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    Curable compositions containing silylated polyurethanes
    1.
    发明授权
    Curable compositions containing silylated polyurethanes 有权
    含有甲硅烷基化聚氨酯的固化组合物

    公开(公告)号：US08609800B2

    公开(公告)日：2013-12-17

    申请号：US12906397

    申请日：2010-10-18

    申请人： Helene Boudet ,  Andreas Bolte ,  Thomas Bachon ,  Lars Zander ,  Christiane Kunze ,  Johann Klein ,  Nicole Ditges

    发明人： Helene Boudet ,  Andreas Bolte ,  Thomas Bachon ,  Lars Zander ,  Christiane Kunze ,  Johann Klein ,  Nicole Ditges

    IPC分类号： C08G18/83

    CPC分类号： C09J175/04 ,  C08G18/10 ,  C08G18/765 ,  C08G2190/00 ,  C08G18/289

    摘要： Silylated polyurethanes can be manufactured by reacting at least one polyol compound, having a molecular weight from 4000 to 20,000 dalton, with a diisocyanate, with a stoichiometric excess of the diisocyanate compound with respect to the polyol compound or compounds, with the result that a polyurethane prepolymer that is isocyanate-terminated is formed; and by subsequently reacting the polyurethane prepolymer with one or more OH-terminated silanes of formula (1) to yield a polyurethane having predominantly terminal alkoxysilyl groups. In formula (1), m is equal to 0, 1, or 2, R1 is an alkyl residue having 1 to 4 carbon atoms, R2 is an alkyl residue having 1 to 4 carbon atoms, R3 is a divalent organic residue having 1 to 12 atoms, selected from C, N, S, and/or O, in the chain, but by preference exclusively carbon atoms, R4 is a hydrogen atom or an alkyl residue having 1 to 10 carbon atoms, and R is a difunctional organic group, preferably a linear or branched alkyl group having 1 to 6 carbon atoms. The silylated polyurethanes are suitable for use in a preparation as an adhesive, sealant, or coating agent.

    摘要翻译： 甲硅烷基化聚氨酯可以通过使至少一种分子量为4000至20,000道尔顿的多元醇化合物与二异氰酸酯相对于多元醇化合物或化合物与化学计量过量的二异氰酸酯化合物反应而制备，结果是聚氨酯 形成异氰酸酯封端的预聚物; 并随后使聚氨酯预聚物与一种或多种式（1）的OH封端的硅烷反应，得到主要具有末端烷氧基甲硅烷基的聚氨酯。 在式（1）中，m等于0,1或2，R 1是具有1至4个碳原子的烷基，R 2是具有1至4个碳原子的烷基，R 3是具有1至 在链中选自C，N，S和/或O的12个原子，但仅仅是碳原子，R4是氢原子或具有1-10个碳原子的烷基，R是双官能有机基团 优选具有1-6个碳原子的直链或支链烷基。 甲硅烷基化聚氨酯适用于作为粘合剂，密封剂或涂层剂的制剂。

    CURABLE COMPOSITIONS CONTAINING SILYLATED POLYURETHANES
    2.
    发明申请
    CURABLE COMPOSITIONS CONTAINING SILYLATED POLYURETHANES 有权
    含有SILYLED聚氨酯的可固化组合物

    公开(公告)号：US20110034627A1

    公开(公告)日：2011-02-10

    申请号：US12906397

    申请日：2010-10-18

    申请人： Helene Boudet ,  Andreas Bolte ,  Thomas Bachon ,  Lars Zander ,  Christiane Kunze ,  Johann Klein ,  Nicole Ditges

    发明人： Helene Boudet ,  Andreas Bolte ,  Thomas Bachon ,  Lars Zander ,  Christiane Kunze ,  Johann Klein ,  Nicole Ditges

