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1.发明申请公开(公告)号：US20130084453A1
公开(公告)日：2013-04-04
申请号：US13581146
申请日：2011-02-25
IPC分类号： C09D175/04 , C08K3/00 , C09D165/02 , C08K13/02
CPC分类号： C09D175/04 , C08G2150/90 , C08K3/11 , C08K13/02 , C09D5/084 , C09D7/63 , C09D161/12 , C09D165/02 , C23C22/40 , C23C22/42 , C23C22/44 , C23C2222/20 , Y10T428/273 , C08K5/56 , C08L75/04
摘要： The present invention provides a chromium-free surface treatment agent, comprising: a resin compound having a specific bisphenol skeleton; cationic urethane resin emulsion; silane coupling agent; an organic titanium chelate compound; a quadrivalent vanadyl compound; a molybdic acid compound; and water, wherein these components are blended at predetermined ratios such that pH value of the surface treatment agent is in the range of 4 to 5. The one-pack type chromium-free surface treatment agent of the present invention exhibits good stability during storage and is capable of forming on a metal material surface a coating film excellent in corrosion resistance at a bending-processed portion of a steel sheet, solvent resistance and paintability after alkali degreasing.
摘要翻译： 本发明提供一种无铬表面处理剂，其包含：具有特定双酚骨架的树脂化合物; 阳离子聚氨酯树脂乳液; 硅烷偶联剂; 有机钛螯合物; 四价氧钒化合物; 钼酸化合物; 和水，其中这些组分以预定比例共混，使得表面处理剂的pH值在4至5的范围内。本发明的单组分型无铬表面处理剂在储存期间表现出良好的稳定性， 能够在金属材料表面上形成在钢板的弯曲加工部分的耐腐蚀性优异的涂膜，耐碱性脱脂后的耐溶剂性和可涂布性。
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2.发明授权Surface treatment agent for zinc or zinc alloy coated steel sheet, zinc or zinc alloy coated steel sheet, and method of producing the steel sheet 有权锌或锌合金涂层钢板，锌或锌合金涂层钢板的表面处理剂及钢板的制造方法公开(公告)号：US09512331B2
公开(公告)日：2016-12-06
申请号：US13581146
申请日：2011-02-25
IPC分类号： C09D175/04 , C23C22/40 , C09D5/08 , C09D7/12 , C08K3/00 , C08K13/02 , C09D165/02 , C09D161/12
CPC分类号： C09D175/04 , C08G2150/90 , C08K3/11 , C08K13/02 , C09D5/084 , C09D7/63 , C09D161/12 , C09D165/02 , C23C22/40 , C23C22/42 , C23C22/44 , C23C2222/20 , Y10T428/273 , C08K5/56 , C08L75/04
摘要： The present invention provides a chromium-free surface treatment agent, comprising: a resin compound having a specific bisphenol skeleton; cationic urethane resin emulsion; silane coupling agent; an organic titanium chelate compound; a quadrivalent vanadyl compound; a molybdic acid compound; and water, wherein these components are blended at predetermined ratios such that pH value of the surface treatment agent is in the range of 4 to 5. The one-pack type chromium-free surface treatment agent of the present invention exhibits good stability during storage and is capable of forming on a metal material surface a coating film excellent in corrosion resistance at a bending-processed portion of a steel sheet, solvent resistance and paintability after alkali degreasing.
