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1.发明申请公开(公告)号：US20140069301A1
公开(公告)日：2014-03-13
申请号：US14119114
申请日：2012-05-07
IPC分类号： C04B24/42
CPC分类号： C04B24/42 , C04B28/02 , C04B28/14 , C04B41/009 , C04B41/4927 , C04B41/64 , C07F7/08 , C07F7/18 , C04B14/28 , C04B22/064 , C04B24/383 , C04B40/0608
摘要： Solid alkali metal salts of organosilanols and/or their hydrolysis/condensation products are prepared by hydrolysis of organosilanes in water and in the presence of a basic alkali metal salt. The products contain predominately methyl and ethyl organic groups, and C4 or higher hydrocarbon groups as well. The solid salts effectively hydrophobe building materials, while being easily mixed with water.
摘要翻译： 有机硅烷醇和/或其水解/缩合产物的固体碱金属盐通过水中有机硅烷和碱式碱金属盐的存在来制备。 该产品主要含有甲基和乙基有机基团，以及C4或更高级的烃基。 固体盐有效地疏水建筑材料，同时容易与水混合。
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公开(公告)号：US20130145966A1
公开(公告)日：2013-06-13
申请号：US13810676
申请日：2011-07-11
IPC分类号： C07F7/08
CPC分类号： C07F7/0836 , C04B24/42 , C04B2111/00672 , C04B2111/27 , C04B2111/60 , C04B2111/62 , C04B2111/70 , C04B2111/72 , C07F7/1804 , Y10T428/2982
摘要： Organosilanolate powders having a low cation to silicon ratio provide superior hydrophobing ability. The powders may be prepared on an industrial scale by hydrolysis of a silane with a basic salt solution, adding an inert organic solvent, and removing gaseous or alcoholic hydrolysis products by evaporation or distillation, precipitating the organosilanolate as a fine powder.
摘要翻译： 具有低阳离子与硅比的有机硅烷醇钠粉末提供了优异的疏水性能。 粉末可以通过用碱性盐溶液水解硅烷，加入惰性有机溶剂和通过蒸发或蒸馏除去气态或醇水解产物而以工业规模制备，将有机硅烷醇化物作为细粉末沉淀。
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3.发明申请Process For The Continuous Preparation Of Organopolysiloxanes Having Aminoalkyl Groups 有权连续制备具有氨基烷基的有机聚硅氧烷的方法公开(公告)号：US20080275194A1
公开(公告)日：2008-11-06
申请号：US12111293
申请日：2008-04-29
CPC分类号： C07F7/0874 , C08G77/16 , C08G77/388
摘要： Organopolysiloxanes having aminoalkyl groups are prepared by (i) reacting (A) linear, cyclic or branched organopolysiloxanes with (B) aminoalkylsilanes which have an SiC-bonded, basic nitrogen-containing hydrocarbon radical and 2 or 3 hydrolyzable groups, or the partial or complete hydrolysis products thereof, optionally in the presence of (C) basic catalysts and/or (D) chain-terminating reagents, and (ii) optionally, after the reaction (i) neutralizing the optionally used basic catalysts (c), with the proviso that compounds (A), (B) and, when used, (D) are reacted continuously in a reaction space whose ratio of length to diameter is equal to or greater than four.
摘要翻译： 具有氨基烷基的有机聚硅氧烷是通过（i）使（A）线性，环状或支化的有机聚硅氧烷与（B）具有SiC键合的碱性含氮烃基和2或3个可水解基团的氨基烷基硅烷反应制备的，或部分或完全 任选在（C）碱性催化剂和/或（D）链终止试剂存在下的水解产物，和（ii）任选地，在反应（i）中和任选使用的碱性催化剂（c）之后， 化合物（A），（B）和使用时（D）在长度与直径的比等于或大于4的反应空间中连续反应。
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4.发明授权Organosiliconate powders, method for the production thereof and use thereof for hydrophobizing mineral building materials 有权有机硅酸盐粉末，其制造方法和用于疏水化矿物建筑材料的用途公开(公告)号：US08961672B2
公开(公告)日：2015-02-24
申请号：US14119114
申请日：2012-05-07
CPC分类号： C04B24/42 , C04B28/02 , C04B28/14 , C04B41/009 , C04B41/4927 , C04B41/64 , C07F7/08 , C07F7/18 , C04B14/28 , C04B22/064 , C04B24/383 , C04B40/0608
摘要： Solid alkali metal salts of organosilanols and/or their hydrolysis/condensation products are prepared by hydrolysis of organosilanes in water and in the presence of a basic alkali metal salt. The products contain predominately methyl and ethyl organic groups, and C4 or higher hydrocarbon groups as well. The solid salts effectively hydrophobe building materials, while being easily mixed with water.
