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    Organopolysiloxane compositions which can be crosslinked to give elastomers
    12.
    发明授权
    Organopolysiloxane compositions which can be crosslinked to give elastomers 失效
    可以交联以产生弹性体的有机聚硅氧烷组合物

    公开(公告)号：US5705588A

    公开(公告)日：1998-01-06

    申请号：US446741

    申请日：1995-05-31

    Applicant: Gerhard Kreis ,  Michael Stepp ,  Johann Mueller

    Inventor： Gerhard Kreis ,  Michael Stepp ,  Johann Mueller

    IPC: C08L83/08 ,  C08L83/04 ,  C08L83/07 ,  C08G77/08

    CPC classification number: C08L83/04 ,  C08G77/20

    Abstract: New organopolysiloxane masses cross-linkable into elastomers by radical formation containing (1) high-viscosity diorganopolysiloxanes with a value equal to at least 3000 Nm, (2) low-viscosity vinyl-containing organopolysiloxanes having 20 to 1.10.sup.6 mPa.multidot.s at 25.degree. C. consisting of siloxane units (M units) having the formulae R.sup.1 R.sub.2 SiO.sub.1/2 and/or R.sub.3 SiO.sub.1/2, of siloxane units (D units) having the formulae R.sup.1 RSiO and/or R.sub.2 SiO and optionally HRSiO, and of siloxane units (T or Q units) having the formulas RSiO.sub.3/2 and/or R.sub.1 SiO.sub.3/2 and/or SiO.sub.2, in which R stands for a monovalent, possibly substituted hydrocarbon residue with 1 to 18 hydrocarbon atoms and R.sub.1 stands for a vinyl residue, provided that the organopolysiloxanes contain at least 1.0% by weight Si-bound vinyl groups; as well as (3) fillers.

    Abstract translation: PCT No.PCT / EP93 / 03465 Sec。 371日期：1995年5月31日 102（e）日期1995年5月31日PCT提交1993年12月9日PCT公布。 第WO94 / 13741号公报 日期1994年6月23日新的有机聚硅氧烷质量通过自由基形成可交联成弹性体，其含有（1）等于至少3000Nm的高粘度二有机聚硅氧烷，（2）低粘度乙烯基的有机聚硅氧烷，其具有20至1.106mPax， 25℃，具有式R1R2SiO1 / 2和/或R3SiO1 / 2的硅氧烷单元（M单元），具有式R1RSiO和/或R2SiO和任选的HRSiO的硅氧烷单元（D单元）和硅氧烷单元（T 或Q单元），其中R表示具有1至18个烃基的单价可能取代的烃残基，R1表示乙烯基残基，条件是： 有机聚硅氧烷含有至少1.0重量％的Si键合的乙烯基; 以及（3）填料。

    Organopolysiloxanes having bifunctional terminal siloxane units
    13.
    发明授权
    Organopolysiloxanes having bifunctional terminal siloxane units 失效
    具有双官能末端硅氧烷单元的有机聚硅氧烷

    公开(公告)号：US5527935A

    公开(公告)日：1996-06-18

    申请号：US305006

    申请日：1994-09-14

    Applicant: Michael Stepp ,  Peter John

    Inventor： Michael Stepp ,  Peter John

    IPC: B01F17/54 ,  C04B41/49 ,  C08G77/12 ,  C08G77/38 ,  C08G77/50 ,  C10M107/50 ,  D06N3/12 ,  C07F7/08

    CPC classification number: D06N3/128 ,  B01F17/0071 ,  C04B41/4961 ,  C08G77/12 ,  C08G77/38 ,  C08G77/50 ,  C10M107/50 ,  C10M2229/045 ,  C10M2229/046 ,  C10M2229/047 ,  C10M2229/048 ,  C10N2240/08

    Abstract: The present invention relates to the organopolysiloxanes having the formula[R.sup.1 Si(OSiR.sup.2.sub.2 X).sub.2 OSiR.sup.2.sub.2 O.sub.1/2 ].sub.a [R.sub.3 SiO.sub.1/2 ].sub.b [R.sub.2 SiO].sub.c [RSiO.sub.3/2 ].sub.d [SiO.sub.2 ].sub.e (1),whereR is optionally substituted C.sub.1 - to C.sub.18 -hydrocarbon radicals,R.sup.1 is an optionally substituted C.sub.6 - to C.sub.15 -hydrocarbon radical having at least one phenyl ring,R.sup.2 is a C.sub.1 - to C.sub.3 -hydrocarbon radical,X is a hydrogen atom or an organic or organosilicon functional group bonded via a divalent, optionally substituted C.sub.2 - to C.sub.15 -hydrocarbon radical, with one or more methylene units of the hydrocarbon radical being able to be replaced by oxygen atoms bonded on both sides to carbon atoms,a is an integer of at least 1 andb, c, d and e are each 0 or a positive integer, and the sum of a, b, c, d and e is at least 3, and the process for the preparation thereof.