摘要翻译： 本发明提供一种无铬表面处理剂，其包含：具有特定双酚骨架的树脂化合物; 阳离子聚氨酯树脂乳液; 硅烷偶联剂; 有机钛螯合物; 四价氧钒化合物; 钼酸化合物; 和水，其中这些组分以预定比例共混，使得表面处理剂的pH值在4至5的范围内。本发明的单组分型无铬表面处理剂在储存期间表现出良好的稳定性， 能够在金属材料表面上形成在钢板的弯曲加工部分的耐腐蚀性优异的涂膜，耐碱性脱脂后的耐溶剂性和可涂布性。
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3.发明授权公开(公告)号：US09200165B2
公开(公告)日：2015-12-01
申请号：US13820869
申请日：2011-09-20
申请人： Toru Imokawa , Takahiro Kubota , Etsuo Hamada , Masayasu Nagoshi
发明人： Toru Imokawa , Takahiro Kubota , Etsuo Hamada , Masayasu Nagoshi
CPC分类号： C09D5/08 , C08G18/0814 , C08K3/11 , C08K5/54 , C09D5/084 , C09D5/086 , C09D175/04 , C23C22/44 , Y10T428/12569 , C08L61/12
摘要： The present invention provides a chromium-free surface treatment liquid which enables forming, on a metal material surface, a film excellent in corrosion resistance at bent portions of a steel sheet, solvent resistance, coating properties after alkaline degreasing, and sweat resistance. The surface treatment liquid contains a resin compound having a specific bisphenol skeleton, a cationic urethane resin emulsion, a silane coupling agent, an organic titanium chelate compound, a quadrivalent vanadyl compound, a molybdate compound, a fluorine compound, and water at predetermined proportions. The pH of the surface treatment liquid is in the range of 4 to 5.
摘要翻译： 本发明提供一种无铬表面处理液，其能够在金属材料表面形成钢板弯曲部的耐腐蚀性优异的膜，耐溶剂性，碱性脱脂后的涂布性，耐汗性。 表面处理液含有规定比例的具有特定双酚骨架的树脂化合物，阳离子性聚氨酯树脂乳液，硅烷偶联剂，有机钛螯合物，四价钒酰化合物，钼酸盐化合物，氟化合物和水。 表面处理液的pH在4〜5的范围内。
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4.发明申请公开(公告)号：US20130171468A1
公开(公告)日：2013-07-04
申请号：US13820869
申请日：2011-09-20
申请人： Toru Imokawa , Takahiro Kubota , Etsuo Hamada , Masayasu Nagoshi
发明人： Toru Imokawa , Takahiro Kubota , Etsuo Hamada , Masayasu Nagoshi
IPC分类号： C09D5/08
CPC分类号： C09D5/08 , C08G18/0814 , C08K3/11 , C08K5/54 , C09D5/084 , C09D5/086 , C09D175/04 , C23C22/44 , Y10T428/12569 , C08L61/12
摘要： The present invention provides a chromium-free surface treatment liquid which enables forming, on a metal material surface, a film excellent in corrosion resistance at bent portions of a steel sheet, solvent resistance, coating properties after alkaline degreasing, and sweat resistance. The surface treatment liquid contains a resin compound having a specific bisphenol skeleton, a cationic urethane resin emulsion, a silane coupling agent, an organic titanium chelate compound, a quadrivalent vanadyl compound, a molybdate compound, a fluorine compound, and water at predetermined proportions. The pH of the surface treatment liquid is in the range of 4 to 5.
摘要翻译： 本发明提供一种无铬表面处理液，其能够在金属材料表面形成钢板弯曲部的耐腐蚀性优异的膜，耐溶剂性，碱性脱脂后的涂布性，耐汗性。 表面处理液含有规定比例的具有特定双酚骨架的树脂化合物，阳离子性聚氨酯树脂乳液，硅烷偶联剂，有机钛螯合物，四价钒酰化合物，钼酸盐化合物，氟化合物和水。 表面处理液的pH在4〜5的范围内。
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公开(公告)号：US20140186614A1
公开(公告)日：2014-07-03
申请号：US14235863
申请日：2012-08-29
申请人： Nobue Fujibayashi , Kazumichi Sashi , Yusuke Okumura , Yasuhide Oshima , Takahiro Kubota , Masayasu Nagoshi
发明人： Nobue Fujibayashi , Kazumichi Sashi , Yusuke Okumura , Yasuhide Oshima , Takahiro Kubota , Masayasu Nagoshi
CPC分类号： H01F41/00 , C09D1/00 , C09D5/08 , C09D5/4476 , C23C18/122 , C23C18/1241 , C23C18/127 , C23C22/74 , C23C2222/20 , H01F1/18 , Y10T428/259 , Y10T428/31663
摘要： An electrical steel sheet with an insulation coating excellent in punchability, coating adhesion property and coating film property after annealing, even without containing any chromium compound in the insulation coating. The insulation coating is formed by applying a surface-treatment agent to at least one side of the electrical steel sheet and drying the surface-treatment agent. The surface-treatment agent contains trialkoxysilane and/or dialkoxysilane (A) in which a substituent bound to Si is constituted only by at least one non-reactive substituent selected from the group consisting of hydrogen, an alkyl group, and a phenyl group; and a silane coupling agent (B), at a mass ratio (A/B) of 0.05 to 1.0.
