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11.
公开(公告)号:US20210322283A1
公开(公告)日:2021-10-21
申请号:US17273042
申请日:2019-08-22
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Michael Jahns , Jacqueline C. Rolf , Martin Goetzinger , Holger Hauptmann
Abstract: The invention relates to a glazing composition suitable for glazing the surface a dental zirconia article. The glazing composition comprises a liquid, glass particles, and hydrophilic silica nano-particles. The invention also relates to a process for sintering a porous dental zirconia article with a glazing composition on its surface.
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12.
公开(公告)号:US20210196579A1
公开(公告)日:2021-07-01
申请号:US17273048
申请日:2019-08-30
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Michael Jahns , Jacqueline C. Rolf , Martin Goetzinger , Holger Hauptmann
Abstract: The invention relates to a glazing composition for a porous dental zirconia article, the glazing composition comprising liquid, glass particles, fluorescing component(s) comprising europium, optionally hydrophilic silica nano-particles, and optionally hydrophobic silica nano-particles, wherein the fluorescing component(s) can be contained in the glass particles or as separate component. The invention also relates to a process for sintering a porous dental zirconia article with a glazing composition on its surface.
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公开(公告)号:US10350032B2
公开(公告)日:2019-07-16
申请号:US15128637
申请日:2015-03-18
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Michael Jahns , Jacqueline C. Rolf , Dajana Zimmermann
IPC: A61C8/00 , A61K6/02 , C04B41/85 , C04B41/00 , C04B41/50 , A61C5/77 , A61C7/00 , A61C13/00 , A61C13/08 , A61C19/06 , B05D1/28 , B05D3/10 , B05D3/12 , C04B111/00 , C04B111/80
Abstract: The invention relates to a process for selectively treating parts of the surface of a porous dental zirconia article, the process comprising the steps of providing a liquid composition and a porous 3-dimensional dental zirconia article having an outer and inner surface, applying the liquid composition to only a part the outer surface and/or inner surface of the porous dental zirconia article, the liquid composition comprising a whitening agent comprising a phosphorous containing component, the phosphorous containing component comprising a phosphate, phosphone or phosphine moiety, with the proviso that at least one P—O unit of the phosphate, phosphone or phosphine moiety is dissociable or able to otherwise interact with zirconia. The invention also relates to a dental zirconia article obtainable or obtained by such a process and a kit of parts comprising a container containing a certain liquid composition.
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公开(公告)号:US10028809B2
公开(公告)日:2018-07-24
申请号:US14436109
申请日:2013-10-02
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Michael Jahns , Holger Hauptmann
IPC: A61C13/00 , A61K6/02 , B32B18/00 , C04B35/486 , C04B35/624 , C04B35/626 , C04B35/632 , C04B35/634 , C04B38/00 , C01G25/02 , B82Y30/00 , A61C13/08 , C04B111/00
Abstract: The invention relates to a porous dental milling block comprising at least two geometrically defined Material Sections A and B, Material Section A comprising a tetragonal zirconia crystal phase in an amount A-T in % and a cubic zirconia crystal phase in an amount A-C in %, Material Section B comprising tetragonal zirconia crystal phase in an amount B-T in % and cubic zirconia crystal phase in an amount B-C in %, wherein (amount of tetragonal phase A-T in %)/(amount of cubic phase content A-C in %)>1 and (amount of tetragonal phase content B-T in %)/(amount of cubic phase content B-C in %)
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15.
公开(公告)号:US12121599B2
公开(公告)日:2024-10-22
申请号:US17273048
申请日:2019-08-30
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Michael Jahns , Jacqueline C. Rolf , Martin Goetzinger , Holger Hauptmann
IPC: A61K6/822 , A61K6/20 , A61K6/833 , A61K6/836 , C03C1/04 , C03C4/00 , C03C4/12 , C03C8/20 , C03C10/00 , C04B41/86
CPC classification number: A61K6/822 , A61K6/20 , A61K6/833 , A61K6/836 , C03C1/04 , C03C4/0021 , C03C4/12 , C03C8/20 , C03C10/0009 , C03C2204/00 , C03C2205/06 , C04B41/86
Abstract: The invention relates to a glazing composition for a porous dental zirconia article, the glazing composition comprising liquid, glass particles, fluorescing component(s) comprising europium, optionally hydrophilic silica nano-particles, and optionally hydrophobic silica nano-particles, wherein the fluorescing component(s) can be contained in the glass particles or as separate component. The invention also relates to a process for sintering a porous dental zirconia article with a glazing composition on its surface.
