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公开(公告)号：US06982126B2
公开(公告)日：2006-01-03
申请号：US10707197
申请日：2003-11-26
申请人： Ramgopal Darolia , Irene Spitsberg , Brett Allen Rohrer Boutwell , Mark Daniel Gorman , Curtis Alan Johnson , Venkat Subramaniam Venkataramani
发明人： Ramgopal Darolia , Irene Spitsberg , Brett Allen Rohrer Boutwell , Mark Daniel Gorman , Curtis Alan Johnson , Venkat Subramaniam Venkataramani
CPC分类号： C23C28/3215 , C23C14/08 , C23C14/083 , C23C28/321 , C23C28/345 , C23C28/3455 , F01D5/288 , F05D2230/90 , F05D2300/611 , Y02T50/67 , Y02T50/671 , Y10T428/12611 , Y10T428/12618 , Y10T428/24355 , Y10T428/24413
摘要： A thermal barrier coating (TBC) for a component intended for use in a hostile thermal environment. The TBC has an interior region and an outer surface region on and contacting the interior region. Both regions are formed of a ceramic material, with the interior region having a lower thermal conductivity than zirconia partially stabilized by about seven weight percent yttria. The interior region constitutes more than half of the thickness of the TBC, and the outer surface region constitutes less than half of the thickness of the TBC. The TBC has a columnar microstructure whereby the interior region and the outer surface region comprise columns of their ceramic materials. The outer surface region is more erosion and impact resistant than the interior region at least in part as a result of the columns thereof being more closely spaced than the columns of the interior region.
摘要翻译： 用于在恶劣热环境中使用的组件的热障涂层（TBC）。 TBC具有内部区域和外部表面区域，并且与内部区域接触。 两个区域由陶瓷材料形成，其内部区域具有比部分稳定约7重量％氧化钇的氧化锆更低的热导率。 内部区域构成TBC厚度的一半以上，外表面区域构成TBC厚度的一半以下。 TBC具有柱状微结构，其中内部区域和外部表面区域包括其陶瓷材料的列。 由于其柱与内部区域的列更紧密地间隔，至少部分地，外表面区域比内部区域具有更多的侵蚀和抗冲击性。
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公开(公告)号：US08084094B2
公开(公告)日：2011-12-27
申请号：US12465884
申请日：2009-05-14
IPC分类号： B05D3/04
CPC分类号： C23C10/02 , C23C10/48 , C23C10/50 , Y10T428/12458 , Y10T428/12736 , Y10T428/1275 , Y10T428/12861 , Y10T428/12875 , Y10T428/12944 , Y10T428/26 , Y10T428/265
摘要： A coating process for an article having a substrate formed of a metal alloy that is prone to the formation of a secondary reaction zone (SRZ). The coating process forms a coating system that includes an aluminum-containing overlay coating and a stabilizing layer between the overlay coating and the substrate. The overlay coating contains aluminum in an amount greater by atomic percent than the metal alloy of the substrate, such that there is a tendency for aluminum to diffuse from the overlay coating into the substrate. The stabilizing layer is predominantly or entirely formed of at least one platinum group metal (PGM), namely, platinum, rhodium, iridium, and/or palladium. The stabilizing layer is sufficient to inhibit diffusion of aluminum from the overlay coating into the substrate so that the substrate remains essentially free of an SRZ that would be deleterious to the mechanical properties of the alloy.
摘要翻译： 一种具有由容易形成二次反应区（SRZ）的金属合金形成的基材的制品的涂布方法。 涂覆工艺形成涂层系统，其包括含铝覆盖涂层和覆盖涂层与基底之间的稳定层。 覆盖涂层含有比基底的金属合金更大原子百分数的铝，使得铝从覆盖涂层扩散到基底中的倾向。 稳定层主要或完全由至少一种铂族金属（PGM），即铂，铑，铱和/或钯形成。 稳定层足以抑制铝从覆盖涂层扩散到衬底中，使得衬底基本上不含对合金的机械性能有害的SRZ。
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13.发明申请ARTICLE PROTECTED BY A THERMAL BARRIER COATING HAVING A GROUP 2 OR 3/GROUP 5 STABILIZATION-COMPOSITION-ENRICHED SURFACE 审中-公开具有2组或3组/ 5组稳定表面的热障涂层保护的物品公开(公告)号：US20100291302A1
公开(公告)日：2010-11-18
申请号：US11684981
申请日：2007-03-12
申请人： John Frederick Ackerman , Venkat Subramanian Venkataramani , Irene T. Spitsberg , Brett Allen Rohrer Boutwell , Ramgopal Darolia
发明人： John Frederick Ackerman , Venkat Subramanian Venkataramani , Irene T. Spitsberg , Brett Allen Rohrer Boutwell , Ramgopal Darolia
IPC分类号： B05D3/10
CPC分类号： C23C28/3215 , C23C28/321 , C23C28/325 , C23C28/345 , C23C28/3455
摘要： A protected article is prepared by providing the article, depositing a bond coat onto an exposed surface of the article, and producing a thermal barrier coating on an exposed surface of the bond coat. The step of producing the thermal barrier coating includes the steps of depositing a primary ceramic coating onto an exposed surface of the bond coat, and depositing a stabilization composition onto an exposed surface of the primary ceramic coating. The stabilization composition includes a first element selected from Group 2 or Group 3 of the periodic table, and a second element selected from Group 5 of the periodic table. The atomic ratio of the amount of the first element to the amount of the second element is at least 1.3, more preferably at least 1:1.