摘要翻译： 具有优异的冲压性，涂布粘合性和退火后的涂膜性能的绝缘涂层的电工钢板，即使在绝缘涂层中也不含任何铬化合物。 通过将表面处理剂施加到电工钢板的至少一面并干燥表面处理剂来形成绝缘涂层。 表面处理剂含有三烷氧基硅烷和/或二烷氧基硅烷（A），其中与Si结合的取代基仅由至少一个选自氢，烷基和苯基的非反应性取代基构成; 和硅烷偶联剂（B），质量比（A / B）为0.05〜1.0。
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公开(公告)号：US07527876B2
公开(公告)日：2009-05-05
申请号：US11899570
申请日：2007-09-06
申请人： Nobue Fujibayashi , Akira Matsuzaki , Satoru Ando , Syuji Nomura , Takahiro Kubota , Yoshikazu Morohoshi , Takashi Nakano , Takashi Okubo , Jun Akui
发明人： Nobue Fujibayashi , Akira Matsuzaki , Satoru Ando , Syuji Nomura , Takahiro Kubota , Yoshikazu Morohoshi , Takashi Nakano , Takashi Okubo , Jun Akui
CPC分类号： B32B15/013 , C23C2/26 , C23C28/00 , Y10T428/12493 , Y10T428/12535 , Y10T428/12611 , Y10T428/12618 , Y10T428/12757 , Y10T428/12799 , Y10T428/12806 , Y10T428/12951 , Y10T428/12972 , Y10T428/27
摘要： A surface-treated steel sheet is disclosed, including a zinc based plated steel sheet having thereon a surface-treated film containing titanium, nickel, aluminum and fluorine and having a film thickness of from 0.05 to 1.0 μm, the surface-treated film having a titanium deposition amount of from 0.01 to 0.5 g/m2 and containing from 0.01 to 5 parts by mass of nickel, from 0.1 to 25 parts by mass of aluminum and from 1 to 500 parts by mass of fluorine relative to 100 parts by mass of titanium. This surface-treated steel sheet does not contain hexavalent chromium in the film thereof at all and has excellent heat discoloration resistance, corrosion resistance and resistance to blackening.
摘要翻译： 公开了一种经表面处理的钢板，其包括其上具有含有钛，镍，铝和氟的表面处理膜并且膜厚度为0.05至1.0μm的锌基电镀钢板，表面处理膜具有 钛沉积量为0.01〜0.5g / m 2，含有0.01〜5质量份的镍，0.1〜25质量份的铝和1〜500质量份的氟，相对于100质量份的钛 。 该表面处理钢板根本不含有六价铬，耐热变色性，耐腐蚀性和耐黑变性优异。
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公开(公告)号：US20130273389A1
公开(公告)日：2013-10-17
申请号：US13825210
申请日：2011-09-28
申请人： Rie Kaneko , Nobue Fujibayashi , Takahiro Kubota
发明人： Rie Kaneko , Nobue Fujibayashi , Takahiro Kubota
CPC分类号： B05D7/14 , B32B15/08 , C08G18/0814 , C08K3/014 , C09D5/084 , C09D5/24 , C09D175/04 , C23C2/26 , C23C22/40 , C23C22/44 , C23C2222/20 , Y10T428/12569
摘要： A method of producing a hot-dip galvanized steel sheet includes applying, to a hot-dip galvanized steel sheet having a Ra of 0.5 to 2.0 μm and a PPI of 150 or more, a predetermined surface treatment agent, i.e., a surface treatment agent containing a specified resin compound, a specified urethane resin having cationy, a specified silane coupling agent having a functional group, a specified organic Ti chelate compound, and a tetravalent vanadyl compound at a specified ratio; and drying the surface treatment agent at a ultimate sheet temperature of 50° C. to 180° C. to form a surface treatment coating film with a coating weight of 0.2 to 1.0 g/m2 on the surface of the steel sheet.
