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公开(公告)号：US20160221903A1
公开(公告)日：2016-08-04
申请号：US14914393
申请日：2014-08-29
Applicant: SHELL OIL COMPANY
Inventor： Evert VAN DER HEIDE , Pieter HUIZENGA
IPC: C07C29/60
CPC classification number: C07C29/60 , C07C29/132 , C07C31/202 , C07C31/205
Abstract: The invention provides a process for the catalytic conversion of a saccharide-containing feedstock in a reactor, wherein saccharide-containing feedstock is provided to the reactor as a feed stream through a feed pipe and is contacted with a catalyst system in the reactor, wherein the saccharide-containing feedstock in the feed pipe is maintained at a temperature below the degradation temperature of the saccharide contained therein and a section of the wall of the reactor at the point where the feed pipe enters the reactor is cooled to a temperature below the temperature of the bulk of the reactor and the reactor contents.
Abstract translation: 本发明提供了一种用于在反应器中催化转化含糖原料的方法，其中将含糖原料作为进料流提供给反应器，并通过进料管与反应器中的催化剂体系接触，其中 进料管中的含糖原料保持在低于其中所含的糖的降解温度的温度，并且在进料管进入反应器的点处的反应器壁的一部分被冷却到低于 大部分反应器和反应器内容物。
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公开(公告)号：US20160096789A1
公开(公告)日：2016-04-07
申请号：US14786306
申请日：2014-04-23
Applicant: SHELL OIL COMPANY
IPC: C07C29/132 , C07H1/08 , A23L1/236 , C07D307/68 , C08G63/16 , A23L2/60 , C07H3/02 , C07D307/50
CPC classification number: C07C29/132 , A23L2/60 , A23L27/34 , A23V2002/00 , C07C51/00 , C07D307/50 , C07D307/68 , C07H1/00 , C07H1/08 , C07H3/02 , C08G63/16 , C12P19/02 , C12P19/24 , C13K3/00 , C07C31/202 , C07C59/185
Abstract: The invention provides a process for the preparation of monoethylene glycol from sucrose comprising the steps of: i) hydrolysing sucrose to form a reaction product stream comprising glucose and fructose; ii) separating the reaction product stream comprising glucose and fructose into a fructose or fructose derivative rich stream and a glucose rich stream; and iii) contacting the glucose rich stream with hydrogen in a reactor in the presence of a solvent and a catalyst system with catalytic hydrogenation abilities to produce a product stream comprising monoethylene glycol.
Abstract translation: 本发明提供从蔗糖制备单乙二醇的方法，包括以下步骤：i）水解蔗糖以形成包含葡萄糖和果糖的反应产物流; ii）将包含葡萄糖和果糖的反应产物流分离成富含果糖或果糖衍生物流和富含葡萄糖的流; 和iii）在溶剂和具有催化氢化能力的催化剂体系的存在下在反应器中使富含葡萄糖的物流与氢气接触，以产生包含单乙二醇的产物流。
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公开(公告)号：US20160052843A1
公开(公告)日：2016-02-25
申请号：US14781735
申请日：2014-04-01
Applicant: SHELL OIL COMPANY
Inventor： Evert VAN DER HEIDE , Pieter HUIZENGA
IPC: C07C29/00
CPC classification number: C07C29/00 , C07C29/132 , C07C29/60 , C07C31/202 , C07C31/205
Abstract: The invention provides a process for the catalytic conversion of a saccharide-containing feedstock in a reactor, wherein saccharide-containing feedstock is provided to the reactor as a feed stream through a feed pipe and is contacted with a catalyst system in the reactor and a reaction product is continuously removed from the reactor and wherein the saccharide-containing feedstock is provided through the feed pipe as a pulsed flow and is alternated with a second feed stream comprising a solvent being provided through the same feed pipe.