摘要翻译： 有机硅烷醇和/或其水解/缩合产物的固体碱金属盐通过水中有机硅烷和碱式碱金属盐的存在来制备。 该产品主要含有甲基和乙基有机基团，以及C4或更高级的烃基。 固体盐有效地疏水建筑材料，同时容易与水混合。
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公开(公告)号：US20090209743A1
公开(公告)日：2009-08-20
申请号：US12304841
申请日：2007-06-06
IPC分类号： C09B29/36 , C07D251/52
CPC分类号： C08G77/388 , A61K8/898 , A61K2800/42 , A61Q19/00 , C08G77/392 , C08G77/395 , C09B57/02 , C09B69/008 , C09B69/101 , C09B69/106 , C09B69/109 , C09D5/1675 , C09G1/16 , C14C11/003 , D06M15/643 , D06P1/0036 , D06P1/0052 , D06P1/0056 , D06P1/5292 , G03G9/08773 , G03G9/08795 , G03G9/09 , G03G9/0924
摘要： The present invention relates to colored organopolysiloxanes comprising units of the formula R1a(RO)bAcR2dSiO(4-a-b-c-d)/2 (I), in which R can be identical or different and is hydrogen or a monovalent, unsubstituted or substituted hydrocarbon radical; R1 can be identical or different and is hydrogen or a monovalent, SiC-bonded, unsubstituted or substituted hydrocarbon radical; R2 can be identical or different and is a substituted monovalent hydrocarbon radical; A can be identical or different and is an organic dye radical free from sulfonic acid groups and sulfonate groups; a is 0, 1, 2 or 3; b is 0, 1, 2 or 3; d is 0, 1, 2 or 3; and c is 0, 1 or 2; with the proviso that the sum a+b+c+d is ≦3, the organopolysiloxane has at least one radical A per molecule, and in the units of the formula (I) where c is other than 0 when d is 0. The invention also relates to a process to the color organopolysiloxane.
摘要翻译： 本发明涉及包含下式的单元的有色有机聚硅氧烷：式中：α-in-line-formula description =“In-line formula”end =“lead”→> R1a（RO）bAcR2dSiO（4-abcd）/ 2（I） 其中R可以相同或不同，为氢或一价，未取代或取代的烃基的“？”in-line-formula description =“In-line Formulas”end =“tail”？ R 1可以相同或不同，为氢或一价，SiC键合的未取代或取代的烃基; R2可以相同或不同，并且是取代的单价烃基; A可以相同或不同，是不含磺酸基和磺酸基的有机染料基团; a是0,1,2或3; b为0,1,2或3; d为0,1,2或3; 且c为0,1或2; 条件是总和a + b + c + d为<= 3，有机聚硅氧烷每分子具有至少一个基团A，并且在式（I）的单元中，当d为0时，c不为0。 本发明还涉及彩色有机聚硅氧烷的方法。
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6.发明申请Multistage Process for Preparing Organopolysiloxanes Comprising Aminoalkyl Groups 有权用于制备包含氨基烷基的有机聚硅氧烷的多级方法公开(公告)号：US20090036618A1
公开(公告)日：2009-02-05
申请号：US12180728
申请日：2008-10-06
IPC分类号： C08F2/01
CPC分类号： C08G77/388
摘要： Organopolysiloxanes having aminoalkyl groups are prepared by(i) reacting(A) linear, cyclic or branched organopolysiloxanes with(B) aminoalkyl silanes having an SiC-bonded hydrocarbon radical comprising basic nitrogen and 2 or 3 hydrolyzable groups, or partial or full hydrolyzates thereof, in the presence of(C) basic catalysts and optionally(D) chain-terminating reagents, at a temperature of at least 60° C., then, after the reaction (i),(ii) deactivating the catalysts (C) and(iii) cooling the product to a temperature below 60° C. before, during or after the deactivation (ii) of the catalysts, with the proviso that the process is performed in at least two successive stirred tanks, the reaction (i) and the cooling (iii) proceeding separately in different stirred tanks.
摘要翻译： 具有氨基烷基的有机聚硅氧烷是通过（i）使（A）线性，环状或支化的有机聚硅氧烷与（B）具有包含碱性氮和2或3个可水解基团的SiC键合的烃基的氨基烷基硅烷或其部分或全部水解产物反应而制备的， 在（C）碱性催化剂和任选的（D）链终止试剂的存在下，在至少60℃的温度下，然后在反应（i）之后，（ii）使催化剂（C）和（ iii）在催化剂失活（ii）之前，期间或之后将产物冷却到低于60℃的温度，条件是该方法在至少两个连续的搅拌釜中进行，反应（i）和 冷却（iii）分别在不同的搅拌釜中进行。
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公开(公告)号：US08748645B2
公开(公告)日：2014-06-10
申请号：US13810676
申请日：2011-07-11
IPC分类号： C07F7/02
CPC分类号： C07F7/0836 , C04B24/42 , C04B2111/00672 , C04B2111/27 , C04B2111/60 , C04B2111/62 , C04B2111/70 , C04B2111/72 , C07F7/1804 , Y10T428/2982
摘要： Organosilanolate powders having a low cation to silicon ratio provide superior hydrophobing ability. The powders may be prepared on an industrial scale by hydrolysis of a silane with a basic salt solution, adding an inert organic solvent, and removing gaseous or alcoholic hydrolysis products by evaporation or distillation, precipitating the organosilanolate as a fine powder.
