; silicon, germanium or combination thereof; oxygen; a metal M, wherein M comprises zinc (Zn), magnesium (Mg), calcium (Ca), strontium (Sr), barium (Ba), or combinations thereof; and an activator comprising europium. The phosphor composition is formed from combining carbonate or oxides of metal M, silicon oxide, and europium oxide; and then firing the combination. A lighting apparatus including the phosphor composition is also provided. The phosphor composition may be combined with an additional phosphor to generate white light.
摘要翻译： 公开了一种磷光体组合物。 磷光体组合物包含至少10原子％的溴; 硅，锗或其组合; 氧; 金属M，其中M包括锌（Zn），镁（Mg），钙（Ca），锶（Sr），钡（Ba）或其组合; 和包含铕的活化剂。 磷光体组合物由结合金属M，氧化硅和氧化铕的碳酸盐或氧化物形成; 然后发射组合。 还提供了包括该荧光体组合物的照明设备。 磷光体组合物可以与另外的磷光体组合以产生白光。
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公开(公告)号：EP2970765B1
公开(公告)日：2019-05-08
申请号：EP14720825.0
申请日：2014-03-14
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公开(公告)号：EP3080230B1
公开(公告)日：2018-07-04
申请号：EP14821427.3
申请日：2014-12-12
CPC分类号： C09K11/616 , H01L33/502 , H01L33/507 , H01L2224/48247 , H01L2224/48257 , H01L2924/181 , H01L2924/00012
摘要： A process for preparing a color stable Mn4+ doped complex fluoride phosphor of formula I includes Ax(M(1−m), Mnm)Fy (I) contacting a first aqueous HF solution comprising (1−m) parts of a compound of formula HxMFy, and a second aqueous HF solution comprising m*n parts of a compound of formula Ax[MnFy], with a third aqueous HF solution comprising (1−n) parts of the compound of formula Ax[MnFy] and a compound of formula AaX, to yield a precipitate comprising the color stable Mn4+ doped complex fluoride phosphor; wherein A is Li, Na, K, Rb, Cs, NR4 or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; R is H, lower alkyl, or a combination thereof; X is an anion; a is the absolute value of the charge of the X anion; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7; 0
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公开(公告)号：EP3313959A1
公开(公告)日：2018-05-02
申请号：EP16727092.5
申请日：2016-05-24
发明人： CAMARDELLO, Samuel, Joseph , SRIVASTAVA, Alok, Mani , DU, Fangming , COMANZO, Holly, Ann , BEERS, William, Winder , COHEN, William, Erwin
IPC分类号： C09K11/59
摘要： A phosphor composition is presented. The phosphor composition includes a first phosphor that includes a phase of general formula (I): L3ZO4(Br2-nXn): Eu2+(I) wherein 0 ≤ n ≤ 1; L is Zn, Mg, Ca, Sr, Ba, or combinations thereof; Z is Si, Ge, or a combination thereof; and X is F, Cl, I, or combinations thereof. A lighting apparatus that includes a light source and the phosphor composition radiationally coupled to the light source is also presented.
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公开(公告)号：EP2771429B1
公开(公告)日：2017-03-01
申请号：EP12766807.7
申请日：2012-09-17
CPC分类号： C09K11/71 , C09K11/595 , C09K11/76 , C09K11/7734 , C09K11/7777 , C09K11/778 , C09K11/7787 , H01J61/48
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公开(公告)号：EP3572480A1
公开(公告)日：2019-11-27
申请号：EP19160916.3
申请日：2014-03-14
发明人： MURPHY, James Edward , NAMMALWAR, Prasanth, Kumar , KARKADA, Nagaveni , LYONS, Robert Joseph , CHOWDHURY, Ashfaqul, Islam , SETLUR, Anant Achyut , GARCIA, Florencio , BEERS, William Winder , DU, Fangming
摘要： A lighting apparatus comprising a semiconductor light source and a color stable Mn 4+ doped phosphor of formula K 2 SiF 6 :Mn 4+ , wherein % intensity loss of the phosphor after exposure to light flux of at least 80 w/cm 2 at a temperature of at least 50ºC for at least 21 hours is ≤ 4%.
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公开(公告)号：EP2990446A1
公开(公告)日：2016-03-02
申请号：EP15182219.4
申请日：2015-08-24
CPC分类号： H01J61/44 , C03C17/23 , C03C17/3417 , C09D5/22 , C09K11/08 , C09K11/57 , C09K11/64 , C09K11/643 , H01J61/20 , H01J61/48
摘要： Coating systems suitable for use in generating fluorescent visible light, and lamps provided with such coating (22) systems. The coating systems includes a phosphor-containing coating that contains at least a first phosphor that is predominantly excited by ultraviolet radiation of a first wavelength to emit visible light and absorbs but is less efficiently excited by ultraviolet radiation of a second wavelength. The coating system further includes a second phosphor that absorbs the ultraviolet radiation of the second wavelength and little if any of the ultraviolet radiation of the first wavelength.
摘要翻译： 适用于产生荧光可见光的涂层系统，以及具有这种涂层（22）系统的灯。 涂层系统包括含磷光体的涂层，其至少包含主要由第一波长的紫外线辐射激发以发射可见光并吸收但不太有效地被第二波长的紫外线辐射激发的第一荧光体。 涂覆系统还包括第二荧光体，其吸收第二波长的紫外线辐射，并且几乎不吸收第一波长的紫外线辐射。
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公开(公告)号：EP2970765A1
公开(公告)日：2016-01-20
申请号：EP14720825.0
申请日：2014-03-14
发明人： MURPHY, James, Edward , NAMMALWAR, Prasanth, Kumar , KARKADA, Nagaveni , LYONS, Robert, Joseph , CHOWDHURY, Ashfaqul, Islam , SETLUR, Anant, Achyut , GARCIA, Florencio , BEERS, William, Winder , DU, Fangming
IPC分类号： C09K11/61
CPC分类号： H01L33/502 , C09K11/616 , C09K2211/181 , C09K2211/188 , H01L33/52 , H01L2224/48091 , H01L2224/48247 , H01L2924/181 , H01L2924/00014 , H01L2924/00012
摘要： A process for synthesizing a color stable Mn4+ doped phosphor includes contacting a precursor of formula I, in gaseous form at an elevated temperature with a fluorine-containing oxidizing agent to form the color stable Mn4+ doped phosphor Ax[MFy]:Mn4+ I wherein A is Li, Na, K, Rb, Cs, NR4 or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; R is H, lower alkyl, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; and y is 5, 6 or 7.
摘要翻译： 用于合成颜色稳定的Mn4 +掺杂荧光体的方法包括使升高温度下气态的式I前体与含氟氧化剂接触以形成颜色稳定的Mn4 +掺杂荧光体Ax [MFy]：Mn4 + I，其中A是 Li，Na，K，Rb，Cs，NR4或其组合; M是Si，Ge，Sn，Ti，Zr，Al，Ga，In，Sc，Hf，Y，La，Nb，Ta，Bi，Gd或它们的组合; R为H，低级烷基或其组合; x是[MFy]离子的电荷的绝对值; y为5,6或7。
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