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1.发明申请公开(公告)号：US20170170514A1
公开(公告)日：2017-06-15
申请号：US15234234
申请日：2016-08-11
发明人： Yong Jun Jang , Ju Young Sung , Yong Sung Lee , Ho Taek Lee , Hyoung Chul Kim , Jong Ho Lee , Hun Gi Jung , Soo Young Cho , Yoon Sung Lee
IPC分类号： H01M10/0562 , H01M10/0525
CPC分类号： H01M10/0562 , C01B17/22 , C01B25/14 , H01B1/10 , H01M10/052 , H01M10/0525 , H01M2220/20 , H01M2300/0068 , Y02E60/122 , Y02T10/7011
摘要： Disclosed is a lithium ion-conductive sulfide-based solid electrolyte which includes nickel sulfide and, accordingly, the solid electrolyte can obtain a novel structure and performance.More particularly, the sulfide-based solid electrolyte includes lithium sulfide (Li2S), diphosphorus pentasulfide (P2S5), and nickel sulfide (Ni3S2) in a specific ratio by mol % and exhibits a novel crystal structure due to nickel (Ni). Accordingly, the sulfide-based solid electrolyte has greater lithium ion conductivity than an conventional sulfide-based solid electrolyte and a stable crystal structure.
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公开(公告)号：US10381682B2
公开(公告)日：2019-08-13
申请号：US15234234
申请日：2016-08-11
发明人： Yong Jun Jang , Ju Young Sung , Yong Sung Lee , Ho Taek Lee , Hyoung Chul Kim , Jong Ho Lee , Hun Gi Jung , Soo Young Cho , Yoon Sung Lee
IPC分类号： H01M10/0562 , H01M10/0525 , C01B25/14 , C01B17/22 , H01B1/10 , H01M10/052
摘要： Disclosed is a lithium ion-conductive sulfide-based solid electrolyte which includes nickel sulfide and, accordingly, the solid electrolyte can obtain a novel structure and performance.More particularly, the sulfide-based solid electrolyte includes lithium sulfide (Li2S), diphosphorus pentasulfide (P2S5), and nickel sulfide (Ni3S2) in a specific ratio by mol % and exhibits a novel crystal structure due to nickel (Ni). Accordingly, the sulfide-based solid electrolyte has greater lithium ion conductivity than an conventional sulfide-based solid electrolyte and a stable crystal structure.
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3.发明申请METHOD FOR MANUFACTURING LITHIUM ION CONDUCTIVE SULFIDE COMPOUND, LITHIUM ION CONDUCTIVE SULFIDE COMPOUND MANUFACTURED BY THE SAME, AND SOLID ELECTROLYTE AND ALL SOLID BATTERY COMPRISING THE SAME 审中-公开制造锂离子导电性硫化合物的方法，由其制造的锂离子导电硫化物化合物和固体电解质以及包含其的所有固体电池公开(公告)号：US20160372785A1
公开(公告)日：2016-12-22
申请号：US14963773
申请日：2015-12-09
发明人： Yong Jun Jang , Ju Young Sung , Yong Sung Lee , Ho Taek Lee , Hyoung Chul Kim , Jong Ho Lee , Hun Gi Jung , Soo Young Cho
IPC分类号： H01M10/0562 , H01M10/0525
CPC分类号： H01M10/0562 , H01M10/0525 , H01M2300/0068
摘要： Disclosed are a method for manufacturing a lithium ion conductive sulfide compound, a lithium ion conductive sulfide compound manufactured by the same, and a solid electrolyte and an all solid battery comprising the same. Particularly, the lithium ion conductive sulfide compound that is manufactured by milling at low temperature so as to increase brittleness of raw materials has differentiated particle distribution, crystal structure and mixing property from the conventional one.
