Process and catalyst for determining nitrogen in a sample according to the Kjeldahl principle
    5.
    发明公开
    Process and catalyst for determining nitrogen in a sample according to the Kjeldahl principle 失效
    Verfahren und Katalysator zur Bestimmung von Stickstoff in einer ProbegemässKjeldahls Methode。

    公开(公告)号:EP0001513A1

    公开(公告)日:1979-04-18

    申请号:EP78300467.4

    申请日:1978-10-06

    CPC classification number: B01J23/18 G01N31/002 Y10T436/176152

    Abstract: In conventional Kjeldahl analysis for determining the nitrogen content of a sample, it is common practice to digest the sample in the presence of a catalyst in order to speed the analysis. The most widely used catalyst is mercuric oxide. While the use of this catalyst gives acceptable results, it is now evident that the environmental and health hazards connected with mercury compounds makes it desirable to avoid the use of large quantities of such compounds.
    It has now been found that an antimonate, preferably potassium antimonate. may be used as the catalyst to give acceptable results while avoiding the above-mentioned problems.
    Accordingly, the present invention provides, inter alia, a process for the determination of the nitrogen content of a sample according to the Kjeldahl principle using a catalyst. characterised in that the catalyst is an antimonate.
    The present invention also relates to such a catalyst and to the use thereof in such a process.

    Abstract translation: 在用于确定样品的氮含量的常规凯氏定氮分析中,通常的做法是在催化剂存在下消化样品以加速分析。 使用最广泛的催化剂是氧化汞。 尽管使用这种催化剂可以得到可以接受的结果,但现在明显的是,与汞化合物相关的环境和健康危害使得避免使用大量的这类化合物是合乎需要的。 现在已经发现,可以使用锑酸盐,优选锑酸钾作为催化剂来提供可接受的结果,同时避免上述问题。 因此,本发明尤其提供了使用催化剂根据凯氏定氮法测定样品的氮含量的方法,其特征在于催化剂是锑酸盐。 本发明还涉及这种催化剂及其在这种方法中的用途。

    A METHOD OF MEASURING SOLUBILITY
    7.
    发明公开
    A METHOD OF MEASURING SOLUBILITY 审中-公开
    方法溶解度测量

    公开(公告)号:EP1428015A4

    公开(公告)日:2008-09-17

    申请号:EP02768567

    申请日:2002-08-16

    Applicant: ANALIZA INC

    Abstract: A method of determining the solubility of a compound in a selected solvent is provided that does not require determination of, or use of, standards having known concentrations of the compound. In one aspect, the method can include preparation of a mixture where not all of a compound is dissolved in the provided solvent, separating undissolved compound from the solvent, and direct determination of the amount of the compound dissolved in the solvent. Methods adapted for use include those where a multiplicity of compounds or solvents are tested in parallel. Devices adapted for these methods are also provided by the present disclosure.

    MEASURING METHOD FOR TOTAL ORGANIC CARBON, MEASURING METHOD FOR TOTAL NITROGEN AND MEASURING APPARATUS FOR THE METHODS
    8.
    发明公开
    MEASURING METHOD FOR TOTAL ORGANIC CARBON, MEASURING METHOD FOR TOTAL NITROGEN AND MEASURING APPARATUS FOR THE METHODS 审中-公开
    测量方法的有机总碳,测量总氮和测量装置,该方法的方法

    公开(公告)号:EP1890141A1

    公开(公告)日:2008-02-20

    申请号:EP05811708.6

    申请日:2005-11-29

    Abstract: Disclosed herein is a method for measuring total organic carbon without the influence of nitrogen components. The method for measuring total organic carbon includes the steps of: (1) adjusting the hydrogen ion concentration of sample water to between pH 4 and pH 6; (2) decomposing organic matter and nitrogen compounds contained in the sample water into carbon dioxide and nitrous acid, respectively, through oxidation and; (3) making the carbon dioxide permeate into measuring water via a gas-permeable part 5a; (4) and measuring the electric conductivity of the measuring water to determine the total organic carbon content of the sample water.

    Abstract translation: 在是用于测量全有机碳,而不氮组分的本发明公开的影响的方法。 用于测量全有机碳的方法,包括以下步骤:(1)调节样品水的氢离子浓度至pH 4和pH 6之间; (2)分解包含在样品水成二氧化碳和亚硝酸,分别通过氧化和有机物和氮化合物; (3)使二氧化碳渗透到通过气体可渗透部5a测量水; (4)和测量所述测量水的电导率来确定矿井样品水的总有机碳含量。

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