Abstract translation: 本发明提供了一种用于在反应器中催化转化含糖原料的方法，其中将含糖原料作为进料流提供给反应器，并通过进料管与反应器中的催化剂体系接触， 产物从反应器中连续除去，其中含糖原料通过进料管作为脉冲流提供，并与包含通过相同进料管提供的溶剂的第二进料流交替。
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公开(公告)号：US20240018419A1
公开(公告)日：2024-01-18
申请号：US18254614
申请日：2021-12-17
Applicant: SHELL OIL COMPANY
Inventor： Pieter HUIZENGA
CPC classification number: C10G3/50 , C10G3/42 , B01J8/24 , C10G2300/1003 , C10G2300/1014 , B01J2208/00849
Abstract: A process includes a.) supplying a biomass feedstock, a fluidizing gas having hydrogen, and a catalyst recirculation stream having deoxygenating catalyst to a mixing zone of a fluidized bed reactor; b.) allowing the biomass feedstock, the fluidizing gas and the deoxygenating catalyst to move upwards through the fluidized bed reactor from the mixing zone to a bulk reactor zone; c.) allowing the biomass feedstock to contact the deoxygenating catalyst in the presence of the fluidizing gas in the bulk reactor zone of the fluidized bed reactor to produce a hydropyrolysis reactor output including at least one non-condensable gas, a partially deoxygenated hydropyrolysis product and char; and d.) withdrawing at least a portion of the deoxygenating catalyst from the bulk reactor zone to form the catalyst recirculation stream that is supplied to the mixing zone in step a).
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公开(公告)号：US20200377438A1
公开(公告)日：2020-12-03
申请号：US16970449
申请日：2019-02-19
Applicant: SHELL OIL COMPANY
Inventor： Pieter HUIZENGA , Kai Jürgen FISCHER
Abstract: A method for separating monoethylene glycol (MEG) from one or more oxygenates. The method includes providing a stream comprising MEG and one or more oxygenates to a distillation column, providing a water feed stream to a bottom of the distillation column, and removing a recovery stream comprising MEG from the distillation column. The distillation column is operated at higher temperatures than the thermal stability of MEG and the one or more oxygenates.
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Patent Agency Ranking
公开(公告)号：US20190202764A1
公开(公告)日：2019-07-04
申请号：US16303250
申请日：2017-05-19
Applicant: SHELL OIL COMPANY
Inventor： Kai Jürgen FISCHER , Pieter HUIZENGA , Carmelo PEREZ GOLF , Evert VAN DER HEIDE
CPC classification number: C07C29/84 , C07C29/80 , C07C31/202
Abstract: The invention provides a process for the production of a high purity first diol, selected from the group consisting of C2 to C7 diols from a product stream comprising two or more C2 to C7 diols, said process comprising the steps of: (i) subjecting the product stream to distillation in a first distillation column to provide a bottoms stream comprising high boiling by-products and a top stream comprising a mixture comprising the two or more C2 to C7 diols; (ii) providing said mixture comprising the two or more C2 to C7 diols as a feed to a second distillation column; (iii) providing a feed comprising an extractant to the second distillation column above the mixture comprising the two or more C2 to C7 diols; (iv) operating the second distillation column at a temperature in the range of from 50 to 250° C. and a pressure in the range of from 0.1 to 400 kPa; (v) removing a stream comprising the first diol and the extractant as a bottoms stream from the second distillation column; and (vi) subjecting the stream comprising the first diol and the extractant to distillation in a third distillation column to provide a top stream comprising the first diol in high purity, wherein the extractant is selected from the group of C3 to C6 sugar alcohols and mixtures thereof.