    IPC分类号： C08L83/08 ,  C08G77/22

    CPC分类号： C09J175/04 ,  C08G18/10 ,  C08G18/765 ,  C08G2190/00 ,  C08G18/289

    摘要： Silylated polyurethanes can be manufactured by reacting at least one polyol compound, having a molecular weight from 4000 to 20,000 dalton, with a diisocyanate, with a stoichiometric excess of the diisocyanate compound with respect to the polyol compound or compounds, with the result that a polyurethane prepolymer that is isocyanate-terminated is formed; and by subsequently reacting the polyurethane prepolymer with one or more OH-terminated silanes of formula (1) to yield a polyurethane having predominantly terminal alkoxysilyl groups. In formula (1), m is equal to 0, 1, or 2, R1 is an alkyl residue having 1 to 4 carbon atoms, R2 is an alkyl residue having 1 to 4 carbon atoms, R3 is a divalent organic residue having 1 to 12 atoms, selected from C, N, S, and/or O, in the chain, but by preference exclusively carbon atoms, R4 is a hydrogen atom or an alkyl residue having 1 to 10 carbon atoms, and R is a difunctional organic group, preferably a linear or branched alkyl group having 1 to 6 carbon atoms. The silylated polyurethanes are suitable for use in a preparation as an adhesive, sealant, or coating agent.

    摘要翻译： 甲硅烷基化聚氨酯可以通过使至少一种分子量为4000至20,000道尔顿的多元醇化合物与二异氰酸酯相对于多元醇化合物或化合物与化学计量过量的二异氰酸酯化合物反应而制备，结果是聚氨酯 形成异氰酸酯封端的预聚物; 并随后使聚氨酯预聚物与一种或多种式（1）的OH封端的硅烷反应，得到主要具有末端烷氧基甲硅烷基的聚氨酯。 在式（1）中，m等于0,1或2，R 1是具有1至4个碳原子的烷基，R 2是具有1至4个碳原子的烷基，R 3是具有1至 在链中选自C，N，S和/或O的12个原子，但仅仅是碳原子，R4是氢原子或具有1-10个碳原子的烷基，R是双官能有机基团 优选具有1-6个碳原子的直链或支链烷基。 甲硅烷基化聚氨酯适用于作为粘合剂，密封剂或涂层剂的制剂。

    HARDENABLE COMPOSITIONS CONTAINING SOFT-ELASTIC SILYLATED POLYURETHANES
    3.
    发明申请
    HARDENABLE COMPOSITIONS CONTAINING SOFT-ELASTIC SILYLATED POLYURETHANES 审中-公开
    包含软 - 弹性硅烷基聚氨酯的复合组合物

    公开(公告)号：US20100331480A1

    公开(公告)日：2010-12-30

    申请号：US12832356

    申请日：2010-07-08

    申请人： Noelle Wrubbel ,  Helene Boudet ,  Andrea Krlejova ,  Andreas Bolte ,  Lars Zander ,  Johann Klein ,  Christiane Kunze

    发明人： Noelle Wrubbel ,  Helene Boudet ,  Andrea Krlejova ,  Andreas Bolte ,  Lars Zander ,  Johann Klein ,  Christiane Kunze

    IPC分类号： C08L75/04 ,  C08G71/04

    CPC分类号： C08G18/4866 ,  C08G18/10 ,  C08G18/4879 ,  C08G18/718 ,  C08G65/30 ,  C08G65/33351 ,  C08G65/336 ,  C08G65/337 ,  C08G2190/00

    摘要： Silyated polyurethanes can be manufactured by (A) converting (i) at least one polyol compound A with a molecular weight of 500-20,000 Dalton, in particular 4000-10,000 Dalton, (ii) with a dihalogenide to a polyol compound B with a molecular weight of 4000-40,000 Dalton, in particular 8000-20,000 Dalton, and subsequent (B) conversion of this polyol B with one or more isocyanatosilanes of formula (1): OCN—R—Si—(R1)m(-OR2)3-m where m is 0.1 or 2, each R2 is an alkyl radical with 1 to 4 carbon atoms, each R1 is an alkyl radical with 1 to 4 carbon atoms and R is a difunctional organic pump. These silylated polyurethanes are suited to use as adhesives, sealant or coating agent in preparations containing one or more such silylated polyurethane.

    摘要翻译： 可以通过（A）将（i）至少一种分子量为500-20,000道尔顿，特别是4000-10,000道尔顿的多元醇化合物A，（ii）与二卤化物转化成多元醇化合物B的分子式 重量为4000-40,000道尔顿，特别是8000-20,000道尔顿，随后（B）将该多元醇B与一种或多种式（1）的异氰酸基硅烷转化：OCN-R-Si-（R1）m（-OR2）3 -m其中m为0.1或2，每个R 2为具有1至4个碳原子的烷基，每个R 1为具有1至4个碳原子的烷基，R为双官能有机泵。 这些甲硅烷基化聚氨酯适于在含有一种或多种这种甲硅烷基化聚氨酯的制剂中用作粘合剂，密封剂或包衣剂。