摘要翻译： 具有低阳离子与硅比的有机硅烷醇钠粉末提供了优异的疏水性能。 粉末可以通过用碱性盐溶液水解硅烷，加入惰性有机溶剂和通过蒸发或蒸馏除去气态或醇水解产物而以工业规模制备，将有机硅烷醇化物作为细粉末沉淀。
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公开(公告)号：US20120238671A1
公开(公告)日：2012-09-20
申请号：US13514027
申请日：2010-11-26
CPC分类号： C08J3/03 , C04B24/42 , C04B28/14 , C04B2111/27 , C08G77/06 , C08G77/12 , C08G77/18 , C08J2383/04 , C08J2383/12 , C08L83/04 , C08L83/00
摘要： Silicone resin emulsions especially suitable for hydrophobing gypsum compositions together with H-siloxanes are prepared by hydrolysis and subsequent distillation to an alcohol content of less than 0.1 weight percent. Use of the emulsion with H-siloxanes provides plaster products such as plasterboard of increased hydrophobicity.
摘要翻译： 通过水解并随后蒸馏至小于0.1重量％的醇含量，制备特别适用于疏水石膏组合物与H-硅氧烷的硅树脂乳液。 乳液与H-硅氧烷的使用提供了石膏产品，例如增加疏水性的石膏板。
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9.发明授权Process for the continuous preparation of organopolysiloxanes having aminoalkyl groups 有权连续制备具有氨基烷基的有机聚硅氧烷的方法公开(公告)号：US07939618B2
公开(公告)日：2011-05-10
申请号：US12111293
申请日：2008-04-29
IPC分类号： C08G77/26
CPC分类号： C07F7/0874 , C08G77/16 , C08G77/388
摘要： Organopolysiloxanes having aminoalkyl groups are prepared by (i) reacting (A) linear, cyclic or branched organopolysiloxanes with (B) aminoalkylsilanes which have an SiC-bonded, basic nitrogen-containing hydrocarbon radical and 2 or 3 hydrolyzable groups, or the partial or complete hydrolysis products thereof, optionally in the presence of (C) basic catalysts and/or (D) chain-terminating reagents, and (ii) optionally, after the reaction (i) neutralizing the optionally used basic catalysts (c), with the proviso that compounds (A), (B) and, when used, (D) are reacted continuously in a reaction space whose ratio of length to diameter is equal to or greater than four.
摘要翻译： 具有氨基烷基的有机聚硅氧烷是通过（i）使（A）线性，环状或支化的有机聚硅氧烷与（B）具有SiC键合的碱性含氮烃基和2或3个可水解基团的氨基烷基硅烷反应制备的，或部分或完全 任选在（C）碱性催化剂和/或（D）链终止试剂存在下的水解产物，和（ii）任选地，在反应（i）中和任选使用的碱性催化剂（c）之后， 化合物（A），（B）和使用时（D）在长度与直径的比等于或大于4的反应空间中连续反应。
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10.发明授权Multistage process for preparing organopolysiloxanes comprising aminoalkyl groups 有权用于制备包含氨基烷基的有机聚硅氧烷的多级方法公开(公告)号：US07759446B2
公开(公告)日：2010-07-20
申请号：US12180728
申请日：2008-07-28
CPC分类号： C08G77/388
摘要： Organopolysiloxanes having aminoalkyl groups are prepared by (i) reacting (A) linear, cyclic or branched organopolysiloxanes with (B) aminoalkyl silanes having an SiC-bonded hydrocarbon radical comprising basic nitrogen and 2 or 3 hydrolyzable groups, or partial or full hydrolyzates thereof, in the presence of (C) basic catalysts and optionally (D) chain-terminating reagents, at a temperature of at least 60° C., then, after the reaction (i), (ii) deactivating the catalysts (C) and (iii) cooling the product to a temperature below 60° C. before, during or after the deactivation (ii) of the catalysts, with the proviso that the process is performed in at least two successive stirred tanks, the reaction (i) and the cooling (iii) proceeding separately in different stirred tanks.
摘要翻译： 具有氨基烷基的有机聚硅氧烷是通过（i）使（A）线性，环状或支化的有机聚硅氧烷与（B）具有包含碱性氮和2或3个可水解基团的SiC键合的烃基的氨基烷基硅烷或其部分或全部水解产物反应而制备的， 在（C）碱性催化剂和任选的（D）链终止试剂的存在下，在至少60℃的温度下，然后在反应（i）之后，（ii）使催化剂（C）和（ iii）在催化剂失活（ii）之前，期间或之后将产物冷却到低于60℃的温度，条件是该方法在至少两个连续的搅拌釜中进行，反应（i）和 冷却（iii）分别在不同的搅拌釜中进行。
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