摘要翻译： 通过提供制品来制备受保护制品，将粘合涂层沉积在制品的暴露表面上，并在粘合涂层的暴露表面上产生热障涂层。 生产热障涂层的步骤包括以下步骤：将初级陶瓷涂层沉积在粘合涂层的暴露表面上，并将稳定化组合物沉积到初级陶瓷涂层的暴露表面上。 稳定化组合物包括选自元素周期表第2族或第3族的第一元素和选自元素周期表第5族的第二元素。 第一元素的量与第二元素的量的原子比为至少1.3，更优选至少1:1。
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公开(公告)号：US20090220684A1
公开(公告)日：2009-09-03
申请号：US12465884
申请日：2009-05-14
IPC分类号： B05D5/12
CPC分类号： C23C10/02 , C23C10/48 , C23C10/50 , Y10T428/12458 , Y10T428/12736 , Y10T428/1275 , Y10T428/12861 , Y10T428/12875 , Y10T428/12944 , Y10T428/26 , Y10T428/265
摘要： A coating process for an article having a substrate formed of a metal alloy that is prone to the formation of a secondary reaction zone (SRZ). The coating process forms a coating system that includes an aluminum-containing overlay coating and a stabilizing layer between the overlay coating and the substrate. The overlay coating contains aluminum in an amount greater by atomic percent than the metal alloy of the substrate, such that there is a tendency for aluminum to diffuse from the overlay coating into the substrate. The stabilizing layer is predominantly or entirely formed of at least one platinum group metal (PGM), namely, platinum, rhodium, iridium, and/or palladium. The stabilizing layer is sufficient to inhibit diffusion of aluminum from the overlay coating into the substrate so that the substrate remains essentially free of an SRZ that would be deleterious to the mechanical properties of the alloy.
摘要翻译： 一种具有由容易形成二次反应区（SRZ）的金属合金形成的基材的制品的涂布方法。 涂覆工艺形成涂层系统，其包括含铝覆盖涂层和覆盖涂层与基底之间的稳定层。 覆盖涂层含有比基底的金属合金更大原子百分数的铝，使得铝从覆盖涂层扩散到基底中的倾向。 稳定层主要或完全由至少一种铂族金属（PGM），即铂，铑，铱和/或钯形成。 稳定层足以抑制铝从覆盖涂层扩散到衬底中，使得衬底基本上不含对合金的机械性能有害的SRZ。
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15.发明申请NI-BASE SUPERALLOY HAVING A COATING SYSTEM CONTAINING A STABILIZING LAYER 失效具有稳定层的涂层体系的NI-BASE SUPERALLOY公开(公告)号：US20080131720A1
公开(公告)日：2008-06-05
申请号：US11565410
申请日：2006-11-30
CPC分类号： C23C10/02 , C23C10/48 , C23C10/50 , Y10T428/12458 , Y10T428/12736 , Y10T428/1275 , Y10T428/12861 , Y10T428/12875 , Y10T428/12944 , Y10T428/26 , Y10T428/265
摘要： A coating process and system for an article having a substrate formed of a metal alloy that is prone to the formation of a secondary reaction zone (SRZ). The coating system includes an aluminum-containing overlay coating and a stabilizing layer between the overlay coating and the substrate. The overlay coating contains aluminum in an amount greater by atomic percent than the metal alloy of the substrate, such that there is a tendency for aluminum to diffuse from the overlay coating into the substrate. The stabilizing layer is predominantly or entirely formed of at least one platinum group metal (PGM), namely, platinum, rhodium, iridium, and/or palladium. The stabilizing layer is sufficient to inhibit diffusion of aluminum from the overlay coating into the substrate so that the substrate remains essentially free of an SRZ that would be deleterious to the mechanical properties of the alloy.
