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104 条记录 (耗时 0.015 秒)

    Hc-co(ch,cho)xh
    91.
    再颁专利
    Hc-co(ch,cho)xh 失效

    公开(公告)号：USRE27969E

    公开(公告)日：1974-04-16

    申请号：US27969D

    申请日：1972-06-08

    IPC分类号： C07F9/08 ,  C07F9/09 ,  C07F9/22 ,  C08G18/46 ,  C08G18/50

    CPC分类号： C08G18/5075 ,  C07F9/08 ,  C07F9/091 ,  C07F9/22 ,  C08G18/4684

    摘要： PHOSPHORUS-CONTAINING COMPOUNDS WHICH ARE USEFUL IN THE PREPARATION OF POLYURETHANES AND WHICH ARE DERIVED FROM (1) PHOSPHORUS COMPOUNDS CONTAINING AT LEAST ONE ACTIVE FUNCTION (2) ALKYLENE OXIDES OR EPIHALOHYDRIN AND (3) DICARBOXYLIC ACID ANHYDRIDES ARE PROVIDED. AMONG THE COMPOUNDS ARE THOSE PREPARED BY REACTING A DICARBOXYLIC ACID ANHYDRIDE WITH A PHOSPHORUS ACID WHICH HAS BEEN PARTIALLY OR COMPLETELY REACTED WITH AN ALKYLENE OXIDE OR EPIHALOHYDRIN, FOLLOWED BY REACTION OF THE CARBOXYL GROUP THUS FORMED WITH ADDITIONAL ALKYLENE OXIDE OR EPIHALOHYDRIN. METHODS FOR PREPARATION OF THE COMPOUNDS ARE ALSO PROVIDED.

    Process for the preparation of phosphonamides
    93.
    发明授权
    Process for the preparation of phosphonamides 失效
    制备磷酰胺的方法

    公开(公告)号：US3558635A

    公开(公告)日：1971-01-26

    申请号：US3558635D

    申请日：1967-11-20

    申请人： RHONE POULENC SA

    发明人： NORMANT HENRI MARIE

    IPC分类号： C07F9/22 ,  C07F9/44 ,  C07F9/59

    CPC分类号： C07F9/591 ,  C07F9/22 ,  C07F9/222 ,  C07F9/224 ,  C07F9/44 ,  C07F9/4407

    摘要： THE INVENTION RELATES TO ALKALI METAL DIAMIDOPHOSPHITES OF FORMULA:

    (-)O-P(-N(-R1)-R2)2 M(+)

    WHERE R1 AND R2 ARE ORGANIC RADICALS AND M IS AN ALKALI METAL, WHICH CAN BE PREPARED BY REACTING A HALOGENOPHOSPHONAMIDE WITH AN ALKALI METAL, FOR EXAMPLE SODIUM, IN A SUITABLE SOLVENT. EXAMPLES OF SUITABLE DIAMIDOPHOSPHITES ARE SODIUM N,N,N'',N''-TETRAMETHYLDIAMIDOPHOSPHITE, N,N,N'',N''-TETRAETHYLDIAMIDEOPHOSPHITE AND DIPIPER IDINOPHOSPHITE. THE INVENTION ALSO RELATES TO A PROCESS FOR CONVERTING THE DIAMIDOPHOSPHITES INTO ORGANIC COMPOUNDS CONTAINING THE

    -P(=O)(-N(-R1)-R2)2

    GROUP BY REACTING THEM WITH A REACTIVE ESTER. THE PHOSPHONAMIDE PRODUCTS ARE USEFUL AS PESTICIDES.

    Process for making organic derivatives of pyrophosphoric and hypophosphoric acids
    98.
    发明授权
    Process for making organic derivatives of pyrophosphoric and hypophosphoric acids 失效
    制造焦磷酸和次磷酸的有机衍生物的方法

    公开(公告)号：US3247198A

    公开(公告)日：1966-04-19

    申请号：US12954661

    申请日：1961-08-07

    申请人： PECHINEY PROGIL SOC FOR THE DE

    发明人： JEAN-MARIE CHEYMOL ,  DE LASSAUNIERE PIERRE EUGENE C ,  MOHAMED SELIM

    IPC分类号： C07F9/08 ,  C07F9/09 ,  C07F9/22 ,  C07F9/24 ,  C07F9/59 ,  C07F9/6533

    CPC分类号： C07F9/6533 ,  C07F9/08 ,  C07F9/098 ,  C07F9/22 ,  C07F9/2433 ,  C07F9/245 ,  C07F9/591

    摘要： Organic tetrasubstituted ester and amide derivatives of pyrophosphoric or hypophosphoric acid are prepared by reacting a tetramethylammonium salt of an appropriately disubstituted derivative of orthophosphoric acid with a halogeno-derivative of an appropriately disubstituted derivative of orthophosphoric or phosphorous acid. The products may be of formula or where R1, R2, R3 and R4 represent radicals (a) of monohydroxy alcohols that are saturated or unsaturated, unsubstituted or nitrated, and belong to the aliphatic, cycloaliphatic, aromatic and/or heterocyclic series, (b) of substituted or unsubstituted monophenols, and/or (c) of aliphatic amines, aromatic amines, cycloaliphatic amines and/or heterocyclic amines in which the nitrogen is in the heterocyclic ring. Many examples are given. Compounds of the above formulae are claimed per se with the provisos that where the R radicals are all from unsubstituted monohydroxy alcohols or unsubstituted monohydroxy phenols, at least one differs from the other three, that where all four R radicals are derived from amines, they all differ from one another, and that when two R radicals are from unsubstituted alcohols and the other two from alkyl amines, either the pair of alcohol radicals or the alkylamine radicals or both pairs are dissimilar. The reaction may be effected in an inert solvent, preferably one in which the (CH2)4NCl formed is insoluble.