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    Process for the preparation of E-isomers of 1-cyclohexyl-2-(1,2,4-triazol-1-yl)-1-penten-3-one derivatives
    1.
    发明授权
    Process for the preparation of E-isomers of 1-cyclohexyl-2-(1,2,4-triazol-1-yl)-1-penten-3-one derivatives 失效
    1-环己基-2-（1,2,4-三唑-1-基）-1-戊烯-3-酮衍生物的E-异构体的制备方法

    公开(公告)号：US4501897A

    公开(公告)日：1985-02-26

    申请号：US523537

    申请日：1983-08-16

    申请人： Wolf Reiser ,  Hans-Ludwig Elbe ,  Peter Feyen

    发明人： Wolf Reiser ,  Hans-Ludwig Elbe ,  Peter Feyen

    IPC分类号： C07D209/08 ,  C07D249/08 ,  C07D521/00

    CPC分类号： C07D231/12 ,  C07D233/56 ,  C07D249/08

    摘要： A process for the preparation of E-isomers of 1-cyclohexyl-2-(1,2,4-triazol-1-yl)-1-penten-3-one derivatives of the formula ##STR1## in which X and Y independently of one another represent hydrogen or halogen by contacting isomers of 1-cyclohexyl-2-(1,2,4-triazol-1-yl)-1-penten-3-one derivatives of the formula ##STR2## in which X and Y have the previously indicated meaning with at least one secondary amine, if desired in the presence of water and/or in the presence of a water immiscible solvent.

    摘要翻译： 制备式（I）的1-环己基-2-（1,2,4-三唑-1-基）-1-戊烯-3-酮衍生物的E-异构体的方法，其中X 和Y彼此独立地表示氢或卤素，通过使式（VI）的1-环己基-2-（1,2,4-三唑-1-基）-1-戊烯-3-酮衍生物的异构体 ），其中如果需要，在水的存在下和/或在与水不混溶的溶剂的存在下，X和Y具有至少一个仲胺的前述含义。

    Process for the preparation of hydroxybenzaldoxime o-ethers
    4.
    发明授权
    Process for the preparation of hydroxybenzaldoxime o-ethers 失效
    制备羟基苯甲醛肟醚的方法

    公开(公告)号：US4973753A

    公开(公告)日：1990-11-27

    申请号：US320145

    申请日：1989-03-07

    申请人： Reinhard Lantzsch ,  Hans-Ludwig Elbe ,  Wolf Reiser ,  Johannes Schmetzer

    发明人： Reinhard Lantzsch ,  Hans-Ludwig Elbe ,  Wolf Reiser ,  Johannes Schmetzer

    IPC分类号： C07C67/00 ,  C07C239/00 ,  C07C251/48 ,  C07D249/08 ,  C07D521/00

    CPC分类号： C07D231/12 ,  C07D233/56 ,  C07D249/08

    摘要： Hydroxybenzaldoxime O-ethers of the formula ##STR1## in which R.sup.1 represents alkyl,are obtained by a process in which a tert.-butoxy-benzaldoxime of the formula ##STR2## is reacted with alkylating agents of the formulaR.sup.1 --Xin whichR.sup.1 has the abovementioned meaning andX represents halogen or OSO.sub.2 OR.sup.1,whereinR.sup.1 again has the abovementioned meaning,in the presence of a strong base and phase transfer catalyst and in the presence of a diluent at temperatures between 0.degree. C. and 50.degree. C., and the products are then treated with anhydrous acid at temperatures between 0.degree. C. and 50.degree. C.,Hydroxybenzaldoxime O-ethers can be used as intermediate products for the synthesis of compounds with a fungicidal, insecticidal and antimycotic activity. The tert.-butoxy-benzalodoxime starting material is a new compound.