摘要翻译： 一种用于具有易于形成二次反应区（SRZ）的由金属合金形成的基底的制品的涂覆方法和系统。 涂层系统包括含铝覆盖涂层和覆盖涂层与基底之间的稳定层。 覆盖涂层含有比基底的金属合金更大原子百分数的铝，使得铝从覆盖涂层扩散到基底中的倾向。 稳定层主要或完全由至少一种铂族金属（PGM），即铂，铑，铱和/或钯形成。 稳定层足以抑制铝从覆盖涂层扩散到衬底中，使得衬底基本上不含对合金的机械性能有害的SRZ。
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公开(公告)号：US07357958B2
公开(公告)日：2008-04-15
申请号：US10904221
申请日：2004-10-29
IPC分类号： C23C16/00
CPC分类号： C23C14/5806 , C23C14/025 , C23C14/16 , F01D5/288 , F05D2230/90 , F05D2300/611
摘要： Methods for depositing an overlay coating on articles intended for use in hostile thermal environments. The coating has a predominantly gamma prime-phase nickel aluminide (Ni3Al) composition suitable for use as an environmental coating and as a bond coat of a thermal barrier coating system. The coating further contains at least one platinum group metal, preferably chromium, optionally one or more reactive elements, and optionally silicon. The coating is deposited by a process that entails forming a platinum group metal layer and at least one separate layer of other constituents of the coating, and then performing a diffusion heat treatment to yield the coating.
摘要翻译： 将覆盖涂层沉积在旨在用于恶劣热环境的物品上的方法。 该涂层主要具有适合用作环境涂层和作为热障涂层系统的粘结层的γ初始相铝酸镍（Ni 3 Al 3 Al）组合物。 涂层还包含至少一种铂族金属，优选铬，任选的一种或多种反应性元素，以及任选的硅。 涂层通过需要形成铂族金属层和至少一层分开的涂层其它成分的方法沉积，然后进行扩散热处理以产生涂层。
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17.发明授权公开(公告)号：US07318955B2
公开(公告)日：2008-01-15
申请号：US10711364
申请日：2004-09-14
申请人： Ramgopal Darolia , Brett Allen Rohrer Boutwell , Brian Thomas Hazel , Bangalore Aswatha Nagaraj , Joseph David Rigney , Roger D. Wustman
发明人： Ramgopal Darolia , Brett Allen Rohrer Boutwell , Brian Thomas Hazel , Bangalore Aswatha Nagaraj , Joseph David Rigney , Roger D. Wustman
IPC分类号： B32B9/00
CPC分类号： C23C14/226 , C23C14/22 , C23C14/505 , C23C28/321 , C23C28/3215 , C23C28/345 , C23C28/3455 , C23C28/42 , F01D5/288 , F05D2230/90 , F05D2300/611 , Y10T428/24355 , Y10T428/24413
摘要： Thermal barrier coating (TBC) and a method of depositing a TBC having a modulated columnar microstructure that exhibits increased impact resistance. The TBC is deposited to have a columnar microstructure in which columns extend from a substrate surface. The columns having inner regions contacting the surface, outer regions near an outermost surface of the TBC, and interior regions therebetween. The inner regions of the columns are substantially normal to the substrate surface and at least one of the interior and outer regions of the columns are nonaligned with its respective inner regions, so that the columns of the columnar microstructure are continuous but modulated between the inner and outer regions to reduce tensile stresses within the columns resulting from particle impact.
摘要翻译： 热屏蔽涂层（TBC）和沉积具有显示出增加的耐冲击性的调制柱状微结构的TBC的方法。 沉积TBC以具有柱状微结构，其中柱从衬底表面延伸。 具有接触表面的内部区域，靠近TBC的最外表面的外部区域以及它们之间的内部区域的列。 柱的内部区域基本上垂直于基底表面，并且柱的内部和外部区域中的至少一个与其相应的内部区域不对齐，使得柱状微结构的列是连续的但是在内部和/ 外部区域以减少由于颗粒撞击引起的柱内的拉伸应力。
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公开(公告)号：US07247393B2
公开(公告)日：2007-07-24
申请号：US11162839
申请日：2005-09-26
CPC分类号： C23C30/00 , Y10T428/12458 , Y10T428/12736 , Y10T428/1275 , Y10T428/12875 , Y10T428/12937 , Y10T428/12944
摘要： An intermetallic composition suitable for use as an environmentally-protective coating on surfaces of components used in hostile thermal environments, including the turbine, combustor and augmentor sections of a gas turbine engine. The coating contains the gamma-prime (Ni3Al) nickel aluminide intermetallic phase and either the beta (NiAl) nickel aluminide intermetallic phase or the gamma solid solution phase. The coating has an average aluminum content of 14 to 30 atomic percent and an average platinum-group metal content of at least 1 to less than 10 atomic percent, the balance of the coating being nickel, one or more of chromium, silicon, tantalum, and cobalt, optionally one or more of hafnium, yttrium, zirconium, lanthanum, and cerium, and incidental impurities.
