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40 条记录 (耗时 0.016 秒)

    Two-component polyurethane adhesive
    1.
    发明授权
    Two-component polyurethane adhesive 失效
    双组分聚氨酯胶粘剂

    公开(公告)号：US5204439A

    公开(公告)日：1993-04-20

    申请号：US932173

    申请日：1992-08-19

    申请人： Jeffrey F. Dormish ,  Peter W. Boerner ,  Randall C. Rains

    发明人： Jeffrey F. Dormish ,  Peter W. Boerner ,  Randall C. Rains

    IPC分类号： C08G18/10 ,  C08G18/48 ,  C08G18/50 ,  C08G18/66 ,  C08G18/76 ,  C09J175/08 ,  C09J175/12

    CPC分类号： C09J175/08 ,  C08G18/10 ,  C08G18/482 ,  C08G18/5048 ,  C08G18/6685 ,  C08G18/7664 ,  C09J175/12

    摘要： This invention relates to a low-viscosity two-component filled polyurethane adhesive comprising(a) a low-viscosity isocyanate component in a quantity sufficient to provide an isocyanate index of about 100 to about 150 comprising an organic polyisocyanate wherein up to 10 equivalent percent of the isocyanate groups of said organic polyisocyanate have been modified by reaction with one or more isocyanate-reactive compounds; and(b) a low-viscosity curative component comprising(i) 5 to 50 equivalent percent, based on the total equivalents of amino and hydroxyl groups of components (b)(i) and (b)(ii), of a polyether polyol and/or a polyether terminated by aromatic amino groups having an equivalent weight greater than 500,(ii) 50 to 95 equivalent percent, based on the total equivalents of amino and hydroxyl groups of components (b)(i) and (b)(ii), of one or more chain extenders and/or crosslinkers, wherein at least one diol chain extender comprises from 50 to 100 percent of the isocyanate-reactive equivalents of component (b)(ii), and(iii) one or more isocyanate-reactive diamines or triamines in a quantity sufficient to produce adequate resistance to flow when components (a) and (b) are mixed;wherein at least one of components (a) or (b) contains at least one filler in a total quantity of from about 10 to about 40 percent by weight of the filled polyurethane adhesive.

    摘要翻译： 本发明涉及一种低粘度双组分填充聚氨酯粘合剂，其包含（a）足够提供约100至约150的异氰酸酯指数的低粘度异氰酸酯组分，其包含有机多异氰酸酯，其中至多10当量％ 所述有机多异氰酸酯的异氰酸酯基团通过与一种或多种异氰酸酯反应性化合物的反应而被改性; 和（b）低粘度固化剂组分，其包含（i）基于组分（b）（i）和（b）（ii））的氨基和羟基的总当量为5〜50当量的聚醚多元醇 基于组分（b）（i）和（b）（b）（i）和（b）的氨基和羟基的总当量，基于当量重量大于500的芳族氨基封端的聚醚，（ii）50至95当量％ ii）一种或多种增链剂和/或交联剂，其中至少一种二醇增链剂包含组分（b）（ii）的异氰酸酯反应当量的50-100％，和（iii）一种或多种异氰酸酯 - 反应性二胺或三胺，其量足以在组分（a）和（b）混合时产生足够的流动阻力; 其中组分（a）或（b）中的至少一种包含总量为填充的聚氨酯粘合剂的约10至约40重量％的至少一种填料。

    Hydrolysis process for polyamines
    6.
    发明授权
    Hydrolysis process for polyamines 失效
    多胺的水解过程

    公开(公告)号：US5283364A

    公开(公告)日：1994-02-01

    申请号：US4808

    申请日：1993-01-15

    申请人： Werner Rasshofer ,  Klaus Konig ,  Hans-Joachim Meiners ,  Gerhard Grogler

    发明人： Werner Rasshofer ,  Klaus Konig ,  Hans-Joachim Meiners ,  Gerhard Grogler

    IPC分类号： C08G18/10 ,  C08G18/46 ,  C08G18/50 ,  C07C85/00

    CPC分类号： C08G18/5048 ,  C08G18/10 ,  C08G18/4623

    摘要： Polyamines containing primary amino groups are made by hydrolyzing an isocyanate with water in the presence of a solvent which is a carboxylic acid amide. The solvent must be used in a quantity of at least 10% by weight solvent based on 100% by weight of isocyanate. The weight ratio of solvent to water must be from 3 to 200. A homogeneous phase is maintained during the hydrolysis which is carried out at temperatures of from 20.degree. to 210.degree. C. A not incorporable basic and/or metal catalyst particularly alkali metal hydroxides may be employed. The polyamines produced by this process are particularly useful for the production of polyurethanes.

