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公开(公告)号:US20180161744A1
公开(公告)日:2018-06-14
申请号:US15738495
申请日:2017-01-17
Applicant: LG CHEM, LTD.
Inventor: Ye Hon KIM , Je Kyun LEE , Kyoung Shil OH
IPC: B01J13/00 , B41N10/02 , B65H37/00 , C01B33/158
Abstract: A method for manufacturing an aerogel sheet according to the present invention includes: a step (a) of preparing a blanket having a plate shape; a step (b) of mixing silica sol with gelling catalyst to prepare a silica sol precursor; and a step (c) of injecting the silica sol precursor prepared in the step (b) to a surface of the blanket prepared in the step (a) through an injection device to gelate the silica sol precursor, wherein, in the step (c), the injection device injects the silica sol precursor while moving from one side to the other side of the surface of the blanket.
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公开(公告)号:US20180134568A1
公开(公告)日:2018-05-17
申请号:US15578641
申请日:2017-03-16
Inventor: Ye Hon KIM , Je Kyun LEE , Hae Jin HWANG , Kyoung Jin LEE
IPC: C01B33/158
CPC classification number: C01B33/1585 , C01B33/158 , C01B33/159 , C01P2004/32 , C01P2004/61 , C01P2006/10 , C01P2006/12
Abstract: The present invention relates to a method for preparing spherical silica aerogel granules and spherical silica aerogel granules prepared thereby. The method for preparing spherical silica aerogel granules, which is suitable for mass production because droplets of a water glass solution are uniformly dispersed with a uniform size in a non-aqueous solvent using a surfactant in a certain step to reduce a process time and enhance productivity, may be provided. The spherical silica aerogel granules having a uniform size prepared by the method may be provided, wherein the spherical silica aerogel granules have a high working property and excellent flowability.
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公开(公告)号:US20160264427A1
公开(公告)日:2016-09-15
申请号:US14650519
申请日:2015-02-04
Applicant: LG CHEM, LTD.
Inventor: Kyoung Shil OH , Jin Hee OH , Ye Hon KIM , Dong Hyun CHO , Mi Ri KIM , Sung Min YU , Je Kyun LEE
IPC: C01B33/158
CPC classification number: C01B33/1585 , C01B33/16 , C01P2006/11 , C01P2006/12
Abstract: Provided is a method for preparing a hydrophobic silica aerogel by using a Soxhlet extraction, and a hydrophobic silica aerogel prepared by using the method. Since the preparation method according to the present invention may simultaneously perform washing and drying of a hydrophobic silica wet gel as well as solvent substitution and may remove an extraction solvent without an additional separation process, a hydrophobic silica aerogel having low tap density and high specific surface area may be easily prepared.
Abstract translation: 提供了通过使用索氏提取法制备疏水性二氧化硅气凝胶的方法和使用该方法制备的疏水性二氧化硅气凝胶。 由于根据本发明的制备方法可以同时进行疏水性二氧化硅湿凝胶的洗涤和干燥以及溶剂置换,并且可以在没有另外的分离过程的情况下除去萃取溶剂,具有低振实密度和高比表面积的疏水性二氧化硅气凝胶 区域可以容易地准备。
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公开(公告)号:US20210147243A1
公开(公告)日:2021-05-20
申请号:US17064148
申请日:2020-10-06
Applicant: LG CHEM, LTD.
Inventor: Ye Hon KIM , Je Kyun LEE , Kyoung Shil OH
IPC: C01B33/152 , B65H37/00 , C01B33/141 , B29C39/00 , C01B33/158 , B29B15/12 , F16L59/06 , F16L59/02 , C01B33/159
Abstract: The present invention relates to a method for manufacturing an aerogel sheet. The method for manufacturing an aerogel sheet includes: a step (a) of preparing silica sol; a step (b) of preparing a gelling catalyst; a step (c) of injecting the silica sol, which is prepared in the step (a), to a surface of a blanket to impregnate the silica sol; and a step (d) of injecting the gelling catalyst, which is prepared in the step (b), to the surface of the blanket, into which the silica sol is impregnated, to gelate the silica sol.
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公开(公告)号:US20190275489A1
公开(公告)日:2019-09-12
申请号:US16375438
申请日:2019-04-04
Applicant: LG CHEM, LTD.
Inventor: Ye Hon KIM , Je Kyun LEE
IPC: B01J13/00 , B01J27/24 , B01J19/24 , C01B33/158 , B01J37/04 , B01J31/02 , D06M11/60 , D06M13/507 , B01J35/12 , B05C3/09 , D06B5/22
Abstract: The present invention relates to an apparatus of manufacturing an aerogel sheet. The apparatus of manufacturing the aerogel sheet includes: a plurality of fixing vessels into which a fiber sheet is inserted; and an impregnation vessels provided with an accommodation part in which the plurality of fixing vessels are stacked in multistage and a silica precursor injection part which injects a silica precursor into the accommodation part to impregnate the silica precursor into the fiber sheet inserted into each of the fixing vessels.