摘要翻译： 适用于在敌对热环境中使用的组件的表面上用作环境保护涂层的金属间组合物，包括燃气涡轮发动机的涡轮机，燃烧器和增压器部分。 该涂层含有γ-prime（Ni 3 Al 3）铝铝化物金属间相和β（NiAl）镍铝化物金属间相或γ固溶体相。 该涂层的平均铝含量为14〜30原子％，平均铂族金属含量为1〜10原子％以下，镀层为镍，铬，硅，钽， 和钴，任选地一种或多种铪，钇，锆，镧和铈以及附带的杂质。
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19.发明授权公开(公告)号：US07544424B2
公开(公告)日：2009-06-09
申请号：US11565410
申请日：2006-11-30
IPC分类号： B32B15/04
CPC分类号： C23C10/02 , C23C10/48 , C23C10/50 , Y10T428/12458 , Y10T428/12736 , Y10T428/1275 , Y10T428/12861 , Y10T428/12875 , Y10T428/12944 , Y10T428/26 , Y10T428/265
摘要： A coating process and system for an article having a substrate formed of a metal alloy that is prone to the formation of a secondary reaction zone (SRZ). The coating system includes an aluminum-containing overlay coating and a stabilizing layer between the overlay coating and the substrate. The overlay coating contains aluminum in an amount greater by atomic percent than the metal alloy of the substrate, such that there is a tendency for aluminum to diffuse from the overlay coating into the substrate. The stabilizing layer is predominantly or entirely formed of at least one platinum group metal (PGM), namely, platinum, rhodium, iridium, and/or palladium. The stabilizing layer is sufficient to inhibit diffusion of aluminum from the overlay coating into the substrate so that the substrate remains essentially free of an SRZ that would be deleterious to the mechanical properties of the alloy.
摘要翻译： 一种用于具有易于形成二次反应区（SRZ）的由金属合金形成的基底的制品的涂覆方法和系统。 涂层系统包括含铝覆盖涂层和覆盖涂层与基底之间的稳定层。 覆盖涂层含有比基底的金属合金更大原子百分数的铝，使得铝从覆盖涂层扩散到基底中的倾向。 稳定层主要或完全由至少一种铂族金属（PGM），即铂，铑，铱和/或钯形成。 稳定层足以抑制铝从覆盖涂层扩散到衬底中，使得衬底基本上不含对合金的机械性能有害的SRZ。
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公开(公告)号：US07250225B2
公开(公告)日：2007-07-31
申请号：US11162838
申请日：2005-09-26
CPC分类号： C23C30/00 , Y10T428/12458 , Y10T428/12736 , Y10T428/1275 , Y10T428/12875 , Y10T428/12937 , Y10T428/12944
摘要： An intermetallic composition suitable for use as an environmentally-protective coating on surfaces of components used in hostile thermal environments, including the turbine, combustor and augmentor sections of a gas turbine engine. The coating contains the gamma-prime (Ni3Al) nickel aluminide intermetallic phase and either the beta (NiAl) nickel aluminide intermetallic phase or the gamma solid solution phase. The coating has an average aluminum content of 14 to 30 atomic percent and an average platinum-group metal content of at least 1 to less than 10 atomic percent, the balance of the coating being nickel, incidental impurities, and optionally hafnium.
摘要翻译： 适用于在敌对热环境中使用的组件的表面上用作环境保护涂层的金属间组合物，包括燃气涡轮发动机的涡轮机，燃烧器和增压器部分。 该涂层含有γ-prime（Ni 3 Al 3）铝铝化物金属间相和β（NiAl）镍铝化物金属间相或γ固溶体相。 该涂层的平均铝含量为14〜30原子％，平均铂族金属含量为1〜10原子％以下，镀层为镍，附带杂质，可选地为铪。
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