    Abstract translation: 本发明涉及具有式[R1Si（OSiR22X）2OSiR22O1 / 2] a [R3SiO1 / 2] b [R2SiO] c [RSiO3 / 2] d [SiO2] e（1）的有机聚硅氧烷，其中R是任选取代的C1 至C 18烃基，R 1为具有至少一个苯环的任选取代的C 6至C 15 - 烃基，R 2为C 1至C 3烃基，X为氢原子或有机或有机硅官能团键合 通过二价，任选取代的C 2 -C 15烃基与烃基的一个或多个亚甲基能够被两侧键合在碳原子上的氧原子代替，a是至少为1的整数，b ，c，d和e各自为0或正整数，a，b，c，d和e之和为3以上。

    Preparation of polydiorganosiloxanes
    15.
    发明授权
    Preparation of polydiorganosiloxanes 失效
    聚二有机硅氧烷的制备

    公开(公告)号：US06998437B2

    公开(公告)日：2006-02-14

    申请号：US10447731

    申请日：2003-05-29

    Applicant: Michael Stepp ,  Wolfgang Keller

    Inventor： Michael Stepp ,  Wolfgang Keller

    IPC: C08L83/04 ,  C08G77/08

    CPC classification number: C08G77/08

    Abstract: Polydiorganosiloxanes of the general formula R1—(OSiR2)nOH  (I) are prepared by reacting hexaorganocyclotrisiloxanes of the formula (R2SiO)3  (II) with alcohols of the formula R1—OH  (III) where each R is the same or different and is a monovalent, optionally substituted hydrocarbon radical, R1 is a monovalent, optionally substituted hydrocarbon radical and n is an integer of at least 3, in the presence of a carbonate salt as a catalyst.

    Abstract translation: 一般的聚二有机硅氧烷

    Process for the preparation of organopolysiloxanes containing organyloxy groups
    16.
    发明授权
    Process for the preparation of organopolysiloxanes containing organyloxy groups 失效
    制备含有有机氧基的有机聚硅氧烷的方法

    公开(公告)号：US5670597A

    公开(公告)日：1997-09-23

    申请号：US381576

    申请日：1995-01-31

    Applicant: Michael Stepp ,  Stefan Oberneder

    Inventor： Michael Stepp ,  Stefan Oberneder

    IPC: C08G77/08 ,  C08G77/18 ,  C08G77/32

    CPC classification number: C08G77/32 ,  C08G77/08 ,  C08G77/18

    Abstract: A process for the preparation of organopolysiloxanes which contain at least one unit of the formula (R.sup.1 O).sub.3-m R.sub.m SiO.sub.1/2 (I) in which R is identical or different and is a hydrogen atom or monovalent, optionally substituted hydrocarbon radical, R.sup.1 is identical or different and is a monovalent, optionally substituted hydrocarbon radical having 1 to 8 carbon atoms and m is 0, 1 or 2, which comprises, in a 1st step, reacting organosilicon compounds (1) which contain at least one Si-bonded hydroxyl group with at least one silane (2) of the formula (R.sup.1 O).sub.4-m SiR.sub.m (II) and/or partial hydrolysates thereof, in which R, R.sup.1 and m have the above mentioned meaning, in the presence of a fluoride salt (3), and, optionally, in a 2nd step, when the reaction has ended, adding component (4) which can bond fluoride ions.

    Abstract translation: 一种制备有机聚硅氧烷的方法，其含有至少一个式（R1O）3-mRmSiO + E，其中R是相同或不同的氢原子或一价的式（R1O）3-mRmSiO + E， 取代的烃基，R 1相同或不同，为具有1至8个碳原子且m为0,1或2的单价任选取代的烃基，其包括在第一步中使包含在其中的有机硅化合物（1） 在式（R1O）4-mSiRm（II）的至少一种硅烷（2）和/或其部分水解产物中，至少一个Si键合的羟基，其中R，R 1和m具有上述含义， 的氟化物盐（3）和任选的第二步，当反应结束时，加入可以结合氟离子的组分（4）。

    Process for preparing organo(poly)siloxanes
    17.
    发明授权
    Process for preparing organo(poly)siloxanes 失效
    制备有机（多）硅氧烷的方法

