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公开(公告)号：US07226530B2
公开(公告)日：2007-06-05
申请号：US10735078
申请日：2003-12-11
IPC分类号： G01N27/04
CPC分类号： G01N27/127 , G01N27/126 , Y10S977/953 , Y10S977/957
摘要： Polymer nanofibers, such as polyaniline nanofibers, with uniform diameters less than 500 nm can be made in bulk quantities through a facile aqueous and organic interfacial polymerization method at ambient conditions. The nanofibers have lengths varying from 500 nm to 10 μm and form interconnected networks in a thin film. Thin film nanofiber sensors can be made of the polyaniline nanofibers having superior performance in both sensitivity and time response to a variety of gas vapors including, acids, bases, redox active vapors, alcohols and volatile organic chemicals.
摘要翻译： 具有均匀直径小于500nm的聚苯胺纳米纤维的聚合物纳米纤维可以通过在环境条件下的容易的水和有机界面聚合方法以大量方式制备。 纳米纤维具有从500nm到10um的长度，并且在薄膜中形成互连的网络。 薄膜纳米纤维传感器可以由聚苯胺纳米纤维制成，其对包括酸，碱，氧化还原活性蒸气，醇和挥发性有机化学品的各种气体蒸气的灵敏度和时间响应都具有优异的性能。
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12.发明授权公开(公告)号：US09118078B2
公开(公告)日：2015-08-25
申请号：US12661688
申请日：2010-03-22
申请人： Jiaxing Huang , Laura J. Cote , Franklin J. Kim
发明人： Jiaxing Huang , Laura J. Cote , Franklin J. Kim
CPC分类号： H01M4/663 , C01B32/182 , H01M4/667 , Y10T428/31504
摘要： A method for forming a film of graphite oxide single layers. In one embodiment, the method includes the steps of preparing a solution of graphite oxide to allow a plurality of graphite oxide single layers to be formed and dispersed in the solution; and applying the solution of graphite oxide onto an air-water interface of water to form a film at the air-water interface, wherein the film comprises a plurality of graphite oxide single layers and is characterized by a packing density, wherein the film of graphite oxide single layers is formed with no presence of a surfactant or stabilizing agent.
摘要翻译： 一种形成单层氧化石墨膜的方法。 在一个实施方案中，该方法包括制备石墨氧化物溶液以允许多个氧化石墨单层形成并分散在溶液中的步骤; 并将氧化石墨溶液施加到水的空气 - 水界面上以在空气 - 水界面处形成膜，其中所述膜包括多个氧化石墨单层，其特征在于填充密度，其中所述石墨膜 在不存在表面活性剂或稳定剂的情况下形成氧化物单层。
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13.发明申请METHODS OF FLASH REDUCTION AND PATTERNING OF GRAPHITE OXIDE AND ITS POLYMER COMPOSITES 有权石墨氧化物及其聚合物复合材料的闪光减少和图案化方法公开(公告)号：US20100221508A1
公开(公告)日：2010-09-02
申请号：US12714955
申请日：2010-03-01
申请人： Jiaxing Huang , Laura Cote , Rodolfo Cruz Silva
发明人： Jiaxing Huang , Laura Cote , Rodolfo Cruz Silva
CPC分类号： C01B31/0476 , B82Y30/00 , B82Y40/00 , C01B32/192 , G03F7/0042 , G03F7/2004 , H01B1/04 , H01B1/24 , Y10T428/24802
摘要： A method of reducing a film of graphite oxide. In one embodiment, the method includes the steps of providing a film of graphite oxide with a thickness d0; and delivering optical energy in a single pulse to the film of graphite oxide at a distance no more than 1.0 cm away from the film of graphite oxide to reduce the film of graphite oxide to a film of graphene with a thickness d, wherein the optical energy has a radiant exposure in the range of between 0.1 and 2 J/cm2, and wherein the thickness d is greater than the thickness d0. In one embodiment, the thickness d≧10×d0.
摘要翻译： 一种还原氧化石墨膜的方法。 在一个实施方案中，该方法包括以下步骤：提供具有厚度d0的氧化石墨膜; 并以单脉冲将光能传递到离石墨氧化物膜不超过1.0cm距离的石墨氧化物膜上，以将氧化石墨膜降低至具有厚度d的石墨烯膜，其中光能 具有在0.1至2J / cm 2范围内的辐射曝光，并且其中厚度d大于厚度d0。 在一个实施例中，厚度d≥10×d0。
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14.发明申请High-Throughput Imaging of Graphene Based Sheets by Fluorescence Quenching Microscopy and Applications of Same 有权通过荧光猝灭显微镜及其应用的石墨烯基片材的高通量成像公开(公告)号：US20110076467A1
公开(公告)日：2011-03-31
申请号：US12893470
申请日：2010-09-29
申请人： Jiaxing Huang , Jaemyung Kim , Laura J. Cote , Franklin J. Kim
发明人： Jiaxing Huang , Jaemyung Kim , Laura J. Cote , Franklin J. Kim
CPC分类号： G01N21/6458 , Y10T428/24802
摘要： A method for imaging a graphene-based film. In one embodiment, the method includes the steps of providing a graphene-based film on a surface of a medium; forming a fluorescent coating over the graphene-based film to form a sample; illuminating the sample with light of a specific wavelength or wavelengths, which is absorbed by the fluorescent coating to cause the fluorescent coating to emit light of wavelengths longer than that of the absorbed light, which is quenched by the graphene-based film such that a visibility contrast is formed between the graphene-based film and the fluorescent coating; and imaging the graphene-based film from the visibility contrast.