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公开(公告)号：US20190062243A1
公开(公告)日：2019-02-28
申请号：US15768964
申请日：2016-10-16
Applicant: SHELL OIL COMPANY
Inventor： Duraisamy MUTHUSAMY , Viet Quoc NGUYEN , Pieter HUIZENGA
IPC: C07C29/145 , B01J23/30 , B01J25/02 , B01J35/00
Abstract: Implementations of the disclosed subject matter provide methods for producing ethylene glycol from a carbohydrate feed may include contacting, in a first reactor under hydrogenation conditions, the carbohydrate feed with a bi-functional catalyst system. The bi-functional catalyst system may include a heterogeneous hydrogenation catalyst, and a soluble retro-Aldol catalyst. The carbohydrate feed may include a concentration of carbohydrate, in the total solution entering the first reactor, of 5-40 wt % in a solvent. An intermediate product stream may be obtained from the first reactor including ethylene glycol. The hydrogenation conditions may include a temperature in the range of from 180-250° C.
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公开(公告)号：US20180362424A1
公开(公告)日：2018-12-20
申请号：US16060221
申请日：2016-12-07
Applicant: SHELL OIL COMPANY
Inventor： Leslie Andrew CHEWTER , Jean Paul Andre Marie Joseph Ghislain LANGE , Duraisamy MUTHUSAMY , Timothy Michael NISBET , Evert VAN DER HEIDE , Pieter HUIZENGA
CPC classification number: C07C29/132 , B01J8/20 , B01J8/22 , B01J10/007 , B01J16/005 , B01J19/1881 , B01J19/2465 , B01J2208/00283 , B01J2219/0011 , C07C29/60 , C07C31/202 , C07C31/205 , C07C2521/06 , C07C2523/22 , C07C2523/26 , C07C2523/28 , C07C2523/30 , Y02P20/582
Abstract: The invention provides a continuous process for the preparation of ethylene glycol and 1, 2-propylene glycol from starting material comprising one or more saccharides, said process being carried out in a reactor system comprising a reactor vessel equipped with an external recycle loop and said process comprising the steps of: i) providing the starting material in a solvent, via an inlet, to the external recycle loop and contacting it therein with a retro-aldol catalyst composition to provide an intermediate stream; ii) then contacting said intermediate stream with hydrogen in the presence of a hydrogenation catalyst composition in the reactor vessel; iii) withdrawing a product stream comprising glycols from the reactor vessel; iv) providing a portion of said product stream, via an outlet, for separation and purification of the glycols contained therein; and v) recycling the remainder of said product stream via the external recycle loop.
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公开(公告)号：US20170240491A1
公开(公告)日：2017-08-24
申请号：US15519843
申请日：2015-09-09
Applicant: SHELL OIL COMPANY
Inventor： Evert VAN DER HEIDE , Pieter HUIZENGA
IPC: C07C29/132
CPC classification number: C07C29/132 , C07C31/202 , C07C31/205
Abstract: The invention provides a process for the catalytic conversion of a saccharide-containing feedstock in a reactor, wherein saccharide-containing feedstock is provided to the reactor as a feed stream through a feed pipe and is contacted with a catalyst system in the reactor and wherein, as the saccharide-containing feedstock is fed through the feed pipe, a solvent stream, initially comprising essentially no saccharide, is fed along the internal walls of the feed pipe.
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公开(公告)号：US20160107965A1
公开(公告)日：2016-04-21
申请号：US14892391
申请日：2014-05-28
Applicant: SHELL OIL COMPANY
Inventor： Fischer Kai Jürgen , Wouter KOOT , Karin BUS , Pieter HUIZENGA
CPC classification number: C07C29/86 , C07C29/80 , C07C31/202 , C07C31/205 , C07C31/207
Abstract: The invention provides a process for the recovery of a first alcohol from a stream comprising two or more alcohols, said process comprising the steps of providing a stream comprising two or more alcohols, providing a solvent stream, combining said stream comprising two or more alcohols with said solvent stream in the presence of water and recovering at least a portion of the first alcohol by liquid-liquid extraction.
Abstract translation: 本发明提供了从包含两种或更多种醇的物流中回收第一种醇的方法，所述方法包括以下步骤：提供包含两种或更多种醇的物流，提供溶剂流，将包含两种或更多种醇的物流与 所述溶剂流在水的存在下并通过液 - 液萃取回收至少一部分第一醇。
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