摘要翻译： 一种热浸镀锌钢板的制造方法，其特征在于，在Ra为0.5〜2.0μm，PPI为150以上的热镀锌钢板上涂布预定的表面处理剂，即表面处理剂 含有特定的树脂化合物，具有阳离子性的规定的聚氨酯树脂，具有官能团的规定的硅烷偶联剂，规定的有机钛螯合物和四价氧钒基化合物， 并将表面处理剂在50℃至180℃的最终板温度下干燥，以在钢板表面上形成涂布重量为0.2至1.0g / m 2的表面处理涂膜。
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公开(公告)号：US20080063896A1
公开(公告)日：2008-03-13
申请号：US11899570
申请日：2007-09-06
申请人： Nobue Fujibayashi , Akira Matsuzaki , Satoru Ando , Syuji Nomura , Takahiro Kubota , Yoshikazu Morohoshi , Takashi Nakano , Takashi Okubo , Jun Akui
发明人： Nobue Fujibayashi , Akira Matsuzaki , Satoru Ando , Syuji Nomura , Takahiro Kubota , Yoshikazu Morohoshi , Takashi Nakano , Takashi Okubo , Jun Akui
IPC分类号： B32B15/01
CPC分类号： B32B15/013 , C23C2/26 , C23C28/00 , Y10T428/12493 , Y10T428/12535 , Y10T428/12611 , Y10T428/12618 , Y10T428/12757 , Y10T428/12799 , Y10T428/12806 , Y10T428/12951 , Y10T428/12972 , Y10T428/27
摘要： A surface-treated steel sheet is disclosed, including a zinc based plated steel sheet having thereon a surface-treated film containing titanium, nickel, aluminum and fluorine and having a film thickness of from 0.05 to 1.0 μm, the surface-treated film having a titanium deposition amount of from 0.01 to 0.5 g/m2 and containing from 0.01 to 5 parts by mass of nickel, from 0.1 to 25 parts by mass of aluminum and from 1 to 500 parts by mass of fluorine relative to 100 parts by mass of titanium. This surface-treated steel sheet does not contain hexavalent chromium in the film thereof at all and has excellent heat discoloration resistance, corrosion resistance and resistance to blackening.
摘要翻译： 公开了一种经表面处理的钢板，其包括其上具有含有钛，镍，铝和氟的表面处理膜并且膜厚度为0.05至1.0μm的锌基电镀钢板，表面处理膜具有 钛沉积量为0.01〜0.5g / m 2，含有0.01〜5质量份的镍，0.1〜25质量份的铝和1〜500质量份的氟 相对于100质量份的钛。 该表面处理钢板根本不含有六价铬，耐热变色性，耐腐蚀性和耐黑变性优异。
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公开(公告)号：US09358581B2
公开(公告)日：2016-06-07
申请号：US13825210
申请日：2011-09-28
申请人： Rie Kaneko , Nobue Fujibayashi , Takahiro Kubota
发明人： Rie Kaneko , Nobue Fujibayashi , Takahiro Kubota
IPC分类号： C23C2/26 , B05D7/14 , C09D5/08 , C09D5/24 , C08G18/08 , C09D175/04 , B32B15/08 , C23C22/40 , C23C22/44 , C08K3/00
CPC分类号： B05D7/14 , B32B15/08 , C08G18/0814 , C08K3/014 , C09D5/084 , C09D5/24 , C09D175/04 , C23C2/26 , C23C22/40 , C23C22/44 , C23C2222/20 , Y10T428/12569
摘要： A method of producing a hot-dip galvanized steel sheet includes applying, to a hot-dip galvanized steel sheet having a Ra of 0.5 to 2.0 μm and a PPI of 150 or more, a predetermined surface treatment agent, i.e., a surface treatment agent containing a specified resin compound, a specified urethane resin having cationy, a specified silane coupling agent having a functional group, a specified organic Ti chelate compound, and a tetravalent vanadyl compound at a specified ratio; and drying the surface treatment agent at a ultimate sheet temperature of 50° C. to 180° C. to form a surface treatment coating film with a coating weight of 0.2 to 1.0 g/m2 on the surface of the steel sheet.
