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    Process for the preparation of polyamines and their use for the preparation of polyurethanes
    1.
    发明授权
    Process for the preparation of polyamines and their use for the preparation of polyurethanes 失效
    制备多胺的方法及其用于制备聚氨酯的用途

    公开(公告)号：US4843107A

    公开(公告)日：1989-06-27

    申请号：US173204

    申请日：1988-03-24

    申请人： Andreas Ruckes ,  Werner Rasshofer ,  Klaus Konig ,  Richard Kopp

    发明人： Andreas Ruckes ,  Werner Rasshofer ,  Klaus Konig ,  Richard Kopp

    IPC分类号： C08G18/64 ,  C08G18/10 ,  C08G18/50 ,  C08G73/02

    CPC分类号： C08G18/5048 ,  C08G18/10

    摘要： Polyamines containing primary amino groups are made by a one-shot process for the hydrolysis of prepolymers containing isocyanate end groups and having an isocyanate content of from 0.5 to 40 weight % with 0.75 to 40 mol of water per equivalent of isocyanate groups in the presence of very small quantities of sodium hydroxide in certain organic, polar solvents. The compounds containing isocyanate groups used for this process are isocyanate prepolymers (preferably containing urethane groups). Hydrolysis according to this process leads directly to the polyamines with elimination of carbon dioxide. These polyamines may be isolated by the usual methods and the removal of the small quantities of catalyst may advantageously be omitted. These polyamines are useful for the preparation of polyurethane(urea)s.

    摘要翻译： 含有伯氨基的多胺通过一步法制备，用于水解包含异氰酸酯端基并且异氰酸酯含量为0.5至40重量％的预聚物，每当异氰酸酯基为0.75至40摩尔水时， 某些有机极性溶剂中极少量的氢氧化钠。 用于该方法的含有异氰酸酯基团的化合物是异氰酸酯预聚物（优选含有氨基甲酸酯基团）。 根据该方法的水解直接导致多胺消除二氧化碳。 这些多胺可以通过常规方法分离，并且可以有利地省略少量催化剂的去除。 这些多胺可用于制备聚氨酯（尿素）。

    Process for the production of polyamines
    3.
    发明授权
    Process for the production of polyamines 失效
    多胺生产工艺

    公开(公告)号：US4843108A

    公开(公告)日：1989-06-27

    申请号：US173350

    申请日：1988-03-24

    申请人： Andreas Ruckes ,  Werner Rasshofer ,  Klaus Konig ,  Richard Kopp

    发明人： Andreas Ruckes ,  Werner Rasshofer ,  Klaus Konig ,  Richard Kopp

    IPC分类号： C08G18/08 ,  C08G18/00 ,  C08G18/10 ,  C08G18/30 ,  C08G18/32 ,  C08G18/40 ,  C08G18/50 ,  C08G18/64

    CPC分类号： C08G18/5048 ,  C08G18/10

    摘要： Polyamines are produced by hydrolyzing isocyanate compounds having an NCO content of from 0.5 to 40 wt. % with from 0.75 to 40 moles of water per equivalent of NCO groups in the presence of from 0.021 to 0.099 wt. % sodium hydroxide and at least 10 wt. % water-miscible polar organic solvent containing nitrile, ketone, sulfoxide or ether groups having a boiling point of from 56.degree. to 250.degree. C. The reaction mixture is maintained in a homogeneous phase. The reaction is carried out at 40.degree. to 170.degree. C. These polyamines are useful in the production of polyurethane(urea)s.

    摘要翻译： 多胺通过水解NCO含量为0.5〜40重量％的异氰酸酯化合物来制造。 在0.021至0.099重量％的存在下，每当量NCO基团具有0.75至40摩尔水。 ％氢氧化钠和至少10wt。 含有沸点为56〜250℃的腈，酮，亚砜或醚基的％水混溶性极性有机溶剂。将反应混合物保持在均匀相中。 反应在40℃至170℃下进行。这些多胺可用于生产聚氨酯（尿素）。

    Process for the preparation of highly elastic plastics
    6.
    发明授权
    Process for the preparation of highly elastic plastics 失效
    制备高弹性塑料的方法

    公开(公告)号：US5159046A

    公开(公告)日：1992-10-27

    申请号：US543649

    申请日：1990-06-26

    申请人： Gerhard Grogler ,  Andreas Ruckes ,  Richard Kopp ,  Heinrich Hess ,  Robert Eiben ,  James M. Barnes

    发明人： Gerhard Grogler ,  Andreas Ruckes ,  Richard Kopp ,  Heinrich Hess ,  Robert Eiben ,  James M. Barnes

    IPC分类号： C07C275/62 ,  C07C273/18 ,  C08G18/70 ,  C08G18/78 ,  C08G18/80

    CPC分类号： C07C273/1809 ,  C07C273/1872 ,  C08G18/703 ,  C08G18/707 ,  C08G18/7818 ,  C08G18/8045

    摘要： The present invention relates to a process for the preparation of a modified 1,5-naphthylene diisocyanate containing urea and biuret groups comprising reacting(a) 1,5-naphthylene diisocyanate in molten form with(b) a mixture comprising about 0.02 to about 0.5 mole of water per mole of 1,5-naphthylene diisocyanate and about 1 to about 10 parts for each part of water of an organic solvent.The present invention further relates to a process for the preparation of elastomeric moldings comprising reacting by the one-shot or prepolymer process at an isocyanate index of 70 to 130 a modified 1,5-naphthylene diisocyanate containing urea and biuret groups with compounds containing at least two isocyanate-reactive groups and having a molecular weight in the range from about 500 to about 10,000 and, optionally, organic compounds containing isocyanate-reactive groups and having a molecular weight in the range from 60 to 499.