    Curable compound comprising silylated polyurethane
    4.
    发明授权
    Curable compound comprising silylated polyurethane 有权
    包含甲硅烷基化聚氨酯的可固化化合物

    公开(公告)号：US08431675B2

    公开(公告)日：2013-04-30

    申请号：US12791974

    申请日：2010-06-02

    申请人： Daniela Braun ,  Johann Klein ,  Christiane Kunze ,  Sara Gonzalez ,  Lars Zander ,  Andreas Bolte ,  Helene Boudet ,  Sarah Schulz

    发明人： Daniela Braun ,  Johann Klein ,  Christiane Kunze ,  Sara Gonzalez ,  Lars Zander ,  Andreas Bolte ,  Helene Boudet ,  Sarah Schulz

    IPC分类号： C08G77/04

    CPC分类号： C09J175/04 ,  C08G18/12 ,  C08G18/282 ,  C08G18/4825 ,  C08G18/765 ,  C08G2190/00 ,  C08G18/718 ,  C08G18/289

    摘要： A method for producing a silylated polyurethane including the steps: (A) converting (i) at least polyol compound having a molecular weight of 4,000-30,000 g/mol and at least one monofunctional compound relative to isocyanates and (ii) at least one diisocyanate at a stoichiometric excess of the sum of the polyol compound(s) and monofunctional compound relative to the diisocyanate compound(s), whereby a hydroxyl-terminated polyurethane prepolymer is formed; and (B) converting the polyurethane prepolymer and one or more isocyanate silane(s) of the formula (I): OCN—R—Si—(R1)m(-OR2)3-m, where m is 0, 1 or 2, each R2 is an alkyl radical having 1 to 4 carbon atoms, each R1 is an alkyl radical having 1 to 4 carbon atoms, and R is a difunctional organic group. Also compounds comprising the silylated polyurethane that can be so produced, and the use thereof as an adhesive and sealant or coating composition.

    摘要翻译： 一种甲硅烷基化聚氨酯的制造方法，包括以下步骤：（A）至少将（i）至少相对于异氰酸酯转化分子量为4,000〜30,000g / mol的多元醇化合物和至少一种单官能化合物，和（ii）至少一种二异氰酸酯 多元醇化合物和单官能化合物相对于二异氰酸酯化合物的总和的化学计量过量，由此形成羟基封端的聚氨酯预聚物; 和（B）将聚氨酯预聚物和一种或多种式（I）的异氰酸酯硅烷转化为：OCN-R-Si-（R1）m（-OR2）3-m，其中m为0,1或2 每个R 2是具有1至4个碳原子的烷基，每个R 1是具有1至4个碳原子的烷基，R 2是双官能的有机基团。 还包括可以如此制备的包含甲硅烷基化聚氨酯的化合物，以及其作为粘合剂和密封剂或涂料组合物的用途。

    CURABLE COMPOUND COMPRISING SILYLATED POLYURETHANE
    5.
    发明申请
    CURABLE COMPOUND COMPRISING SILYLATED POLYURETHANE 有权
    包含SILYLATED聚氨酯的可固化化合物

    公开(公告)号：US20100280209A1

    公开(公告)日：2010-11-04

    申请号：US12791974

    申请日：2010-06-02

    申请人： Daniela Braun ,  Johann Klein ,  Christiane Kunze ,  Sara Gonzalez ,  Lars Zander ,  Andreas Bolte ,  Helene Boudet ,  Sarah Schulz

    发明人： Daniela Braun ,  Johann Klein ,  Christiane Kunze ,  Sara Gonzalez ,  Lars Zander ,  Andreas Bolte ,  Helene Boudet ,  Sarah Schulz

    IPC分类号： C08G71/04

    CPC分类号： C09J175/04 ,  C08G18/12 ,  C08G18/282 ,  C08G18/4825 ,  C08G18/765 ,  C08G2190/00 ,  C08G18/718 ,  C08G18/289

    摘要： A method for producing a silylated polyurethane including the steps: (A) converting (i) at least polyol compound having a molecular weight of 4,000-30,000 g/mol and at least one monofunctional compound relative to isocyanates and (ii) at least one diisocyanate at a stoichiometric excess of the sum of the polyol compound(s) and monofunctional compound relative to the diisocyanate compound(s), whereby a hydroxyl-terminated polyurethane prepolymer is formed; and (B) converting the polyurethane prepolymer and one or more isocyanate silane(s) of the formula (I): OCN—R—Si—(R1)m(-OR2)3-m, where m is 0, 1 or 2, each R2 is an alkyl radical having 1 to 4 carbon atoms, each R1 is an alkyl radical having 1 to 4 carbon atoms, and R is a difunctional organic group. Also compounds comprising the silylated polyurethane that can be so produced, and the use thereof as an adhesive and sealant or coating composition.

