摘要:
A process for producing silanes represented by the general formula SI.sub.n H.sub.2n+2 wherein n is 1 or 2, which comprises (a) preparing a silicon-magnesium alloy containing at least one element selected from the goup consisting of Li, Na, K, Ca, Ba, Ti, Zr, Nb, Cr, Mo, Mn, Fe, Co, Ni, Pd, Cu, Ag, Zn, Cd, Al, Sn, Pb, Bi, Se, S and C as a third component element; (b) reacting the alloy containing the third component element with an acid in an ammonia solvent; and (c) thus, varying the ratio of Si.sub.2 H.sub.6 formed to SiH.sub.4 formed.
摘要翻译:一种制备由通式SInH 2 n + 2表示的硅烷的方法,其中n为1或2,其包括(a)制备含有至少一种选自由Li,Na,K,Ca, Ba,Ti,Zr,Nb,Cr,Mo,Mn,Fe,Co,Ni,Pd,Cu,Ag,Zn,Cd,Al,Sn,Pb,Bi,Se,S和C作为第三成分元素; (b)使含有第三组分元素的合金与氨在氨溶剂中的酸反应; 和(c)因此改变形成的Si 2 H 6与形成的SiH 4的比例。
摘要:
A process for disproportionating silanes, which comprises contacting a silane having at least one Si--H bond represented by the general formulaR.sub.l H.sub.m SiX.sub.4-(l+m)wherein R represents an alkyl or aryl group, X represents a halogen atom or an alkoxy group, l is 0, 1 or 2, and m is 1, 2 or 3 and l+m is 1, 2 or 3, and when l is 2, R's may be identical or different, and when l+m is 1 or 2, X's may be identical or different, with a reaction product of a strong acid-type cation exchange resin with an amine and disproportionating the silane.
摘要翻译:一种用于歧化硅烷的方法,其包括使具有由通式R 1 H m SiX 4 - (1 + m)表示的至少一个Si-H键的硅烷接触,其中R表示烷基或芳基,X表示卤素原子或烷氧基, l为0,1或2,m为1,2或3,l + m为1,2或3,当l为2时,R可以相同或不同,当l + m为1或2时, X可以相同或不同,强酸型阳离子交换树脂与胺的反应产物和歧化硅烷。
摘要:
A process for producing silicon hydrides represented by the general formula Si.sub.n H.sub.2n+2 wherein n is a positive integer of 1 to 6, which comprises reacting a silicon-containing alloy with an aqueous solution of an acid in the presence of at least one inert organic solvent having a boiling range of from -60.degree. C. to 250.degree. C.
摘要:
A process for preparing an organic silicon compound is here disclosed which comprises the step of reacting a halogenated hydrocarbon selected from the group consisting ##STR1## wherein each of X.sup.1 to X.sup.16 is selected from the group consisting of hydrogen, an alkyl group, alkenyl group, phenyl group, naphthyl group, alkoxy group, acyl group, alkylamino group and dialkylamino group having 1 to 20 carbon atoms which are unsubstituted or substituted and a halogen atom; and each of at least one of X.sup.1 to X.sup.4, at least one of X.sup.8 to X.sup.10 and at least one of X.sup.11 to X.sup.16 is a halogen atom,with a silane selected from the group consisting of SiH.sub.4, Si.sub.2 H.sub.6 and Si.sub.3 H.sub.8.
摘要:
A numerical control apparatus provides for manual shift operation involving feed shafts of a machine tool in terms of a work coordinate system easily and readily understood by an operator. The numerical control apparatus includes a manual shift amount input unit for receiving an amount of manual shift involving linear feed shafts as operator-input data in terms of a work coordinate system defined on the work revolved or rotated by a rotary feed shaft. The numerical control apparatus further includes a manual shift amount cumulative storage for cumulatively storing the received amount of manual shift in terms of a work coordinate system. Also included is a cumulative shift amount coordinate converter for converting the cumulative amount of shift from the work coordinate system data to data in terms of machine coordinate system defined on the machine tool. The apparatus's manual shift amount superimposing unit then superimposes the converted cumulative amount of shift on a controlled variable commanded in a machining program to generate the result to servo drivers.