    摘要翻译： 含羧基酰胺的溶剂存在下，通过用水水解异氰酸酯制备含有伯氨基的多胺。 溶剂必须使用至少10重量％的溶剂，基于100重量％的异氰酸酯。 溶剂与水的重量比必须为3至200.在水解期间保持均相，其在20至210℃的温度下进行。不合并的碱性和/或金属催化剂，特别是碱金属氢氧化物 可以被雇用。 通过该方法生产的多胺特别可用于生产聚氨酯。

    Polyamines and processes for the production of such polyamines and of polyurethane plastics therefrom
    9.
    发明授权
    Polyamines and processes for the production of such polyamines and of polyurethane plastics therefrom 失效
    用于生产这种多胺和聚氨酯塑料的多胺和方法

    公开(公告)号：US4386218A

    公开(公告)日：1983-05-31

    申请号：US308326

    申请日：1981-10-05

    申请人： Werner Rasshofer ,  Dieter Dieterich ,  Holger Meyborg

    发明人： Werner Rasshofer ,  Dieter Dieterich ,  Holger Meyborg

    IPC分类号： C07C275/62 ,  B01J23/02 ,  B01J31/08 ,  C07B61/00 ,  C07C271/20 ,  C07C271/26 ,  C07C273/18 ,  C07C275/00 ,  C07C275/14 ,  C08G18/00 ,  C08G18/10 ,  C08G18/32 ,  C08G18/50 ,  C08G18/65 ,  C08G18/83 ,  C07C127/15 ,  C07C127/24

    CPC分类号： C08G18/83 ,  C07C273/1809 ,  C08G18/10 ,  C08G18/5048

    摘要： A compound having a terminal isocyanate group is hydrolyzed to produce a polyamine having a urethane and/or a urea and/or a biuret group. More particularly, a carbamate is made by mixing an isocyanate prepolymer having urethane and/or urea and/or biuret groups present with aqueous base solutions at a temperature of from 0.degree. to 0.degree. C. and in quantities such that the equivalent ratio of hydroxyl to isocyanate groups is between from 0.3:1 to .gtoreq.1.01 to 1. The carbamate is then treated with an acid ion exchanger to form an amine. The amine is then removed from any other material which may be present. A preferred polyamine thus-produced corresponds to the general formula: ##STR1## in which each R radical may represent a divalent straight or branched-chain aliphatic radical; a divalent cycloaliphatic radical; a 4,4'- and/or a 2,4'-dicyclohexylmethane radical; or a 2,4- and/or 2,6-methyl cyclohexane radical. Such an amine may be reacted with a polyisocyanate and optionally with other known additives to form a polyurethane plastic or foam.

    摘要翻译： 将具有末端异氰酸酯基的化合物水解以制备具有氨基甲酸酯和/或脲和/或缩二脲基的多胺。 更具体地，氨基甲酸酯是通过在0℃至0℃的温度下混合存在有氨基甲酸酯和/或脲和/或缩二脲基的异氰酸酯预聚物和/或缩二脲基与碱水溶液形成的，其量使得羟基的当量比 到异氰酸酯基团之间的比例为0.3:1至> / = 1.01:1。然后用酸式离子交换剂处理氨基甲酸酯以形成胺。 然后将胺从可能存在的任何其它材料中除去。 如此制备的优选的多胺对应于通式：其中每个R基团可以表示二价直链或支链脂族基团; 二价脂环族基团; 4,4'-和/或2,4'-二环己基甲基基团; 或2,4-和/或2,6-甲基环己烷基。 这样的胺可以与多异氰酸酯和任选地与其它已知的添加剂反应以形成聚氨酯塑料或泡沫。

    Catalytic hydrolysis process for polyamines
    10.
    发明授权
    Catalytic hydrolysis process for polyamines 失效
    多胺催化水解过程

    公开(公告)号：US4931595A

    公开(公告)日：1990-06-05

    申请号：US389384

    申请日：1989-08-02

    申请人： Werner Rasshofer

    发明人： Werner Rasshofer

    IPC分类号： C08G18/00 ,  C07C67/00 ,  C07C209/00 ,  C07C209/62 ,  C07C211/14 ,  C08G18/08 ,  C08G18/10 ,  C08G18/18 ,  C08G18/22 ,  C08G18/50 ,  C08G18/65 ,  C08G18/83

    CPC分类号： C08G18/5048 ,  C08G18/0804 ,  C08G18/10 ,  C08G18/1825 ,  C08G18/225

    摘要： Polyamines containing primary amino groups are prepared in a single stage process by hydrolyzing an isocyanate in the presence of a catalyst incorporable through an NCO reactive group and a water-miscible aprotic-dipolar solvent. This hydrolysis is carried out at from 20.degree. to 210.degree. C. with the reactants being in substantially homogeneous phase. The isocyanate starting material has an NCO content of from 0.5 to 40% by weight. The catalyst is used in a quantity of at least 0.0001% by weight, based on 100% by weight of isocyanate compound. The water-miscible solvent is used in a quantity of at least 10% by weight, based on 100% by weight of isocyanate compound. The polyamines thus produced are particularly useful in the production of polyurethanes.

    摘要翻译： 通过在可通过NCO反应性基团和水混溶性非质子 - 偶极溶剂掺入的催化剂存在下水解异氰酸酯，在单阶段方法中制备含有伯氨基的多胺。 该水解在20至210℃下进行，反应物基本上是均匀的相。 异氰酸酯原料的NCO含量为0.5〜40重量％。 基于100重量％的异氰酸酯化合物，催化剂的用量为至少0.0001重量％。 基于100重量％的异氰酸酯化合物，水混溶性溶剂的用量至少为10重量％。 如此生产的聚胺在聚氨酯的生产中特别有用。