    公开(公告)号：US5223595A

    公开(公告)日：1993-06-29

    申请号：US872387

    申请日：1992-04-23

    Applicant: Michael Stepp ,  Johann Muller ,  Silvia Schofberger

    Inventor： Michael Stepp ,  Johann Muller ,  Silvia Schofberger

    IPC: C08G77/06 ,  C08G77/08 ,  C08G77/16 ,  C08G77/20 ,  C08G77/22

    CPC classification number: C08G77/08 ,  C08G77/16 ,  C08G77/20

    Abstract: A process for preparing organo(poly)siloxanes of the formulaR.sup.1 R.sub.2 Si(OSiR.sub.2).sub.m (OSiR.sub.2).sub.n OHwhich comprises reacting a hexaorganocyclotrisiloxane of the formula(R.sub.2 SiO).sub.3with a sil(ox)anol of the formulaR.sup.1 R.sub.2 Si(OSiR.sub.2).sub.m OHin the presence of a catalyst which contains fluoride ions, in which R is the same or different and represents a monovalent, optionally substituted hydrocarbon radical, R.sup.1 represents a hydrogen atom or a monovalent, optionally substituted hydrocarbon radical, m is 0 or an integer of at least 1 and n is an integer of at least 3.An alkali metal fluoride or an alkali metal fluoride bonded to a support material is preferably used as the catalyst in the process of this invention.

    Abstract translation: 制备式R 1 R 2 Si（OSiR 2）m（OSiR 2）n OH的有机（聚）硅氧烷的方法，其包括使式（R 2 SiO）3的六有机基三硅氧烷与式R 1 R 2 Si（OSiR 2）m OH的硅（ox） 存在含有氟离子的催化剂，其中R相同或不同并且表示一价的任选取代的烃基，R 1表示氢原子或一价，任选取代的烃基，m为0或至少为整数 1，n为3以上的整数。作为本发明方法中的催化剂，优选使用与载体材料结合的碱金属氟化物或碱金属氟化物。

    PROCESS FOR PREPARING BIS- AND TRIS(SILYLORGANO)AMINES
    19.
    发明申请
    PROCESS FOR PREPARING BIS- AND TRIS(SILYLORGANO)AMINES 审中-公开
    制备双相和三氯乙烯（SILYLORGANO）胺的方法

    公开(公告)号：US20110282088A1

    公开(公告)日：2011-11-17

    申请号：US13142622

    申请日：2010-01-19

    Applicant: Michael Stepp ,  Markus Jandke

    Inventor： Michael Stepp ,  Markus Jandke

    IPC: C07F7/18

    CPC classification number: C07F7/1804 ,  C07F7/081

    Abstract: The invention provides a process for preparing silylorganoamines of the general formula (1) R′3-nR1nSi—R2—NR3—R4—SiR″3-mR5m (1) by reacting (aminoorganyl)silanes of the general formula (2), H—NR3—R4—SiR″3-mR5m (2) with (haloorganyl)silanes of the general formula (3) R′3-nR1nSi—R2—X (3), where R′, R″, R1, R2, R3, R4, R5, X, m and n are each defined as per claim 1, said reaction comprising the following steps: a) reacting the (haloorganyl)silane of the general formula (3) and the (aminoorganyl)silane of the general formula (2) at a temperature of 0 to 250° C. to form, as well as the silylorganoamine of the general formula (1), the ammonium halide of the (aminoorganyl)silane of the general formula (2) as a by-product, b) adding a base (B), which results in complete or partial ester interchange, in which the (aminoorganyl)silane of the general formula (2) is released again and forms the halide of the base (B), the halide of the base (B) being liquid at temperatures of at most 200° C., and c) removing the liquid halide formed from the base (B).

    Abstract translation: 本发明提供了通式（1）的通式（2）的（氨基有机基）硅烷，H（C 1 -C 6）烷基，C 1 -C 4烷基， （3）R'3-nR1nSi-R2-X（3）的（卤代有机基）硅烷，其中R'，R“，R1，R2，R3（-NR3-R4-SiR”）3-mR5m（2）与通式 所述反应包括以下步骤：a）使通式（3）的（卤代有机基）硅烷与通式（3）所示的（氨基有机基）硅烷反应，其中R 4，R 5，X，m和n各自如权利要求1所定义。 （2）在0-250℃的温度下形成通式（1）的甲硅烷基有机胺，作为副产物的通式（2）的（氨基有机基）硅烷的卤化铵 ，b）加入碱（B），其导致完全或部分酯交换，其中通式（2）的（氨基有机基）硅烷再次被释放并形成碱（B）的卤化物， 基体（B）在回火时呈液态 最高为200℃，c）除去由碱（B）形成的液态卤化物。

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