    摘要翻译： 一种甲硅烷基化聚氨酯的制造方法，包括以下步骤：（A）至少将（i）至少相对于异氰酸酯转化分子量为4,000〜30,000g / mol的多元醇化合物和至少一种单官能化合物，和（ii）至少一种二异氰酸酯 多元醇化合物和单官能化合物相对于二异氰酸酯化合物的总和的化学计量过量，由此形成羟基封端的聚氨酯预聚物; 和（B）将聚氨酯预聚物和一种或多种式（I）的异氰酸酯硅烷转化为OCN-R-Si-（R1）m（-OR2）3-m，其中m为0,1或2 每个R 2是具有1至4个碳原子的烷基，每个R 1是具有1至4个碳原子的烷基，R 2是双官能的有机基团。 还包括可以如此制备的包含甲硅烷基化聚氨酯的化合物，以及其作为粘合剂和密封剂或涂料组合物的用途。

    HARDENABLE COMPOSITIONS BASED ON SILYLATED POLYURETHANES
    6.
    发明申请
    HARDENABLE COMPOSITIONS BASED ON SILYLATED POLYURETHANES 审中-公开
    基于苯乙烯基聚氨酯的复合组合物

    公开(公告)号：US20110028640A1

    公开(公告)日：2011-02-03

    申请号：US12906215

    申请日：2010-10-18

    申请人： Johann Klein ,  Sara Gonzalez ,  Lars Zander ,  Christiane Kunze ,  Thomas Bachon ,  Andreas Bolte ,  Martin Majolo ,  Thomas Tamcke

    发明人： Johann Klein ,  Sara Gonzalez ,  Lars Zander ,  Christiane Kunze ,  Thomas Bachon ,  Andreas Bolte ,  Martin Majolo ,  Thomas Tamcke

    IPC分类号： C08L83/08 ,  C08G77/08

    CPC分类号： C08G18/4866 ,  C08G18/10 ,  C08G18/227 ,  C08G2190/00 ,  C09J175/08 ,  C08G18/718

    摘要： The invention relates to a method for producing cross-linkable formulations. In a first step of the method, at least one α,ω-difunctional organic polymer of formula (1) X-A-X (1) is converted into organyloxysilyl-terminated polymers P1, using organofunctional silanes of formula (2) Y—R—Si—(R1)m(—OR2)3m (2), in the presence of catalysts (A) selected from the group consisting of potassium, iron, indium, zinc, bismuth and copper compounds. In said formulae, R is a bivalent, optionally substituted hydrocarbon group which comprises between 1 and 12 carbon atoms and can be interrupted with heteroatoms, R1 and R2 are the same or different, monovalent, optionally substituted hydrocarbon groups which comprise between 1 and 12 carbon atoms and can be interrupted with heteroatoms, A is bivalent, optionally substituted hydrocarbon group which comprises at least 6 carbon atoms and can be interrupted with heteroatoms, m is equal to 0, 1 or 2, X is a hydroxyl group and Y is an isocyanate group, or X is an isocyanate group and Y is a hydroxyl group or a primary or secondary amino group. In a second step, the polymers P1 obtained in the first step are mixed with a silane condensation catalyst (B) selected from the group consisting of compounds of elements of the third main group and/or fourth secondary group and heterocyclic organic amines, amine complexes of the element compounds, or the mixtures thereof. Optionally, said mixture is mixed with other substances (C). The formulations do not contain organic tin compounds, and are suitable for using as adhesives, sealants, or coating agents.

