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    Method and device for the production of alkylene oxide addition products
    2.
    发明授权
    Method and device for the production of alkylene oxide addition products 有权
    用于生产环氧烷加成产物的方法和装置

    公开(公告)号：US08273925B2

    公开(公告)日：2012-09-25

    申请号：US12524172

    申请日：2007-12-08

    申请人： Stefan Franzen ,  Thomas Koelker

    发明人： Stefan Franzen ,  Thomas Koelker

    IPC分类号： C07C29/00 ,  B01J19/00

    CPC分类号： C08G65/2609 ,  C08G65/2615 ,  C08G65/2621 ,  C08G65/2696

    摘要： A method for the production of alkylene oxide addition products comprising (i) charging a stirred reactor with a starting compound capable of adding on or inserting alkylene oxides, introducing at least one alkylene oxide plus a different diluent gas, wherein a portion of said alkylene oxide reacts in a liquid phase with said starting compound, and the remaining alkylene oxide together with said diluent gas forms a gas phase above the liquid phase, (ii) continuously drawing off said liquid phase from the bottom of the reactor via an outlet stub, and recycling to the top of the reactor via an external circulation system, which comprises at least one heat exchanger and at least one Venturi nozzle within said external circulation system, and (iii) metering said gas phase comprising alkylene oxide into said Venturi nozzle via a vacuum line.

    摘要翻译： 一种用于生产环氧烷加成产物的方法，包括（i）向搅拌反应器中加入能够加入或插入烯化氧的起始化合物，引入至少一种环氧烷加上不同的稀释气体，其中一部分所述环氧烷烃 在液相中与所述起始化合物反应，剩余的环氧烷与所述稀释气体一起在液相上形成气相，（ii）经由出口残渣从反应器的底部连续地抽出液相，以及 通过外部循环系统再循环到反应器的顶部，外部循环系统包括至少一个热交换器和在所述外部循环系统内的至少一个文丘里喷嘴，以及（iii）通过真空将所述包含环氧烷的气相计量到所述文丘里喷嘴中 线。

    METHOD FOR PRODUCING POLYOLS CONTAINING AMINO GROUPS
    3.
    发明申请
    METHOD FOR PRODUCING POLYOLS CONTAINING AMINO GROUPS 审中-公开
    生产含有氨基团的多元醇的方法

    公开(公告)号：US20120184705A1

    公开(公告)日：2012-07-19

    申请号：US13498772

    申请日：2010-09-27

    申请人： Klaus Lorenz ,  Manfred Schmidt

    发明人： Klaus Lorenz ,  Manfred Schmidt

    IPC分类号： C08G18/32 ,  C07C217/08 ,  C07C213/04

    CPC分类号： C08G65/30 ,  C08G18/10 ,  C08G18/3819 ,  C08G18/5021 ,  C08G18/7664 ,  C08G65/2621

    摘要： The present invention provides a simple method with no processing for producing polyols based on amino group-containing starter compounds. Unless explicitly specified, polyols are understood to be polyether polyols, polyether ester polyols and also polyether ester amide polyols. The invention also provides the polyols obtainable by the method according to the invention and the use of the polyols according to the invention to produce polyurethane materials.

    摘要翻译： 本发明提供了一种基于含氨基起始化合物制备多元醇的方法。 除非另有明确规定，多元醇被理解为聚醚多元醇，聚醚酯多元醇以及聚醚酯酰胺多元醇。 本发明还提供可通过本发明的方法获得的多元醇以及根据本发明的多元醇的用途来生产聚氨酯材料。

    Method for providing polymers with durable improved properties
    7.
    发明授权
    Method for providing polymers with durable improved properties 失效

    公开(公告)号：US4045510A

    公开(公告)日：1977-08-30

    申请号：US616183

    申请日：1975-09-24

    申请人： Robert B. Login

    发明人： Robert B. Login

    IPC分类号： C08G18/50 ,  C08G65/26 ,  C08L67/02 ,  C08L77/00 ,  C09K3/16 ,  D06M13/165 ,  D06M15/55 ,  D06M15/564 ,  C08L63/00

    CPC分类号： D06M15/564 ,  C08G18/5021 ,  C08G65/2621 ,  C08L67/02 ,  C08L77/00 ,  C09K3/16 ,  D06M13/165 ,  D06M15/55 ,  D06M2200/00 ,  Y10S8/08

    摘要： Polymers reactive towards free amino groups, such as polyamides, polyureas, polyurethanes or polyesters, are provided with durable modified properties by being brought into contact with an additive polymeric material which (a) is compatible with the polymer being treated, (b) contains a plurality of oxyalkylene groups effective to impart to the modified polymer improved properties such as reduced static propensity, modified dyeability, or greater water absorbency; and (c) has one or more reactive sites, in the form of a pendant free primary amino group or potential primary amino group, blocked by the dehydration of an aldehyde or a ketone with the amine, which in either case affords the capability in proper circumstances of attaching the modifying polymeric material to the polymer being treated by a covalent chemical bond. Suitable modifying polymers are made by reacting a diamino or higher amino compound with a proportion of an aldehyde or ketone sufficient to block at least some of the amino groups present, oxyalkylating the blocked starting material through a surviving amino group to an extent capable of affording the desired properties, and if desired, cross-linking or chain-extending the resulting material to obtain a substance of increased molecular weight. Modifying polymers so made may be used as such (i.e., in the aldehyde- or ketone-blocked form) for treatment of the reactable polymer to be modified, either by blending into a melt or by surface treatment of freshly produced fiber or sheet material. The formation of free amino groups in the modifying polymer can occur in situ when the modified polymer is exposed to water under suitable conditions. The modifying polymer may also be used in a free amino form generated by hydrolyzing before bringing it into contact with the polymer to be modified. Novel treated polymers are thus produced which display modified properties which are retained despite repeated washings and/or long-continued use.