摘要翻译： 一种热浸镀锌钢板的制造方法，其特征在于，在Ra为0.5〜2.0μm，PPI为150以上的热浸镀锌钢板上涂布预定的表面处理剂，即表面处理剂 含有特定的树脂化合物，具有阳离子性的规定的聚氨酯树脂，具有官能团的规定的硅烷偶联剂，规定的有机钛螯合物和四价氧钒基化合物， 并将表面处理剂在50℃至180℃的最终板温度下干燥，以在钢板表面上形成涂布重量为0.2至1.0g / m 2的表面处理涂膜。
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公开(公告)号：US09260774B2
公开(公告)日：2016-02-16
申请号：US13638188
申请日：2011-03-14
申请人： Katsuya Hoshino , Takahiro Kubota , Masahiko Tada , Masayasu Nagoshi , Wataru Tanimoto , Hideo Kijima , Kazuhiko Higai
发明人： Katsuya Hoshino , Takahiro Kubota , Masahiko Tada , Masayasu Nagoshi , Wataru Tanimoto , Hideo Kijima , Kazuhiko Higai
CPC分类号： C23C2/26 , B21B1/22 , B21B2001/228 , C23C2/06 , C23C22/53 , C23C22/83 , C23C28/025 , C23C28/345
摘要： An object of the present invention is to make it possible, without necessitating an alkali pretreatment, to form a zinc oxide layer having excellent sliding properties on a hot dip galvanized steel sheet not subjected to alloying after galvanizing and thus having a relatively low degree of surface activity. Another object of the present invention is to make it possible to manufacture a hot dip galvanized steel sheet having higher area ratio of Zn oxide layer formed on a coating surface and larger thickness of the Zn oxide layer. Specifically, the present invention provides a method for manufacturing a hot dip galvanized steel sheet comprising: subjecting a steel sheet to hot dip galvanizing and subsequent temper rolling; bringing the steel sheet into contact with acidic solution having pH buffering capacity; retaining the steel sheet for 1 second to 60 seconds after the contact with the acidic solution; and rinsing the steel sheet with water, to form a zinc oxide layer on a coating surface of the steel sheet, characterized in that the method further comprising:carrying out the temper rolling by either rolling the steel sheet first with a dull roll having Ra≧2.0 μm at rolling reduction rate ≦5% and then with a bright roll having Ra≦0.1 μm at rolling reduction rate ≦3% or rolling the steel sheet first with a bright roll having Ra≦0.1 μm at rolling reduction rate ≦3% and then with a dull roll having Ra≦2.0 μm at rolling reduction rate ≦5%.
摘要翻译： 本发明的目的是，在不需要碱预处理的情况下，可以在镀锌后未进行合金化的热镀锌钢板上形成具有优异滑动性的氧化锌层，从而具有相对低的表面度 活动。 本发明的另一个目的是使得可以制造具有在涂层表面上形成的较高面积比的Zn氧化物层和较大厚度的氧化锌层的热浸镀锌钢板。 具体而言，本发明提供一种热镀锌钢板的制造方法，其特征在于，包括：对钢板进行热浸镀锌和随后的回火轧制; 使钢板与具有pH缓冲能力的酸性溶液接触; 在与酸性溶液接触后将钢板保持1秒至60秒; 并用水冲洗钢板，在钢板的涂层表面上形成氧化锌层，其特征在于，还包括：通过用Ra≧的钝辊首先轧制钢板进行回火轧制， 轧制压下率为2.0μm，nlE为5％，然后以Ra＆nlE为光亮辊;在轧制压下率为0.1μm的条件下，首先用Ra＆nlE的光辊轧制钢板，轧制压下率为0.1μm; 3％，然后用具有Ra＆nlE的钝辊;2.0μm的轧制压下率＆nlE; 5％。
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