    摘要翻译： 其中R1代表烷基的式“IMAGE”的羟基苯甲醛肟O-醚通过下列方法获得，其中式（ⅩⅧ）的叔丁氧基 - 苯甲醛肟与式R 1 -X的烷基化剂反应，其中R 1 具有上述含义，X表示卤素或OSO 2 OR 1，其中R1在强碱和相转移催化剂存在下，在0℃至50℃的温度下，在稀释剂存在下，再次具有上述含义， 然后在0℃至50℃的温度下用无水酸处理产物，羟基苯甲醛肟O-醚可用作合成具有杀真菌，杀虫和抗真菌活性的化合物的中间产物。 叔丁氧基苯并肟原料是一种新的化合物。

    Novel substituted azolylvinyl ketones and carbinols as fungicides and plant growth regulators
    5.
    发明授权
    Novel substituted azolylvinyl ketones and carbinols as fungicides and plant growth regulators 失效
    新型取代的唑基乙烯基酮和甲醇作为杀真菌剂和植物生长调节剂

    公开(公告)号：US4728356A

    公开(公告)日：1988-03-01

    申请号：US754788

    申请日：1985-07-12

    申请人： Hans-Ludwig Elbe ,  Wolf Reiser ,  Erik Regel ,  Karl H. Buchel ,  Paul Reinecke ,  Wilhelm Brandes ,  Klaus Lurssen ,  Paul-Ernst Frohberger

    发明人： Hans-Ludwig Elbe ,  Wolf Reiser ,  Erik Regel ,  Karl H. Buchel ,  Paul Reinecke ,  Wilhelm Brandes ,  Klaus Lurssen ,  Paul-Ernst Frohberger

    IPC分类号： A01N43/50 ,  A01N43/653 ,  C07D233/60 ,  C07D249/08 ,  C07D521/00

    CPC分类号： C07D231/12 ,  A01N43/50 ,  A01N43/653 ,  C07D233/56 ,  C07D249/08

    摘要： A substituted azolylvinyl ketone or carbinol of the formula ##STR1## in which R.sup.1 represents optionally substituted cycloalkyl with 3 to 5 carbon atoms, substituted cyclohexyl or the grouping ##STR2## wherein R.sup.3 represents optionally substituted phenyl, alkenyl, alkinyl, cyano or the grouping --Z--R.sup.4,whereinR.sup.4 represents alkyl, halogenoalkyl, optionally substituted phenyl or optionally substituted phenylalkyl andZ represents O, S, SO or SO.sub.2,n represents a number from 0 to 2,R.sup.2 represents alkyl, alkenyl, alkinyl, in each case optionally substituted phenyl or phenylalkyl, or in each case optionally substituted cycloalkyl, cycloalkylalkyl, cycloalkenyl, cycloalkenylalkyl, bicycloalkyl or bicycloalkenyl, but R.sup.2 does not represent optionally substituted phenyl at the same time as R.sup.1 represents optionally substituted cycloalkyl with 3 to 5 carbon atoms or substituted cyclohexyl or R.sup.3 represents optionally substituted phenyl,X represents the CO or CH(OH) group andY represents a nitrogen atom or the CH group,or an addition product thereof with an acid or metal salt.The products are active in combating fungi and in regulating the growth of plants.

    摘要翻译： 其中R 1表示任选取代的具有3至5个碳原子的环烷基，取代的环己基或基团，其中R 3表示任选取代的苯基，烯基，炔基，氰基或基团 - Z-R4，其中R4代表烷基，卤代烷基，任选取代的苯基或任选取代的苯基烷基，Z代表O，S，SO或SO 2，n代表0至2的数，R 2代表烷基，烯基，炔基， 取代的苯基或苯基烷基，或者在每种情况下都是任选取代的环烷基，环烷基烷基，环烯基，环烯基烷基，双环烷基或双环烯基，但R 2不同时代表任选取代的苯基，其中R 1表示任选取代的具有3至5个碳原子的环烷基或取代的环己基 或R 3表示任选取代的苯基，X表示CO或CH（OH）基团，Y表示氮气 m或CH基团，或其与酸或金属盐的加成产物。 该产品在防治真菌和调节植物生长方面发挥积极作用。

    Combating fungi with 1-phenyl-2-(1,2,4-triazol-1-yl)-prop-2-en-1-ones
    7.
    发明授权
    Combating fungi with 1-phenyl-2-(1,2,4-triazol-1-yl)-prop-2-en-1-ones 失效
    将真菌与1-苯基-2-（1,2,4-三唑-1-基） - 丙-2-烯-1-酮

