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16 条记录 (耗时 0.018 秒)

    ORGANOIRIDIUM COMPLEX FOR ORGANIC ELECTROLUMINESCENT ELEMENTS
    11.
    发明申请
    ORGANOIRIDIUM COMPLEX FOR ORGANIC ELECTROLUMINESCENT ELEMENTS 有权

    公开(公告)号：US20220093879A1

    公开(公告)日：2022-03-24

    申请号：US17426082

    申请日：2020-01-28

    申请人： TANAKA KIKINZOKU KOGYO K.K. ,  UNIVERSITY PUBLIC CORPORATION OSAKA

    发明人： Yasushi MASAHIRO ,  Junichi TANIUCHI ,  Shigeyuki YAGI

    IPC分类号： H01L51/00 ,  C07F15/00 ,  C09K11/06

    摘要： The present invention relates to an organoiridium complex for an organic electroluminescent element in which a C-N ligand and an ancillary ligand are coordinated with iridium. This organoiridium complex contains a 2-(dibenzo[b,d]thiophen-4-yl)quinolinate ligand having at least one methyl group introduced thereinto coordinated as the C-N ligand, and is represented by the following Formula. The present inventive organoiridiurn complex is suitable as a red emitting phosphorescent material for an OLED, has high photoluminescence quantum yield ΦPL, and is excellent in color purity. (In the aforementioned Formula, R1, R2, R3, R4, R5, R6, and R7 are each a methyl group or a hydrogen atom, provided that at least one of R1, R2, R3, R4 is a methyl group; and X-Y is the ancillary ligand.)

    IRIDIUM COMPLEX PRODUCTION METHOD
    13.
    发明申请
    IRIDIUM COMPLEX PRODUCTION METHOD 审中-公开

    公开(公告)号：US20170253623A1

    公开(公告)日：2017-09-07

    申请号：US15503822

    申请日：2015-08-28

    申请人： TANAKA KIKINZOKU KOGYO K.K.

    发明人： Yasushi MASAHIRO ,  Toshiyuki SHIGETOMI ,  Junichi TANIUCHI ,  Ryosuke HARADA

    IPC分类号： C07F15/00 ,  H01L51/00 ,  C09K11/06

    CPC分类号： C07F15/004 ,  C07C45/77 ,  C07C49/92 ,  C07F15/00 ,  C09K11/06 ,  C09K2211/185 ,  C23C16/18 ,  H01L51/0002 ,  H01L51/0085 ,  H01L51/5016

    摘要： A method for manufacturing tris(β-diketonato)iridium by reacting β-diketone with an iridium compound, in which an activation treatment including (a) an alkali treatment and (b) an acid treatment described below is applied to the iridium compound to activate the iridium compound, and to subsequently react the β-diketone, (a) an alkali treatment: a treatment of adding alkali to a solution of the iridium compound to raise pH of the solution to a more alkaline side than that before the alkali addition and to not less than 10, and (b) an acid treatment: a treatment of adding acid to the solution subjected to the alkali treatment to lower pH of the solution to a more acidic side than that before the acid addition and to make the pH difference between solutions before and after the acid addition be not less than 0.1 and not more than 10. The present invention allows manufacture of tris(β-diketonato)iridium utilizing a wide variety of β-diketones.

    RAW MATERIAL AND PRODUCTION METHOD FOR CYCLOMETALLIZED IRIDIUM COMPLEX
    15.
    发明申请
    RAW MATERIAL AND PRODUCTION METHOD FOR CYCLOMETALLIZED IRIDIUM COMPLEX 审中-公开
    用于循环的IRIDIUM复合材料的原料和生产方法

    公开(公告)号：US20160326198A1

    公开(公告)日：2016-11-10

    申请号：US15109927

    申请日：2014-12-16

    申请人： TANAKA KIKINZOKU KOGYO K.K. ,  NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY

    发明人： Hideo KONNO ,  Junichi TANIUCHI ,  Ryosuke HARADA ,  Toshiyuki SHIGETOMI ,  Yasushi MASAHIRO

    IPC分类号： C07F15/00

    CPC分类号： C07F15/0033 ,  C07C49/92 ,  C07F15/004

    摘要： The present invention relates to a raw material for a cyclometalated iridium complex, and provides a technique that makes it possible to obtain a cyclometalated iridium complex in higher yield at a lower reaction temperature than using tris(2,4-pentanedionato)iridium(III). The present invention relates to a raw material for a cyclometalated iridium complex, including an organic iridium material for producing a cyclometalated iridium complex, the organic iridium material being a tris(β-diketonato)iridium(III), in which an asymmetric β-diketone is coordinated to iridium.

    摘要翻译： 本发明涉及环金属化铱络合物的原料，并且提供了一种技术，其可以在比使用三（2,4-戊二酮）铱（III）的较低的反应温度下以更高的产率获得环金属化铱络合物。 。 本发明涉及一种环金属铱络合物的原料，包括用于制备环金属化铱络合物的有机铱材料，有机铱材料是三（β-二酮）铱（III），其中不对称β-二酮 与铱配合。

    METHOD FOR PRODUCING SILVER PARTICLES, AND SILVER PARTICLES PRODUCED BY SAID METHOD
    16.
    发明申请
    METHOD FOR PRODUCING SILVER PARTICLES, AND SILVER PARTICLES PRODUCED BY SAID METHOD 审中-公开
    生产银颗粒的方法，以及通过方法生产的银颗粒

    公开(公告)号：US20160303659A1

    公开(公告)日：2016-10-20

    申请号：US15101859

    申请日：2014-12-11

    申请人： TANAKA KIKINZOKU KOGYO K.K.

    发明人： Yuichi MAKITA ,  Yuusuke OHSHIMA ,  Hidekazu MATSUDA ,  Junichi TANIUCHI ,  Noriaki NAKAMURA ,  Hitoshi KUBO

    IPC分类号： B22F9/30 ,  B82Y40/00 ,  B22F1/00 ,  B82Y30/00

    CPC分类号： B22F9/30 ,  B22F1/0003 ,  B22F1/0018 ,  B22F1/0062 ,  B22F2301/255 ,  B22F2304/054 ,  B22F2304/056 ,  B22F2998/10 ,  B82Y30/00 ,  B82Y40/00 ,  H01B1/02

    摘要： The present invention provides a method for producing silver particles, including the steps of: mixing a thermally decomposable silver compound and an amine compound to prepare a silver-amine complex as a precursor; and heating the silver-amine complex at a heating temperature equal to or higher than the decomposition temperature of the silver-amine complex to precipitate silver particles, the silver compound being silver carbonate, the amine compound being terminated with a primary amino group on at least one end and containing a predetermined hydrocarbon group R with a carbon number of 4 to 10. In the method of the present invention, silver particles with the particle size controlled to fall within the range of 20 nm to 200 nm in terms of an average particle size can be produced.

    摘要翻译： 本发明提供一种银粒子的制造方法，包括以下步骤：将可热分解的银化合物和胺化合物混合，制备作为前体的银 - 胺络合物; 并在银 - 胺络合物的分解温度以上的加热温度下加热银 - 胺络合物，沉淀银粒子，银化合物为碳酸银，至少在伯胺基上封端的胺化合物 一端并含有碳原子数为4〜10的规定的烃基R。在本发明的方法中，将粒径控制在20nm〜200nm范围内的银粒子平均粒子 尺寸可以生产。