公开(公告)号：US09353208B2

公开(公告)日：2016-05-31

申请号：US14259884

申请日：2014-04-23

Applicant: Hexion Inc.

Inventor： Stephen W. Arbuckle ,  Gabriele Badini ,  John Huggins ,  Sanjay Gangal

IPC: C08G8/24 ,  C08J3/12 ,  C08G8/22

CPC classification number: C08G8/24 ,  C08G8/22 ,  C08J3/12 ,  C08J2361/08 ,  C08J2361/12 ,  C08L61/12

Abstract: Sol-gel resins can be prepared using one or two-step processes to produce small granules or pellets of resin that are easy to handle. The methods include agitating phenolic compounds and aldehydes in the presence of a catalyst and a solvent. The reactants are brought together over a period of time to avoid an undesirable buildup of heat within the reaction mass. Condensation of the material continues under agitation sufficient to knead the material as it gels. During this gelation, the material begins to form into smaller parts until particles, the shape of granules, are produced. The condensation continues to the degree that the material is no longer capable of sintering during packaging and storage. The material thus made can be easily discharged, packaged, portioned, and further processed.

Abstract translation: 溶胶 - 凝胶树脂可以使用一步或两步法制备，以生产易于处理的小颗粒或树脂颗粒。 所述方法包括在催化剂和溶剂的存在下搅拌酚类化合物和醛。 将反应物在一段时间内聚合在一起，以避免反应物料内不希望的热积聚。 材料的冷凝在搅拌下持续，足以在其凝胶时捏合材料。 在这种凝胶化过程中，材料开始形成较小的部分，直到产生颗粒的形状。 冷凝继续到在包装和储存期间材料不再能够烧结的程度。 由此制成的材料可以容易地排出，包装，分割和进一步加工。

公开(公告)号：US09234077B2

公开(公告)日：2016-01-12

申请号：US14060944

申请日：2013-10-23

Applicant: Hexion Inc.

Inventor： Jim D. Elmore ,  Larry Steven Corley ,  Jerry R. Hite

IPC: C08G65/26 ,  C08G65/333 ,  C08G73/02 ,  C08L79/02 ,  C08G59/44 ,  C08L63/00 ,  C08L63/02

CPC classification number: C08G65/33306 ,  C08G59/44 ,  C08G65/2621 ,  C08G65/2624 ,  C08G65/2627 ,  C08G65/33396 ,  C08G73/028 ,  C08L63/00 ,  C08L79/02

Abstract: Compositions and methods for forming surfactants, aqueous dispersions, and curing agents are provided. In one aspect, the invention relates to improved epoxy functional surfactants prepared by reaction of an epoxy composition and an amidoamine composition formed from a blend of acid-terminated polyoxyalkylene polyols. The improved epoxy functional surfactants may be reacted with an excess of epoxy composition and water to result in an aqueous dispersion. The amidoamine composition may be a reaction mixture of a diamine compound and an acid terminated polyoxyalkylene composition formed from two or more polyoxyalkylene polyol compounds. The epoxy functional surfactant may be reacted with amine compounds to form a compound suitable as a curing agent.

公开(公告)号：US20150148487A1

公开(公告)日：2015-05-28

申请号：US14610852

申请日：2015-01-30

Applicant: Hexion Inc.

Inventor： Yingchao Zhang ,  Raman C. Subrayan ,  Vinay Malhotra ,  David A. Snover

IPC: C08L67/00 ,  C08L33/00 ,  C08L33/08 ,  C08L33/26 ,  C08L29/04 ,  C08L33/02

CPC classification number: C08L67/00 ,  C03C25/1095 ,  C03C25/24 ,  C03C25/323 ,  C08K5/07 ,  C08L29/04 ,  C08L33/00 ,  C08L33/02 ,  C08L33/08 ,  C08L33/26 ,  D04H1/587 ,  D04H1/64 ,  D04H13/00 ,  D06M13/224 ,  Y10T442/2779 ,  Y10T442/2787 ,  Y10T442/2811 ,  Y10T442/2844 ,  Y10T442/2861 ,  Y10T442/2934 ,  Y10T442/2967 ,  Y10T442/2992

Abstract: Polyester materials, methods for making polyesters materials, and uses of the polyester materials in binder materials and articles of manufacture are disclosed. In one embodiment, a process is provided for preparing a polyester solution, including mixing monomers of at least one organic acid containing at least three carboxylic groups and at least one multi-hydroxyl alcohol containing at least three hydroxyl groups to form a reaction mixture, heating the reaction mixture to a first temperature, polymerizing the monomers at the first temperature until reaching an acid value from about 200 to about 400 mg KOH/g, adjusting the temperature to a second temperature less than the first temperature, and forming the polyester solution. The polyester materials may be mixed with cross-linking materials to form binder materials. The binder material may then be used to form articles of manufacture.

Abstract translation: 公开了聚酯材料，聚酯材料的制备方法以及聚酯材料在粘合剂材料和制品中的应用。 在一个实施方案中，提供了制备聚酯溶液的方法，包括混合至少一种含有至少三个羧基的有机酸的单体和至少含有至少三个羟基的多羟基醇以形成反应混合物，加热 将反应混合物转化为第一温度，在第一温度下聚合单体，直到达到约200至约400mg KOH / g的酸值，将温度调节至低于第一温度的第二温度，并形成聚酯溶液。 聚酯材料可以与交联材料混合以形成粘合剂材料。 然后可以将粘合剂材料用于形成制品。