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公开(公告)号:US12209156B2
公开(公告)日:2025-01-28
申请号:US17763839
申请日:2020-09-14
Applicant: ADEKA CORPORATION
Inventor: Hiromi Takenouchi , Kensaku Akimoto , Kenji Kakiage , Hirokatsu Shinano , Tomofumi Yokomizo
Abstract: The present invention provides a method of producing sulfur-modified polyacrylonitrile, including: a step (1) of heating polyacrylonitrile and elemental sulfur in a rotating-type heating container including a discharge pipe and a sulfur vapor recovery unit while rotating the rotating-type heating container; a step (2) of liquefying a sulfur vapor by the sulfur vapor recovery unit while discharging hydrogen sulfide generated in the heating step; and a step (3) of returning the liquefied sulfur to a mixture of the sulfur and the polyacrylonitrile of the step (1).
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公开(公告)号:US11223045B2
公开(公告)日:2022-01-11
申请号:US16756580
申请日:2018-10-30
Applicant: ADEKA CORPORATION
Inventor: Hirokatsu Shinano , Kenji Kakiage , Yohei Aoyama
Abstract: Disclosed is a sulfur-based electrode active material with which a nonaqueous electrolyte secondary battery that has a large capacity and exhibits less deterioration of the cycle characteristics can be obtained even when an electrode is employed in which the sulfur-based electrode active material is used as an electrode active material and an aluminum foil is used as a current collector. Also disclosed is a method for producing an organosulfur electrode active material, including a step of obtaining an organosulfur compound by heat-treating an organic compound and sulfur and a step of treating the organosulfur compound with a basic compound. The organosulfur compound is preferably sulfur-modified polyacrylonitrile, and the basic compound is preferably ammonia. The organosulfur compound may be treated with the basic compound after the organosulfur compound is ground, or may be ground in a medium that contains the basic compound.
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公开(公告)号:US10774259B2
公开(公告)日:2020-09-15
申请号:US15745968
申请日:2016-07-29
Applicant: ADEKA CORPORATION
Inventor: Masatoshi Homma , Kazuyuki Noda , Hirokatsu Shinano , Kensaku Akimoto , Daisuke Sawamoto
Abstract: An encapsulated agent includes a central part and an outer part that covers a surface of the central part. The central part contains a viscosity-reducing material that reduces viscosity of a fluid to be used in a hydrofracturing technique. The outer part contains a plurality of particulate substances and a holding material that holds the plurality of particulate substances and enables gradual release of the central part in the fluid. The outer part involves distribution of the plurality of particulate substances that allows a content to have one or more local maxima in a direction away from the central part.
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公开(公告)号:US11594732B2
公开(公告)日:2023-02-28
申请号:US16960782
申请日:2019-02-25
Applicant: ADEKA CORPORATION
Inventor: Hiromi Takenouchi , Tomofumi Yokomizo , Hirokatsu Shinano , Kenji Kakiage , Yuta Nohara , Yohei Aoyama
Abstract: Disclosed is an electrode active material that has a large charge discharge capacity, a high initial efficiency, as well as excellent cycle characteristics and rate characteristics and is favorably used in a non-aqueous electrolyte secondary battery. An organo sulfur-based electrode active material contains sodium and potassium in a total amount of 100 ppm by mass to 1000 ppm by mass; an electrode for use in a secondary battery, the electrode containing the organo sulfur-based electrode active material as an electrode active material; and a non-aqueous electrolyte secondary battery including the electrode. Preferably, the organo sulfur-based electrode active material further contains iron in an amount of 1 ppm by mass to 20 ppm by mass. Preferably, the organo sulfur-based electrode active material is sulfur-modified polyacrylonitrile, and the amount of sulfur in the organo sulfur-based electrode active material is 25 mass % to 60 mass %.
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公开(公告)号:US20150064623A1
公开(公告)日:2015-03-05
申请号:US14381772
申请日:2013-03-05
Applicant: ADEKA CORPORATION
Inventor: Takeo Oishi , Koichi Kimijima , Nobuhide Tominaga , Hirokatsu Shinano , Daisuke Sawamoto
IPC: G03F7/004 , C07D209/88 , C07D403/12
CPC classification number: G03F7/0045 , C07D209/86 , C07D209/88 , C07D211/70 , C07D233/06 , C07D241/06 , C07D401/12 , C07D403/12 , G03F7/038
Abstract: A novel compound having satisfactory sensitivity (base generating performance), a photosensitive resin composition containing the compound as a photo-initiator, and a cured product of the composition are provided. Specifically, a compound represented by general formula (1) (compound (1)), a photosensitive resin composition containing (A) a photo-initiator including at least one compound (1) and (B) a photosensitive resin are provided. Preferred are the compound (1) in which R1 is an unsubstituted or substituted C6-C20 aromatic hydrocarbon group, the compound (1) in which at least one of R5, R6, R7, R8, R9, R10, and R11 is nitro, and the compound (1) in which n is 0. The symbols in general formula (1) are as defined in the description.
Abstract translation: 提供具有令人满意的灵敏度的新化合物(碱产生性能),含有该化合物作为光引发剂的感光性树脂组合物和该组合物的固化物。 具体而言,提供由通式(1)表示的化合物(化合物(1)),含有(A)含有至少一种化合物(1)和(B)感光性树脂的光引发剂的感光性树脂组合物。 优选的是其中R 1是未取代或取代的C 6 -C 20芳族烃基的化合物(1),其中R 5,R 6,R 7,R 8,R 9,R 10和R 11中的至少一个是硝基的化合物(1) 和其中n为0的化合物(1)。通式(1)中的符号如说明书中所定义。
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公开(公告)号:US09594302B2
公开(公告)日:2017-03-14
申请号:US14381772
申请日:2013-03-05
Applicant: ADEKA CORPORATION
Inventor: Takeo Oishi , Koichi Kimijima , Nobuhide Tominaga , Hirokatsu Shinano , Daisuke Sawamoto , Kiyoshi Murata
IPC: G03F7/004 , C07D209/88 , C07D211/70 , C07D233/06 , C07D241/06 , C07D403/12 , C07D401/12 , C07D209/86 , G03F7/038
CPC classification number: G03F7/0045 , C07D209/86 , C07D209/88 , C07D211/70 , C07D233/06 , C07D241/06 , C07D401/12 , C07D403/12 , G03F7/038
Abstract: A novel compound having satisfactory sensitivity (base generating performance), a photosensitive resin composition containing the compound as a photo-initiator, and a cured product of the composition are provided. Specifically, a compound represented by general formula (1) (compound (1)), a photosensitive resin composition containing (A) a photo-initiator including at least one compound (1) and (B) a photosensitive resin are provided. Preferred are the compound (1) in which R1 is an unsubstituted or substituted C6-C20 aromatic hydrocarbon group, the compound (1) in which at least one of R5, R6, R7, R8, R9, R10, and R11 is nitro, and the compound (1) in which n is 0. The symbols in general formula (1) are as defined in the description.
Abstract translation: 通式(1)中的符号如说明书中所定义。
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