Process for stable biocide dispersion
    11.
    发明授权
    Process for stable biocide dispersion 失效
    稳定的杀生物剂分散方法

    公开(公告)号:US5319000A

    公开(公告)日:1994-06-07

    申请号:US880405

    申请日:1992-05-08

    摘要: The present invention relates, in one aspect, to a process for preparing a storage-stable dispersion of a biocide which comprises the steps of: (a) mixing a plastisol, comprising a resin and a carrier, and a biocide to provide a mixture of said plastisol and said biocide (b) heating said mixture of plastisol and biocide to an elevated temperature of between about 30.degree. C. and about 100.degree. C. to provide a homogeneous, storage stable dispersion, said dispersion containing said biocide in an amount of between about one and about 30 weight percent based upon the weight of said dispersion, said resin being present in an amount of between about 5 and about 75 weight percent based upon the weight of said dispersion, with the proviso that when the weight percent of said resin in said dispersion is between about 30% and about 75%, then said elevated temperature is between 30.degree. C. and 45.degree. C., and when the weight percent of said resin in said dispersion is between about 5% and about 29%, then said elevated temperature is between 46.degree. C. and 100.degree. C., and (c) cooling the dispersion to a temperature of between about -20.degree. C. and about 40.degree. C. to provide a storage-stable mixture having a viscosity of between about 2,000 and about 30,000 centipoise.

    摘要翻译: 本发明一方面涉及一种制备杀生物剂的储存稳定分散体的方法,该方法包括以下步骤:(a)将包含树脂和载体的增塑溶胶与杀生物剂混合以提供 所述增塑溶胶和所述杀生物剂(b)将所述增塑溶胶和杀生物剂的混合物加热至约30℃至约100℃的升高温度以提供均匀的储存稳定的分散体,所述分散体含有所述杀生物剂的量为 基于所述分散体的重量约1至约30重量%,所述树脂以所述分散体的重量计约5至约75重量%的量存在,条件是当所述分散体的重量百分数 所述分散体中的树脂为约30%至约75%,然后所述升高温度为30℃至45℃,当所述分散体中所述树脂的重量百分数为约5%至约29% ,t 母鸡表示升温在46℃至100℃之间,和(c)将分散体冷却至约-20℃至约40℃的温度,以提供具有粘度的储存稳定的混合物 介于约2,000至约30,000厘泊之间。

    Process for preparing 2,6-dichloropyridine
    15.
    发明授权
    Process for preparing 2,6-dichloropyridine 失效
    制备2,6-二氯吡啶的方法

    公开(公告)号:US5468864A

    公开(公告)日:1995-11-21

    申请号:US190956

    申请日:1994-02-03

    IPC分类号: C07D213/61

    CPC分类号: C07D213/61

    摘要: The present invention relates to a process for preparing 2,6-dichloropyridine which comprises reacting an organic solvent-free, catalyst-free reaction mixture comprising 2-chloropyridine and chlorine in the presence of a hydrogen chloride scavenger and ultraviolet light, and optionally in the presence of added moisture, at a temperature of between about 90.degree. C. and about 185.degree. C. Also claimed is a method for preventing calcium chloride plugging of the chlorine feed stream and for preventing calcium chloride build-up in the above reaction mixture which comprises adding moisture in the form of water or steam, or a combination thereof, to the reaction mixture prior to, or during, the reaction of said process.

    摘要翻译: 本发明涉及一种制备2,6-二氯吡啶的方法,该方法包括在氯化氢清除剂和紫外光的存在下使含有无溶剂的,不含催化剂的包含2-氯吡啶和氯的反应混合物反应, 在约90℃至约185℃的温度下存在加入的水分。还要求保护氯原料流中氯化钙堵塞和防止氯化钙在上述反应混合物中积聚的方法 包括在所述方法的反应之前或期间,将水或水蒸气或其组合的形式加入反应混合物中。

    In-situ generation of zinc pyrithione in personal care compositions
    17.
    发明授权
    In-situ generation of zinc pyrithione in personal care compositions 失效
    在个人护理组合物中原位生成吡啶硫酮锌

    公开(公告)号:US6162446A

    公开(公告)日:2000-12-19

    申请号:US38026

    申请日:1998-03-11

    摘要: Disclosed is a personal care composition comprising: (a) water or an alcohol, (b) at least one dispersant or surfactant, and (c) as an antimicrobial or preservative additive, particles of an in-situ transchelation reaction product of a zinc compound selected from the group consisting of zinc salts of organic acids, zinc salts of inorganic acids, zinc hydroxide, zinc oxide, and combinations thereof, said zinc compound being soluble in said water or alcohol, with pyrithione acid or a pyrithione salt that is soluble in said water or alcohol. Also disclosed is a process for preparing the personal care composition, and a coated substrate containing a coating of the personal care composition.

    摘要翻译: 公开了一种个人护理组合物,其包含:(a)水或醇,(b)至少一种分散剂或表面活性剂,和(c)作为抗微生物剂或防腐剂添加剂,锌化合物的原位经交换反应产物的颗粒 选自有机酸的锌盐,无机酸的锌盐,氢氧化锌,氧化锌及其组合,所述锌化合物可溶于所述水或醇,与吡啶硫酮酸或吡啶硫酮盐可溶于 说水或酒精。 还公开了一种制备个人护理组合物的方法,以及含有个人护理组合物的涂层的涂覆基质。

    Process for incorporating biocides into a liquid dispersion
    18.
    发明授权
    Process for incorporating biocides into a liquid dispersion 失效
    将杀生物剂掺入液体分散体的方法

    公开(公告)号:US5639803A

    公开(公告)日:1997-06-17

    申请号:US747076

    申请日:1991-08-19

    IPC分类号: A01N25/10 C08K5/00 C08K5/12

    摘要: This invention relates to a multi-step process for preparing a storage-stable dispersion of a biocide which comprises the steps of: (a) contacting a heat-swellable resin with a carrier to provide a liquid mixture of a resin and a carrier, (b) heating said liquid mixture to an elevated temperature to cause the resin to swell by virtue of carrier absorption into the resin to provide a swelled resin in said liquid mixture, and (c) adding a biocide to said swelled resin and mixing to provide a homogeneous, storage-stable liquid dispersion.

    摘要翻译: 本发明涉及一种用于制备杀生物剂的储存稳定分散体的多步骤方法,其包括以下步骤:(a)使热溶胀性树脂与载体接触以提供树脂和载体的液体混合物( b)将所述液体混合物加热到升高的温度,以使树脂由于载体吸收而溶胀到树脂中以在所述液体混合物中提供溶胀的树脂,和(c)向所述溶胀的树脂中加入杀生物剂并混合以提供 均匀,储存稳定的液体分散体。