摘要翻译： 公开了一种锂离子导电性硫化物的制造方法，其制造的锂离子导电性硫化物以及固体电解质及包含该锂离子导电性硫化物的全固体电池。 特别地，通过在低温下研磨而增加原料的脆性制造的锂离子传导性硫化物化合物具有与常规颗粒分布，晶体结构和混合性能的差异。
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公开(公告)号：US10074871B2
公开(公告)日：2018-09-11
申请号：US15288494
申请日：2016-10-07
发明人： Hyoung Chul Kim , Hun Gi Jung , Jong Ho Lee , Hae Weon Lee , Byung Kook Kim , Ji Won Son , Wo Dum Jung
IPC分类号： H01M10/0562 , H01M10/0525 , C01B17/22 , H01B1/10
CPC分类号： H01M10/0562 , C01B17/22 , H01B1/10 , H01M10/0525 , H01M2300/0068
摘要： A method for preparing a lithium ion conductive sulfide, which is capable of independently controlling the elemental ratio of lithium (Li), phosphorus (P), sulfur (S), etc, is provided. The method for preparing a lithium ion conductive sulfide can provide a lithium ion conductive sulfide having a crystal structure and an anion cluster distribution distinguished from those of existing ones.
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公开(公告)号：US09970118B2
公开(公告)日：2018-05-15
申请号：US15390462
申请日：2016-12-23
发明人： Jong Sup Hong , Si Won Kim , Man Soo Park , Hyoung Chul Kim , Kyung Joong Yoon , Ji Won Son , Jong Ho Lee , Hae Weon Lee , Byung Kook Kim
IPC分类号： H01M4/04 , C25B11/04 , B05D1/30 , B05D3/10 , B05D3/04 , B41F15/08 , H01M4/88 , H01M4/86 , H01M4/90
CPC分类号： C25B11/0478 , B05D1/30 , B05D3/0453 , B05D3/108 , B41F15/08 , C25B1/00 , C25B1/04 , C25B9/08 , H01M4/04 , H01M4/8605 , H01M4/8842 , H01M4/8846 , H01M4/885 , H01M4/9025 , H01M4/905 , H01M4/9058
摘要： A method for uniformly forming a nickel-metal alloy catalyst in a fuel electrode of a solid oxide electrolysis cell is provided.Specifically, before the nickel-metal alloy catalyst is formed, a metal oxide is uniformly distributed on nickel oxide contained in the fuel electrode through infiltration of a metal oxide precursor solution and hydrolysis of urea.
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公开(公告)号：US11631878B2
公开(公告)日：2023-04-18
申请号：US17212261
申请日：2021-03-25
发明人： Ho Il Ji , Jong Ho Lee , Byung Kook Kim , Ji Won Son , Kyung Joong Yoon , Hyoung Chul Kim , Sang Baek Park , Sung Eun Yang , Jun Seok Kim
IPC分类号： H01M8/1253 , H01M4/90 , H01M4/88 , H01M4/86 , H01M8/12
摘要： Disclosed is a method of manufacturing a solid oxide fuel cell including a multi-layered electrolyte layer using a calendering process. The method for manufacturing a solid oxide fuel cell is a continuous process, thus providing high productivity and maximizing facility investment and processing costs. In addition, the solid oxide fuel cell manufactured by the method includes an anode that is free of interfacial defects and has a uniform packing structure, thereby advantageously greatly improving the production yield and power density. In addition, the solid oxide fuel cell has excellent interfacial bonding strength between respective layers included therein, and includes a multi-layered electrolyte layer in which the secondary phase at the interface is suppressed and which has increased density, thereby advantageously providing excellent output characteristics and long-term stability even at an intermediate operating temperature.
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公开(公告)号：US11329314B2
公开(公告)日：2022-05-10
申请号：US16596659
申请日：2019-10-08
发明人： Hyoung chul Kim , Byung Kook Kim , Hun Gi Jung , Kyung Yoon Chung , Jong Ho Lee , Hae Weon Lee , Ji Won Son , Eu Deum Jung , Ji Su Kim , Sung Jun Choi
IPC分类号： H01M4/02 , H01M10/0562 , H01M10/0525 , C01B25/14
摘要： Disclosed are a sulfide-based solid electrolyte imparted with improved lithium ion conductivity and a method of preparing the same. More particularly, disclosed is a sulfide-based solid electrolyte containing a lithium element (Li), a phosphorus element (P), a sulfur element (S) and a halogen element (X), and including a crystal phase of an argyrodite crystal structure, wherein a molar ratio (X/P) of the halogen element (X) to the phosphorus element (P) is higher than 1.