摘要翻译： 一种用于成像基于石墨烯的膜的方法。 在一个实施方案中，该方法包括以下步骤：在介质的表面上提供基于石墨烯的膜; 在石墨烯基膜上形成荧光涂层以形成样品; 用由荧光涂层吸收的特定波长或波长的光照射样品，以使荧光涂层发射比被吸收的光长的波长的光，其被基于石墨烯的膜骤冷，使得可见度 在石墨烯基膜和荧光涂层之间形成对比度; 并从可见度对比度对石墨烯膜进行成像。
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15.发明授权Methods of flash reduction and patterning of graphite oxide and its polymer composites 有权石墨氧化物及其聚合物复合材料的闪光还原和图案化方法公开(公告)号：US08968525B2
公开(公告)日：2015-03-03
申请号：US12714955
申请日：2010-03-01
申请人： Jiaxing Huang , Laura Cote , Rodolfo Cruz Silva
发明人： Jiaxing Huang , Laura Cote , Rodolfo Cruz Silva
CPC分类号： C01B31/0476 , B82Y30/00 , B82Y40/00 , C01B32/192 , G03F7/0042 , G03F7/2004 , H01B1/04 , H01B1/24 , Y10T428/24802
摘要： A method of reducing a film of graphite oxide. In one embodiment, the method includes the steps of providing a film of graphite oxide with a thickness d0; and delivering optical energy in a single pulse to the film of graphite oxide at a distance no more than 1.0 cm away from the film of graphite oxide to reduce the film of graphite oxide to a film of graphene with a thickness d, wherein the optical energy has a radiant exposure in the range of between 0.1 and 2 J/cm2, and wherein the thickness d is greater than the thickness d0. In one embodiment, the thickness d≧10×d0.
摘要翻译： 一种还原氧化石墨膜的方法。 在一个实施方案中，该方法包括以下步骤：提供具有厚度d0的氧化石墨膜; 并以单脉冲将光能传递到离石墨氧化物膜不超过1.0cm距离的石墨氧化物膜上，以将氧化石墨膜降低至具有厚度d的石墨烯膜，其中光能 具有在0.1至2J / cm 2范围内的辐射曝光，并且其中厚度d大于厚度d0。 在一个实施例中，厚度d≥10×d0。
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16.发明授权High-throughput imaging of graphene based sheets by fluorescence quenching microscopy and applications of same 有权通过荧光淬灭显微镜及其应用的石墨烯基片材的高通量成像公开(公告)号：US08426120B2
公开(公告)日：2013-04-23
申请号：US12893470
申请日：2010-09-29
申请人： Jiaxing Huang , Jaemyung Kim , Laura J. Cote , Franklin J. Kim
发明人： Jiaxing Huang , Jaemyung Kim , Laura J. Cote , Franklin J. Kim
IPC分类号： G03F7/20
CPC分类号： G01N21/6458 , Y10T428/24802
摘要： A method for imaging a graphene-based film. In one embodiment, the method includes the steps of providing a graphene-based film on a surface of a medium; forming a fluorescent coating over the graphene-based film to form a sample; illuminating the sample with light of a specific wavelength or wavelengths, which is absorbed by the fluorescent coating to cause the fluorescent coating to emit light of wavelengths longer than that of the absorbed light, which is quenched by the graphene-based film such that a visibility contrast is formed between the graphene-based film and the fluorescent coating; and imaging the graphene-based film from the visibility contrast.
摘要翻译： 一种用于成像基于石墨烯的膜的方法。 在一个实施方案中，该方法包括以下步骤：在介质的表面上提供基于石墨烯的膜; 在石墨烯基膜上形成荧光涂层以形成样品; 用由荧光涂层吸收的特定波长或波长的光照射样品，以使荧光涂层发射比被吸收的光长的波长的光，其被基于石墨烯的膜骤冷，使得可见度 在石墨烯基膜和荧光涂层之间形成对比度; 并从可见度对比度对石墨烯膜进行成像。
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公开(公告)号：US07144949B2
公开(公告)日：2006-12-05
申请号：US10735079
申请日：2003-12-11
IPC分类号： C08K3/00
CPC分类号： B82Y30/00 , D01F6/76 , Y10T428/2991
摘要： Polymer nanofibers, such as polyaniline nanofibers, with uniform diameters less than 500 nm can be made in bulk quantities through a facile aqueous and organic interfacial polymerization method at ambient conditions. The nanofibers have lengths varying from 500 nm to 10 μm and form interconnected networks in a thin film. Thin film nanofiber sensors can be made of the polyaniline nanofibers having superior performance in both sensitivity and time response to a variety of gas vapors including, acids, bases, redox active vapors, alcohols and volatile organic chemicals.
