摘要:
A reaction with distillation column is provided with a plurality of discrete catalytic reaction containers. The containers contain a plurality of solid catalyst particles which form a catalytic reaction zone. The containers also comprise a liquid collection tray cover which defines a liquid accumulation zone immediately overlying the catalytic reaction zone. Overflow weirs are provided on the tray cover to allow for overflow of liquid on the tray cover. A member may be provided within the containers to create an open area within the catalytic reaction zone to facilitate entry of the liquid into the catalytic reaction zone. The containers can be individually positioned within the reactor to suit particular process requirements.
摘要:
A reaction with distillation column is provided with a plurality of discrete catalytic reaction containers. The containers contain a plurality of solid catalyst particles which form a catalytic reaction zone. The containers also include a liquid collection tray cover which defines a liquid accumulation zone immediately overlying the catalytic reaction zone. Overflow weirs are provided on the tray cover to allow for overflow of liquid on the tray cover. A member may be provided within the containers to create an open area within the catalytic reaction zone to facilitate entry of the liquid into the catalytic reaction zone. The containers can be individually positioned within the reactor to suit particular process requirements.
摘要:
A column having a region for reaction with distillation of fluid streams is provided with structures which include distillation trays that allow for the accumulation of liquid from a liquid stream and the passage of a vapor stream through the liquid for interaction therewith. The structures include catalyst beds which extend downwardly from the trays and are housed within at least partially perforate containers. A portion of the liquid on the tray is catalytically reacted as it is driven through the catalyst bed by the liquid head created by the accumulated liquid. Another portion of the liquid may be directed through a bypass which also extends downwardly from the tray and allows the liquid to bypass the catalyst bed so that higher volumetric flow rates can be achieved. A still further portion of the liquid can be directed to a zone between adjacent catalyst beds or within a catalyst bed for developing a liquid head to force the liquid laterally through the catalyst bed.
摘要:
A reaction with distillation structure utilizes a plurality of distillation trays and catalyst containers which provide a catalytic reaction zone and a primary flow path for descending liquid streams. Catalytic reaction of the liquid streams within the catalyst reaction zone formed in the containers occurs concurrently with fractionation of the reaction products on the distillation trays. The containers may extend continuously through the reaction zone of the distillation reactor to allow for dump loading and removal of the solid particulate catalyst. Alternatively, the catalyst containers may extend from one tray toward a lower tray without passing through the latter. Structure may also be provided within the containers to influence system hydraulics through the accumulation of liquid within the catalyst bed. This is done by providing an open area interiorly of the catalyst bed into which liquid on the distillation tray is driven. This open area communicates with a liquid accumulation zone wherein liquid accumulates until a sufficient liquid head drives the liquid generally horizontally outward, through the catalyst bed.
摘要:
A reaction with distillation structure utilizes a plurality of distillation trays and catalyst containers which provide a catalytic reaction zone and a primary flow path for descending liquid streams. Catalytic reaction of the liquid streams within the catalyst reaction zone formed in the containers occurs concurrently with fractionation of the reaction products on the distillation trays. The containers may extend continuously through the reaction zone of the distillation reactor to allow for dump loading and removal of the solid particulate catalyst. Alternatively, the catalyst containers may extend from one tray toward a lower tray without passing through the latter. Structure may also be provided within the containers to influence system hydraulics through the accumulation of liquid within the catalyst bed. This is done by providing an open area interiorly of the catalyst bed into which liquid on the distillation tray is driven. This open area communicates with a liquid accumulation zone wherein liquid accumulates until a sufficient liquid head drives the liquid generally horizontally outward, through the catalyst bed.
摘要:
A downcomer having a screened or otherwise liquid permeable wall is provided for use in a mass transfer or distillation column. The liquid permeable wall provides another avenue for liquid to be removed from the downcomer to increase the liquid handling capacity of the downcomer. When wetted, the liquid permeable wall provides a barrier against vapor entry into the downcomer through the wall.
摘要:
A mass transfer or heat exchange column is provided with a vapor distributor which circulates a vapor stream about the inner periphery of the column. The vapor stream is discharged from the distributor through an at least partially open bottom and, optionally, a plurality of spaced apart outlet ports in an inner annular wall of the distributor. A deflector extends upwardly along the inner annular wall to deflect the vapor stream away from a circumferential flow path along the inward face of the wall. The deflector may also extend outwardly under the flow channel to deflect, in a radially inward direction, vapor exiting the flow channel through the open bottom of the distributor.
摘要:
A mass transfer or heat exchange column is provided with a vapor distributor having, in one embodiment, a deflecting surface which directs a vapor stream about the inner periphery of the column. Following discharge from the distributor, the vapor stream contacts circumferentially spaced guide vanes which redirect the vapor stream toward the center of the column to cause a more uniform distribution of the vapor stream across the horizontal cross section of the column.
摘要:
A vapor-liquid contact tray is provided which includes a plurality of openings and associated fixed roof structures which redirect vapor flowing vertically upward through the openings to horizontal flow paths. Each fixed roof structure includes a generally planar deflector which overlies and is spaced above the associated opening in the tray. The deflector is joined to the tray by end plates connected at one end to the tray and at the other end to the deflector. In one embodiment the deflector is generally parallel to the tray and divides the vertically flowing vapor stream into roughly equal oppositely flowing vapor streams. In other embodiments, the deflector is inclined in relation to the tray to preferentially direct the vapor stream in one direction or to split the vapor stream into equal portions which are directed in the same general direction. The openings and deflectors are arranged to more uniformly push the vapor and hence the liquid into and through those areas of the tray where liquid stagnation and gradients are a problem. The fixed roof structures in the row of apertures closest to liquid receiving area at the inlet end of the tray are oriented so that the end plates shield the openings against entry of liquid leaving the receiving area. Louvre-type fixed roof structures are used in association with at least some of the openings in the first row so that more rapid frothing of the liquid can be achieved with reduced incidence of liquid weeping through openings in successive rows of openings.
摘要:
A method for operating a column having a region for reaction with distillation of fluid streams is provided with structures including catalyst-filled containers having liquid permeable upper surfaces which allow for the accumulation and flow of liquid from a liquid stream. The containers include catalyst beds positioned beneath the upper surface of the containers. A portion of the liquid on the containers is driven through the catalyst bed by the liquid head created by the accumulated liquid and is catalytically reacted. Another portion of the liquid may be directed through a downcomer which allows the accumulated liquid to leave the container without passing through the catalyst bed so that higher volumetric flow rates can be achieved.