摘要:
The polyolefin composite film is excellent in low-temperature heat sealability, heat-sealing strength and transparency, and at least has surface layer [i]//intermediate layer [iii]//core layer [ii], wherein the surface layer [i] includes a propylene resin composition including 0-50 wt % of a specific propylene/α-olefin random copolymer (A) and/or a specific 1-butene/α-olefin copolymer (E), and 50-100 wt % of a propylene polymer (B) having a melting point of 120-170° C. ((A), (E) and (B) in the surface layer totals 100 wt %); the core layer [ii] includes a propylene resin composition including 70-100 wt % of a crystalline polypropylene (C) having a melting point of 150-170° C., and 0-30 wt % of the copolymer (A) ((C) and (A) in the core layer totals 100 wt %); and the intermediate layer [iii] includes a propylene resin composition including 50-95 wt% of the crystalline polypropylene (C) and 50-5% of the polymer (B), the copolymer (A), and/or the copolymer (E) ((C), (B), (A) and (E) in the intermediate layer totals 100 wt %).
摘要:
To provide an organic electroluminescent element having a low driving voltage, high current efficiency and high voltage efficiency.An organic electroluminescent element comprising an anode, a cathode and an organic layer disposed between the anode and the cathode, wherein the organic layer comprises a mixed layer containing a light-emitting low molecular compound and/or a charge-transporting low molecular compound in a film containing an insolubilized polymer obtained by insolubilizing an insolubilizing polymer, and, adjacent to the mixed layer, a layer containing a light-emitting low molecular compound and a charge-transporting low molecular compound and not containing an insolubilized polymer.
摘要:
The polyolefin composite film is excellent in low-temperature heat sealability, heat-sealing strength and transparency, and at least has surface layer [i]//intermediate layer [iii]//core layer[i], wherein the surface layer[i]includes a propylene resin composition including 0-50 wt % of a specific propyleneα-olefin random copolymer (A) and/or a specific 1-buteneα-olefin copolymer (E), and 50-100 wt % of a propylene polymer (B) having a melting point of 120-170° C. ((A), (E) and (B) in the surface layer totals 100 wt %); the core layer [ii]includes a propylene resin composition including 70-100 wt % of a crystalline polypropylene (C) having a melting point of 150-170° C., and 0-30 wt % of the copolymer (A) ((C) and (A) in the core layer totals 100 wt %); and the intermediate layer[iii]includes a propylene resin composition including 50-95 wt % of the crystalline polypropylene (C) and 50-5 % of the polymer (B), the copolymer (A), andor the copolymer (E) ((C), (B), (A) and (E) in the intermediate layer totals 100 wt %).
摘要:
To provide an organic electroluminescent element having a low driving voltage, high current efficiency and high voltage efficiency.An organic electroluminescent element comprising an anode, a cathode and an organic layer disposed between the anode and the cathode, wherein the organic layer comprises a mixed layer containing a light-emitting low molecular compound and/or a charge-transporting low molecular compound in a film containing an insolubilized polymer obtained by insolubilizing an insolubilizing polymer, and, adjacent to the mixed layer, a layer containing a light-emitting low molecular compound and a charge-transporting low molecular compound and not containing an insolubilized polymer.
摘要:
In a position measuring method, GPS ranging data obtained at a reference station 1 and an observation station 2 is inputted to four solution calculating sections 12, RTK solutions such as a fix solution at the observation station 2 are calculated in the solution calculating sections 12 according to the RTK system, and the RTK solutions are inputted to a solution obtaining unit 13. Further, it is decided whether or not the RTK solutions include multiple fix solutions. When it is decided that the RTK solutions include multiple fix solutions, deviations between the fix solutions are determined and it is decided whether or not the deviations exceed an allowable value. When it is decided that none of the deviations exceed the allowable value, predetermined arithmetic processing is performed on the fix solutions to obtain a normal fix solution. Moreover, the solution calculating sections are sequentially restarted at predetermined time intervals.