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公开(公告)号:US20180370809A1
公开(公告)日:2018-12-27
申请号:US15742865
申请日:2017-03-07
Applicant: LG CHEM, LTD.
Inventor: Dong Kwon LEE , Ye Hon KIM , Jong Ku LEE , Je Kyun LEE
IPC: C01B33/158 , B01D3/14 , B01D5/00
CPC classification number: C01B33/1585 , B01D3/14 , B01D5/0045 , B01D5/006 , C02F1/52
Abstract: The system for preparing silica aerogel comprises a raw material supply part transferring at least one raw material of de-ionized water, water glass, a surface modifier, an inorganic acid, and an organic solvent to a mixing part, the mixing part mixing the raw materials transferred from the raw material supply part to produce silica wet gel, a separating part separating at least one raw material of the raw materials from the mixture containing the silica wet gel transferred from the mixing part, a drying part drying the silica wet gel transferred from the separating part to produce the silica aerogel, a recovery part recovering a portion of the vaporized raw material of the raw materials used in at least one of the mixing part and the drying part, and a heat transfer part transferring heat to at least one of the mixing part and the drying part.
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公开(公告)号:US20180354805A1
公开(公告)日:2018-12-13
申请号:US15736736
申请日:2017-02-03
Applicant: LG CHEM, LTD.
Inventor: Ye Hon KIM , Je Kyun LEE , Kyoung Shil OH
IPC: C01B33/158 , B01J31/02 , B01J27/24 , B01J35/12 , B65H16/10 , B65H18/08 , B65H20/06 , B65H20/02 , B65H37/00 , B05C3/132 , B05C3/12 , D06M13/507 , D06M11/60 , D06B5/22 , D06B3/10 , D06M15/333 , D06M15/347
Abstract: The present invention relates to a method for manufacturing an aerogel sheet and comprises: a step (a) of impregnating an acid solution into a fiber sheet to clean the fiber sheet by using the acid solution and impregnating a binder solution into the fiber sheet that is cleaned by using the acid solution to manufacture a pre-processed fiber sheet; a step (b) of impregnating a silica precursor into the pre-processed fiber sheet; and a step (c) of a gelling catalyst into the fiber sheet into which the silica precursor is impregnated to gelate the silica precursor.
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公开(公告)号:US20180264793A1
公开(公告)日:2018-09-20
申请号:US15755487
申请日:2017-02-07
Applicant: LG CHEM, LTD.
Inventor: Ye Hon KIM , Je Kyun LEE , Kyoung Shil OH
IPC: B32B37/12 , C08K3/36 , B32B37/15 , C01B33/159
CPC classification number: B32B37/12 , B01J13/0091 , B29B15/127 , B29C39/14 , B29C70/504 , B32B5/02 , B32B7/08 , B32B27/12 , B32B33/00 , B32B37/15 , B32B37/203 , B32B37/206 , B32B38/0012 , B32B38/164 , B32B2037/243 , B32B2038/0052 , B32B2266/126 , B32B2305/026 , B32B2307/102 , B32B2307/304 , B32B2307/722 , B32B2309/02 , B32B2309/027 , B32B2309/105 , C01B33/145 , C01B33/146 , C01B33/155 , C01B33/1585 , C01B33/159 , C08K3/36
Abstract: The present invention relates to a method for manufacturing a composite sheet comprising an aerogel sheet, which comprises: a step (S10) of preparing a fiber sheet (10); a step (S20) of laminating the aerogel sheet (30) on each of both surfaces of the fiber sheet (10); and a step (S30) of applying heat and a pressure to the aerogel sheet (30) and the fiber sheet (10), which are laminated, to bond the sheets to each other and to manufacture the composite sheet (40) in which the aerogel sheet (30), the fiber sheet (10), the aerogel sheet (30) are laminated.
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公开(公告)号:US20180179074A1
公开(公告)日:2018-06-28
申请号:US15738511
申请日:2017-02-03
Applicant: LG CHEM, LTD.
Inventor: Ye Hon KIM , Je Kyun LEE
IPC: C01B33/158 , C01B33/145 , B01J31/02 , B01J27/24 , B01J37/04
Abstract: The present invention relates to an apparatus of manufacturing an aerogel sheet. The apparatus of manufacturing the aerogel sheet includes: a fixing vessel into which a blanket is inserted; and an impregnation device putting a silica sol precursor into the blanket inserted into the fixing vessel to impregnate and gelate the silica sol precursor, wherein the impregnation device includes a rotation roller moving from one end to the other end of a top surface of the blanket while rotating to put the stored silica sol precursor into the blanket and thereby to impregnate and gelate the silica sol precursor.
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