摘要翻译： 具有均匀直径小于500nm的聚苯胺纳米纤维的聚合物纳米纤维可以通过在环境条件下的容易的水和有机界面聚合方法以大量方式制备。 纳米纤维具有从500nm到10um的长度，并且在薄膜中形成互连的网络。 薄膜纳米纤维传感器可以由聚苯胺纳米纤维制成，其对包括酸，碱，氧化还原活性蒸气，醇和挥发性有机化学品的各种气体蒸气的灵敏度和时间响应都具有优异的性能。
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公开(公告)号：US10135059B2
公开(公告)日：2018-11-20
申请号：US13537686
申请日：2012-06-29
申请人： Jiaxing Huang , Hee Dong Jang , Jiayan Luo
发明人： Jiaxing Huang , Hee Dong Jang , Jiayan Luo
IPC分类号： C09C1/46 , H01M8/16 , H01M4/04 , H01M4/583 , H01M4/88 , H01M4/96 , B82Y30/00 , B82Y40/00 , C01B32/194
摘要： In one aspect of the present invention, a method of for synthesizing compression- and aggregation-resistant particles includes forming a graphene dispersion solution with micron-sized graphene-based material sheets, nebulizing the graphene dispersion solution to form aerosol droplets, passing the aerosol droplets through a horizontal tube furnace pre-heated at a predetermined temperature by a carrier gas, and drying the aerosol droplets to concentrate and compress the micron-sized graphene-based material sheets into crumpled particles of sub-micron scale.
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公开(公告)号：US08825884B2
公开(公告)日：2014-09-02
申请号：US13339182
申请日：2011-12-28
申请人： Wenxue Wang , Jiaxing Huang
发明人： Wenxue Wang , Jiaxing Huang
CPC分类号： H04L69/22
摘要： A protocol identification method and a protocol identification device are provided. The protocol identification method includes acquiring a performance index of protocol characteristic information according to characteristic conditions of the protocol characteristic information; calculating identification probabilities of the protocol characteristic information employed by DPI under a preset statistical strategy according to a DPI identification result; determining an optimal sequence of all protocol characteristic information in a DPI identification library according to the performance index and the identification probabilities of the protocol characteristic information; and performing protocol identification on a received message according to the optimal sequence. The optimal sequence for protocol identification is determined according to the identification probabilities, the protocol characteristic information with a high match success probability may be matched first, and the protocol characteristic information with a high match failure probability may be matched later, which thereby improves the protocol match performance.
摘要翻译： 提供协议识别方法和协议识别装置。 协议识别方法包括根据协议特征信息的特征条件获取协议特征信息的性能指标; 根据DPI识别结果，在预设的统计策略下计算DPI采用的协议特征信息的识别概率; 根据性能指标和协议特性信息的识别概率，确定DPI识别库中所有协议特性信息的最优序列; 并根据最佳顺序对接收到的消息执行协议标识。 根据识别概率确定协议识别的最优序列，可以首先匹配具有高匹配成功概率的协议特征信息，并且可以稍后匹配具有高匹配失败概率的协议特征信息，从而改进协议 匹配表现。
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20.发明申请CRUMPLED PARTICLES, METHODS OF SYNTHESIZING SAME AND APPLICATIONS USING SAME 审中-公开致密颗粒，其合成方法和使用相同的应用公开(公告)号：US20130004798A1
公开(公告)日：2013-01-03
申请号：US13537686
申请日：2012-06-29
申请人： Jiaxing Huang , Hee Dong Jang , Jiayan Luo
发明人： Jiaxing Huang , Hee Dong Jang , Jiayan Luo
CPC分类号： H01M4/04 , B82Y30/00 , B82Y40/00 , C01B32/194 , C01P2004/03 , C01P2004/04 , C01P2006/10 , H01M4/583 , H01M4/88 , H01M4/96 , H01M8/16 , Y02E60/527
摘要： In one aspect of the present invention, a method of for synthesizing compression- and aggregation-resistant particles includes forming a graphene dispersion solution with micron-sized graphene-based material sheets, nebulizing the graphene dispersion solution to form aerosol droplets, passing the aerosol droplets through a horizontal tube furnace pre-heated at a predetermined temperature by a carrier gas, and drying the aerosol droplets to concentrate and compress the micron-sized graphene-based material sheets into crumpled particles of sub-micron scale.
摘要翻译： 在本发明的一个方面，用于合成抗压缩和抗聚集颗粒的方法包括用微米尺寸的石墨烯材料片形成石墨烯分散液，将石墨烯分散液雾化以形成气溶胶液滴，使气雾剂液滴 通过在预定温度下由载气预热的水平管式炉，并干燥气溶胶液滴以将微米尺寸的石墨烯材料片材压缩并压缩成亚微米级的皱巴巴的颗粒。
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