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公开(公告)号:US11738372B2
公开(公告)日:2023-08-29
申请号:US16769310
申请日:2018-12-06
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Anja Friedrich , Michael Jahns , Malte Korten , Christian A. Richter , Bastian P. Kirchner , Gallus Schechner , Daniel D. Oberpertinger , Wolfgang Weinmann
IPC: B08B3/10 , A61C5/77 , B29C64/35 , B33Y40/20 , B22F10/12 , B22F10/68 , B22F12/10 , B22F12/90 , B33Y80/00 , B29L31/00 , B22F10/40
CPC classification number: B08B3/104 , A61C5/77 , B22F10/12 , B22F10/68 , B22F12/10 , B22F12/90 , B29C64/35 , B33Y40/20 , B22F10/40 , B29L2031/7536 , B33Y80/00
Abstract: A system (1) for washing a 3D-printed object (4). The system (1) has a washing device (2) and a workpiece (3) that includes the 3D-printed object (4). The washing device (2) has a container (7) that forms a process chamber (8) for receiving a liquid cleaning agent (9), and the container (7) has an inlet (10) into the process chamber (8). The workpiece (3) further has a support structure (6) that supports the 3D-printed object (4) and a base (5) supporting the support structure (6). The base (5), in a mating relationship with the inlet (10), forms a restraint preventing the workpiece (3) from passing through the inlet (10) in a situation in which the workpiece (3) is placed with the 3D-printed object (4) located within the process chamber (8).
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公开(公告)号:US11207246B2
公开(公告)日:2021-12-28
申请号:US16485952
申请日:2018-03-02
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Mark B. Agre , Bradley D. Craig , Michael Jahns , William V. Chiu
Abstract: Disclosed herein are curable glass ionomer compositions that include a first paste and a second paste, and methods for using the disclosed compositions. The first paste includes water, a polyacid, and a non acid-reactive filler. The second paste includes water and an acid-reactive filler. At least one of the first paste and the second paste further includes substantially crystalline inorganic fibers. In some embodiments, the water content of the first paste and the second paste of the paste/paste GI composition disclosed herein is less than 20% by weight, based on the total weight of the composition.
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公开(公告)号:US20200324479A1
公开(公告)日:2020-10-15
申请号:US16769310
申请日:2018-12-06
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Anja Friedrich , Michael Jahns , Malte Korten , Christian A. Richter , Bastian P. Kirchner , Gallus Schechner , Daniel D. Oberpertinger , Wolfgang Weinmann
Abstract: A system (1) for washing a 3D-printed object (4). The system (1) has a washing device (2) and a workpiece (3) that includes the 3D-printed object (4). The washing device (2) has a container (7) that forms a process chamber (8) for receiving a liquid cleaning agent (9), and the container (7) has an inlet (10) into the process chamber (8). The workpiece (3) further has a support structure (6) that supports the 3D-printed object (4) and a base (5) supporting the support structure (6). The base (5), in a mating relationship with the inlet (10), forms a restraint preventing the workpiece (3) from passing through the inlet (10) in a situation in which the workpiece (3) is placed with the 3D-printed object (4) located within the process chamber (8).
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公开(公告)号:US20200230029A1
公开(公告)日:2020-07-23
申请号:US16485952
申请日:2018-03-02
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Mark B. Agre , Bradley D. Craig , Michael Jahns , William V. Chiu
Abstract: Disclosed herein are curable glass ionomer compositions that include a first paste and a second paste, and methods for using the disclosed compositions. The first paste includes water, a polyacid, and a non acid-reactive filler. The second paste includes water and an acid-reactive filler. At least one of the first paste and the second paste further includes substantially crystalline inorganic fibers. In some embodiments, the water content of the first paste and the second paste of the paste/paste GI composition disclosed herein is less than 20% by weight, based on the total weight of the composition.
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公开(公告)号:US10709529B2
公开(公告)日:2020-07-14
申请号:US15500442
申请日:2015-07-30
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Michael Jahns , Hans R. Schnagl
IPC: A61C13/00 , A61K6/78 , A61K6/818 , A61K6/824 , A61K6/833 , A61K6/891 , A61C5/20 , A61C5/77 , A61C7/00 , A61C8/00 , A61C13/08 , A61C13/271 , A61C13/277 , C04B35/488 , C04B41/00 , C04B41/46 , C04B41/53 , C04B41/82 , C04B41/91 , C09D17/00
Abstract: The present invention relates to a kit of parts comprising a dental mill blank comprising a porous zirconia material and a colouring solution for colouring the porous zirconia material. The porous zirconia material comprises Zr oxide calculated as ZrO2: from 80 to 97 wt.-%, Al oxide calculated as Al2O3: from 0 to 0.15 wt.-%, Y oxide calculated as Y2O3: from 1 to 10 wt.-%, Bi oxide calculated as Bi2O3: from 0.01 to 0.2 wt.-%, the porous zirconia material not comprising Fe calculated as Fe2O3 in an amount of more than 0.01 wt.-%, wt.-% with respect to the weight of the porous zirconia material. The colouring solution comprises solvent(s), colouring agent(s) comprising metal ions selected from Tb, Er, Pr, Mn or combinations thereof, the solution not comprising Fe ions in an amount of more than 0.01 wt.-%, the solution not comprising Bi ions in an amount of more than 0.01 wt.-%, wt.-% with respect to the weight of the colouring solution. The invention also relates to a process of producing a dental restoration, the process comprising the steps: providing a dental mill blank comprising a porous zirconia material as described in any of the preceding claims, machining an article out of the porous zirconia material, the article having the shape of a dental restoration with an outer and inner surface, providing a colouring solution as described in any of the preceding claims, applying the colouring solution to at least portions of the surface of the article having the shape of a dental restoration.
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