    公开(公告)号：US4435411A

    公开(公告)日：1984-03-06

    申请号：US259304

    申请日：1981-04-30

    申请人： Wolf Reiser ,  Hans-Ludwig Elbe ,  Karl Buchel ,  Paul-Ernst Frohberger ,  Wilhelm Brandes

    发明人： Wolf Reiser ,  Hans-Ludwig Elbe ,  Karl Buchel ,  Paul-Ernst Frohberger ,  Wilhelm Brandes

    IPC分类号： A01N43/653 ,  C07D249/08 ,  C07D521/00 ,  A01N43/64 ,  C07F1/08

    CPC分类号： C07D231/12 ,  A01N43/653 ,  C07D233/56 ,  C07D249/08

    摘要： A 1-phenyl-2-(1,2,4-triazol-1-yl)-prop-2-en-1-one of the formula ##STR1## in which R is methyl, ethyl, isopropyl, alkyl with more than 3 carbon atoms, optionally substituted cycloalkyl, optionally substituted cycloalkenyl, optionally substituted alkenyl, optionally substituted alkynyl, optionally substituted phenoxyphenyl, or phenylalkyl which is optionally substituted in the alkyl part and/or in the phenyl part,X each independently is halogen, optionally substituted phenyl or optionally substituted phenoxy, andn is 0, 1, 2 or 3,or an addition product thereof with a physiologically acceptable acid or a metal salt which possesses fungicidal activity.

    摘要翻译： 1-苯基-2-（1,2,4-三唑-1-基） - 丙-2-烯-1-酮，其中R是甲基，乙基，异丙基，烷基，多于 3个碳原子，任选取代的环烷基，任选取代的环烯基，任选取代的烯基，任选取代的炔基，任选取代的苯氧基苯基或在烷基部分和/或苯基部分任选取代的苯基烷基，X各自独立地为卤素， 苯基或任选取代的苯氧基，n为0,1,2或3，或其与具有杀真菌活性的生理学上可接受的酸或金属盐的加成产物。

    Process for the preparation of oxiranes
    8.
    发明授权
    Process for the preparation of oxiranes 失效
    环氧乙烷的制备方法

    公开(公告)号：US4929735A

    公开(公告)日：1990-05-29

    申请号：US185211

    申请日：1988-04-22

    申请人： Wolf Reiser ,  Peter Feyen

    发明人： Wolf Reiser ,  Peter Feyen

    IPC分类号： C07D405/06 ,  C07D301/02 ,  C07D303/08 ,  C07D303/22 ,  C07D521/00

    CPC分类号： C07D303/22 ,  C07D231/12 ,  C07D233/56 ,  C07D249/08 ,  C07D303/08

    摘要： A process for the preparation of an oxirane of the formula ##STR1## in which X is 4-chlorobenzyl, 4-phenylphenoxy or 1H-(1,2,4)-triazolyl,comprising reacting dimethyl sulphate with an excess of dimethyl sulphide thereby to form trimethylsulphonium methyl-sulphate of the formula(CH.sub.3).sub.3 S.sym.CH.sub.3 SO.sub.4 .crclbar.,and without prior isolation reacting the trimethylsulphonium methyl-sulphate with a keytone of the formula ##STR2## in the presence of solid potassium hydroxide or sodium hydroxide in dimethyl sulphide at a temperature between 0.degree. C. and 50.degree. C.

    摘要翻译： 制备式“IMAGE”的环氧乙烷的方法，其中X是4-氯苄基，4-苯基苯氧基或1H-（1,2,4） - 三唑基，包括使硫酸二甲酯与过量的二甲基硫醚反应，从而 形成式（CH 3）3 S（+）CH 3 SO 4（ - ）的三甲基锍甲基硫酸盐，并且不经事先分离，在固体氢氧化钾或氢氧化钠存在下，使甲基硫酸三甲基锍与式 二硫化碳在0℃至50℃的温度下进行。

    Process for the preparation of 3-isomers of 1-cyclohexyl-2-(1,2,4-triazol-1-yl)-1-penten-3-one derivatives
    9.
    发明授权
    Process for the preparation of 3-isomers of 1-cyclohexyl-2-(1,2,4-triazol-1-yl)-1-penten-3-one derivatives 失效
    1-环己基-2-（1,2,4-三唑-1-基）-1-戊烯-3-酮衍生物的3-异构体的制备方法