    摘要翻译： 本发明涉及一种生产可交联制剂的方法。 在该方法的第一步中，使用式（2）的有机官能硅烷将至少一种式（1）XAX（1）的α，ω-双官能有机聚合物转化为有机甲硅烷基封端的聚合物P1，Y-R-Si- （R1）m（-OR2）3m（2），在选自钾，铁，铟，锌，铋和铜化合物的催化剂（A）的存在下。 在所述式中，R是二价任选取代的烃基，其包含1至12个碳原子并且可被杂原子间隔，R 1和R 2是相同或不同的，包含1至12个碳的单价，任选取代的烃基 原子并且可以被杂原子中断，A是二价的，任选取代的烃基，其包含至少6个碳原子并且可以被杂原子间隔，m等于0,1或2，X是羟基，Y是异氰酸酯 基团，或X为异氰酸酯基团，Y为羟基或伯或仲氨基。 在第二步骤中，将第一步中获得的聚合物P1与选自第三主族和/或第四仲
    子的元素化合物和杂环有机胺的硅烷缩合催化剂（B），胺络合物 的元素化合物，或其混合物。 任选地，将所述混合物与其它物质（C）混合。 配方不含有机锡化合物，适用于粘合剂，密封剂或涂层剂。

    Compositions consisting of partially silyl-terminated polymers
    8.
    发明授权
    Compositions consisting of partially silyl-terminated polymers 有权
    由部分甲硅烷基封端的聚合物组成的组合物

    公开(公告)号：US08067508B2

    公开(公告)日：2011-11-29

    申请号：US12416404

    申请日：2009-04-01

    申请人： Daniela Braun ,  Johann Klein ,  Thomas Bachon ,  Andreas Bolte ,  Christiane Kunze

    发明人： Daniela Braun ,  Johann Klein ,  Thomas Bachon ,  Andreas Bolte ,  Christiane Kunze

    IPC分类号： C08L83/06

    CPC分类号： C08L101/10 ,  C08G18/3893 ,  C08G18/4825 ,  C08G18/71 ,  C08G18/718

    摘要： This disclosure relates to a curable composition comprising at least one polymer A with at least one reactive silyl group and at least one polymer B with at least one reactive silyl group, the number of reactive silyl groups in the polymer A being greater or equal to the number of silyl groups in polymer B and the reactive silyl groups being capable of cross-linking to form siloxane bonds. The disclosure also relates to preparations containing a composition of this type and to the use of said compositions.

    摘要翻译： 本公开涉及包含至少一种具有至少一个反应性甲硅烷基的聚合物A和至少一种具有至少一个反应性甲硅烷基的聚合物B的可固化组合物，聚合物A中的反应性甲硅烷基的数目大于或等于 聚合物B中的甲硅烷基数以及反应性甲硅烷基能够交联以形成硅氧烷键。 本公开还涉及含有这种类型的组合物和所述组合物的用途的制剂。

    Curable composition
    10.
    发明授权
    Curable composition 有权
    可固化组合物

    公开(公告)号：US08748511B2

    公开(公告)日：2014-06-10

    申请号：US13267295

    申请日：2011-10-06

    申请人： Andreas Bolte ,  Helene Boudet ,  Bernhard Schoettmer ,  Nick Spielkamp

    发明人： Andreas Bolte ,  Helene Boudet ,  Bernhard Schoettmer ,  Nick Spielkamp

    IPC分类号： C08K7/22 ,  C08G18/42

    CPC分类号： C09J171/02 ,  C08G65/336

    摘要： Curable compositions comprising a) an alkoxysilane and/or acyloxysilane terminated polymer having at least one end group of the general formula (I) -An-R—SiXYZ (I) and b) hollow microspheres made of a copolymer obtained by the polymerization of methacrylonitrile and at least one monomer M2 selected from the group consisting of acrylic acid, methacrylic acid, acrylic acid alkyl esters and methacrylic acid alkyl esters, wherein the copolymer comprises at maximum 5 wt. % units that are due to the installation of additional monomers and is free of units containing chlorine, to a method for the production thereof and to the use thereof as silane cross-linking adhesive, sealing or coating substances.

    摘要翻译： 可固化组合物，其包含a）具有至少一个具有通式（I）-n-R-SiXYZ（I）的端基的烷氧基硅烷和/或酰氧基硅烷封端的聚合物，和b）由通过甲基丙烯腈的聚合获得的共聚物制成的中空微球 和选自丙烯酸，甲基丙烯酸，丙烯酸烷基酯和甲基丙烯酸烷基酯的至少一种单体M2，其中所述共聚物包含最多5wt。 由于安装另外的单体而且不含有氯的单元，其制备方法以及作为硅烷交联粘合剂，密封或涂覆物质的用途的单位为％。