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公开(公告)号：US10483550B2
公开(公告)日：2019-11-19
申请号：US15630471
申请日：2017-06-22
发明人： Kyung Joong Yoon , Seung-Hwan Lee , Mansoo Park , Jongsup Hong , Hyoungchul Kim , Ji-Won Son , Jong Ho Lee , Byung Kook Kim , Hae-Weon Lee
IPC分类号： H01M4/88 , H01M4/90 , H01M8/12 , H01M8/1253 , H01M8/124
摘要： Provided is a solid oxide cell including a fuel electrode layer, electrolyte layer and an air electrode layer, wherein a diffusion barrier layer is provided between the air electrode layer and the electrolyte layer, the diffusion barrier layer includes: a first diffusion barrier layer formed on the electrolyte layer and including a sintered ceria-based metal oxide containing no sintering aid; and a second diffusion barrier layer formed on the first diffusion barrier layer and including a sintered product of a ceria-based metal oxide mixed with a sintering aid, the first diffusion barrier layer includes a sintered product of nanopowder and macropowder of a ceria-based metal oxide, and the first diffusion barrier layer and the second diffusion barrier layer are sintered at the same time. The diffusion barrier layer is densified, shows high interfacial binding force and prevents formation of a secondary phase derived from chemical reaction with the electrolyte.
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公开(公告)号：US10020536B2
公开(公告)日：2018-07-10
申请号：US15404708
申请日：2017-01-12
发明人： Hyoung Chul Kim , Sung Jun Choi , Jeong Hun Kim , Wo Dum Jung , Hun Gi Jung , Ji Won Son , Jong Ho Lee , Byung Kook Kim , Hae Weon Lee
IPC分类号： H01M10/052 , H01M10/0562
CPC分类号： H01M10/0562 , C01B17/20 , C01B17/22 , H01M2300/0068
摘要： A method for preparing a sulfide-based solid electrolyte which is stable upon exposure to the air is provided. Specifically, a stabilization layer is formed on the surface of a sulfide-based solid electrolyte particle through treatment with a reactive gas.The sulfide-based solid electrolyte with superior air stability can be obtained because oxidation or reduction reactions with water, etc. in the air occur on the stabilization layer rather than on the sulfide-based solid electrolyte particle.
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10.发明授权公开(公告)号：US09966624B2
公开(公告)日：2018-05-08
申请号：US15346105
申请日：2016-11-08
发明人： Kyung Joong Yoon , Seung-Hwan Lee , Mansoo Park , Jongsup Hong , Hyoungchul Kim , Ji-Won Son , Jong Ho Lee , Byung Kook Kim , Hae-Weon Lee
IPC分类号： H01M8/12 , H01M8/1253 , H01M8/126 , H01M8/124
CPC分类号： H01M8/1253 , C01F17/0018 , C01G51/006 , C01P2002/72 , C01P2004/03 , C01P2004/04 , C04B35/50 , C04B35/6281 , C04B35/62815 , C04B35/62823 , C04B35/62886 , C04B35/62892 , C04B2235/3203 , C04B2235/3208 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3229 , C04B2235/3262 , C04B2235/3272 , C04B2235/3275 , C04B2235/3281 , C04B2235/3284 , C04B2235/443 , C04B2235/5436 , C04B2235/5445 , C04B2235/5454 , C04B2235/785 , C04B2235/786 , C04B2235/9615 , H01M8/126 , H01M2008/1293 , H01M2300/0074 , H01M2300/0077
摘要： Provided is a method for manufacturing a sintered body for an electrolyte and an electrolyte for a fuel cell using the same. More particularly, the following disclosure relates to a method for preparing an electrolyte having a firm thin film layer by using a sintered body having controlled sintering characteristics, and application of the electrolyte to a solid oxide fuel cell. It is possible to control the sintering characteristics of a sintered body through a simple method, such as controlling the amounts of crude particles and nanoparticles. In addition, an electrode using the obtained sintered body having controlled sintering characteristics is effective for forming a firm thin film layer. Further, such an electrolyte having a firm thin film layer formed thereon inhibits combustion of fuel with oxygen when it is applied to a fuel cell, and thus shows significantly effective for improving the quality of a cell.
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