    公开(公告)号：US4607108A

    公开(公告)日：1986-08-19

    申请号：US623800

    申请日：1984-06-22

    申请人： Peter Feyen ,  Gebhard Rauleder ,  Wolf Reiser

    发明人： Peter Feyen ,  Gebhard Rauleder ,  Wolf Reiser

    IPC分类号： C07D209/08 ,  C07D249/08 ,  C07D521/00

    CPC分类号： C07D231/12 ,  C07D233/56 ,  C07D249/08

    摘要： The known E-isomers of compounds of the formula ##STR1## in which X and Y independently of each other represent hydrogen or halogen,are obtained according to a new process, in which triazolylketones of the formula ##STR2## in which X and Y have the above mentioned meaning, are reacted with an excess of cyclohexanecarbaldehyde in the presence of a non-polar organic diluent and in the presence of a catalyst mixture of organic acids and secondary amines in a molar ratio of 1:0.5 to 1:1 at temperatures between 40.degree. and 100.degree. C. by continuously removing the water formed and subsequently working up in the manner that is described in the specification.

    摘要翻译： 根据新方法获得式（I）化合物的已知E-异构体，其中X和Y彼此独立地表示氢或卤素，其中式（I）的三唑基酮 其中X和Y具有上述含义，在非极性有机稀释剂的存在下与过量的环己烷甲醛反应，并且在有机酸和仲胺的催化剂混合物存在下，摩尔比为1:0.5 通过连续地除去形成的水并随后按照说明书中描述的方式进行处理，在40℃至100℃的温度下加热至1:1。

    Fungicidal agents
    10.
    发明授权
    Fungicidal agents 失效
    杀真菌剂

    公开(公告)号：US4826857A

    公开(公告)日：1989-05-02

    申请号：US176479

    申请日：1988-04-01

    申请人： Wolfgang Kramer ,  Joachim Weissmuller ,  Wolf Reiser ,  Dieter Berg ,  Wilhelm Brandes ,  Paul Reinecke

    发明人： Wolfgang Kramer ,  Joachim Weissmuller ,  Wolf Reiser ,  Dieter Berg ,  Wilhelm Brandes ,  Paul Reinecke

    IPC分类号： A01N43/36 ,  A01N43/40 ,  A01N43/46 ,  A01N43/50 ,  A01N43/54 ,  A01N43/60 ,  A01N43/653 ,  A01N43/84 ,  A01N47/38 ,  A01N47/42 ,  A01N43/64

    CPC分类号： A01N43/84 ,  A01N43/36 ,  A01N43/40 ,  A01N43/50 ,  A01N43/54 ,  A01N43/60 ,  A01N43/653 ,  A01N47/38 ,  A01N47/42

    摘要： A synergistic fungicidal composition comprising a fungicidally effective amount of at least one amino compound of the formula ##STR1## in which R represents optionally substituted cycloalkyl or optionally substituted aryl,R.sup.1 represents hydrogen or alkyl,R.sup.2 represents alkyl,R.sup.3 represents alkyl andR.sup.4 represents alkyl, alkenyl or alkinyl, orR.sup.3 and R.sup.4, together with the nitrogen atom to which they are bonded, represent an optionally substituted saturated heterocyclic radical, which can contain further hetero-atoms,X represents oxygen or sulphur,Y represents oxygen, sulphur or the methylene group,m represents 0 or 1 andn represents 0 or 1,or an addition product thereof with an acid, metal salt or quaternizing agent, and at least one member selected from the group consisting of several individually known fungicides.

    摘要翻译： 一种协同杀真菌组合物，其包含杀真菌有效量的至少一种下式的氨基化合物，其中R表示任选取代的环烷基或任选取代的芳基，R 1表示氢或烷基，R 2表示烷基，R 3表示烷基，R 4表示烷基 ，链烯基或炔基，或者R 3和R 4与它们所键合的氮原子一起代表任选取代的饱和杂环基，其可含有其它杂原子，X表示氧或硫，Y表示氧，硫或 亚甲基，m表示0或1，n表示0或1，或其与酸，金属盐或季铵化剂的加成产物，以及选自几种单独已知的杀真菌剂中的至少一种。