    摘要翻译： 本发明涉及一种制备含脲和缩二脲基团的改性的1,5-亚萘基二异氰酸酯的方法，包括使（a）熔融形式的1,5-亚萘基二异氰酸酯与（b）约0.02至约0.5的混合物 摩尔水/摩尔1,5-亚萘基二异氰酸酯和约1至约10份的每份有机溶剂的水。 本发明还涉及一种制备弹性体模制品的方法，其包括通过一步或预聚物方法在异氰酸酯指数为70至130的情况下使含有脲和缩二脲基团的改性的1,5-亚萘基二异氰酸酯与至少含有化合物 两个异氰酸酯反应性基团，分子量在约500至约10,000的范围内，以及任选的含有异氰酸酯反应性基团并且分子量在60至499范围内的有机化合物。

    Process for the production of N,N'-bis-(3-aminophenyl)-ureas
    9.
    发明授权
    Process for the production of N,N'-bis-(3-aminophenyl)-ureas 失效
    制备N，N'-二 - （3-氨基苯基） - 脲的方法

    公开(公告)号：US4994611A

    公开(公告)日：1991-02-19

    申请号：US436393

    申请日：1989-11-14

    申请人： Andreas Ruckes ,  Gerhard Grogler ,  Richard Kopp

    发明人： Andreas Ruckes ,  Gerhard Grogler ,  Richard Kopp

    IPC分类号： C07C273/18 ,  C07C275/40

    CPC分类号： C07C273/1854

    摘要： The present invention is directed to a process for the preparation of N,N'-bis-(3-aminophenyl)-ureas corresponding to formula (I) ##STR1## wherein R represents a linear or branched C.sub.1 -C.sub.6 alkyl group which is in the 2-, 4- and/or 6-position,characterized in that the corresponding phenylene diamines are reacted with urea in a molar ratio of greater than 2:1 in chlorobenzene as solvent.

    摘要翻译： 本发明涉及一种制备对应于式（I）的N，N'-双 - （3-氨基苯基） - 脲的方法，其中R表示直链或支链的C 1 -C 6烷基 其位于2-，4-和/或6-位，其特征在于相应的亚苯基二胺在氯苯作为溶剂中以大于2:1的摩尔比与脲反应。

    Process for the production of cold-setting polyurethane urea elastomers
    10.
    发明授权
    Process for the production of cold-setting polyurethane urea elastomers 失效
    生产冷凝聚氨酯脲弹性体的方法

    公开(公告)号：US4882411A

    公开(公告)日：1989-11-21

    申请号：US245877

    申请日：1988-09-16

    申请人： Gerhard Grogler ,  Andreas Ruckes ,  Heinrich Hess ,  Richard Kopp

    发明人： Gerhard Grogler ,  Andreas Ruckes ,  Heinrich Hess ,  Richard Kopp

    IPC分类号： C08G18/66 ,  C08G18/10 ,  C08G18/48 ,  C08G18/65

    CPC分类号： C08G18/4837 ,  C08G18/10

    摘要： The present invention relates to a process for the production of polyurethane urea elastomers from(a) NCO-terminated prepolymers based on polyisocyanates and polyethers having a molecular weight of 400 to about 10,000 and an ethylene oxide content of about 10 to 60 mole-% and(b) solid diaminodiphenyl ureas corresponding to the formula ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 may be the same or different and represent hydrogen or C.sub.1 -C.sub.6 alkyl radicals and wherein the amino groups are in the m-and/or p-position to the urea group,characterized in that the NCO prepolymers are reacted with the diaminodiphenyl ureas in powder-form in a heterogeneous phase at temperatures of about 5.degree. to 40.degree. C.The present invention is also directed to the polyurethane urea elastomers prepared by this process.

    摘要翻译： 本发明涉及从（a）基于聚异氰酸酯和聚醚的分子量为400至约10,000并且环氧乙烷含量为约10至60摩尔％的NCO封端的预聚物制备聚氨酯脲弹性体的方法，以及 （b）对应于式“IMAGE”的固体二氨基二苯脲，其中R 1，R 2，R 3和R 4可以相同或不同，表示氢或C 1 -C 6烷基，并且其中氨基在m-和/或p 位置，其特征在于NCO预聚物与二氨基二苯基脲在非常相中以粉末形式在约5℃至40℃的温度下反应。本发明还涉及制备的聚氨酯脲弹性体 通过这个过程。