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11.发明授权公开(公告)号：US06652603B2
公开(公告)日：2003-11-25
申请号：US09896806
申请日：2001-06-29
申请人： Juraj Babjak , Feng Zou
发明人： Juraj Babjak , Feng Zou
IPC分类号： B01D900
CPC分类号： C01G53/04 , C01D5/00 , C02F1/22 , C02F2101/20
摘要： A method for removing sodium sulfate from nickel and ammonia containing aqueous effluents. The effluents, typically from a nickel hydroxide production process, are cooled to or below 30° C. to crystallize and precipitate the sodium sulfate and dewater the effluent. The sodium sulfate is retrieved and the remaining solution is recycled back to the nickel hydroxide production process.
摘要翻译： 从含镍和含氨水的废水中除去硫酸钠的方法。 通常来自氢氧化镍生产过程的流出物被冷却至或低于30℃以结晶并沉淀硫酸钠并使流出物脱水。 回收硫酸钠，将剩余的溶液循环回氢氧化镍生产过程。
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公开(公告)号：US5281494A
公开(公告)日：1994-01-25
申请号：US519530
申请日：1990-05-04
CPC分类号： C01G53/04 , H01M4/52 , C01P2002/72 , C01P2004/03 , C01P2004/32 , C01P2006/11 , C01P2006/20 , C01P2006/60 , C01P2006/80
摘要： A novel process for the production of nickel hydroxide wherein particulate nickel is reacted with oxygen in the presence of liquid water at a temperature of at least 180.degree. C. The invention also includes the nickel hydroxide product so produced.
摘要翻译： 一种用于生产氢氧化镍的新方法，其中颗粒状镍在液态水存在下在至少180℃的温度下与氧反应。本发明还包括如此制备的氢氧化镍产品。
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公开(公告)号：US4957543A
公开(公告)日：1990-09-18
申请号：US368193
申请日：1989-06-16
申请人： Juraj Babjak , Victor A. Ettel , Vladimir Paserin
发明人： Juraj Babjak , Victor A. Ettel , Vladimir Paserin
CPC分类号： C22B23/00 , B01D39/2051 , B22F3/1137 , C22B5/20 , C23C16/16 , H01M4/808 , B22F2998/00 , Y10T428/12479 , Y10T428/12486
摘要： The invention provides a nickel foam and a method of forming a nickel foam for a nickel containing battery. An open-cell foam structure is placed in a nickel carbonyl gas containing structure. The foam structure is heated to a temperature at which nickel carbonyl decomposes. Nickel from the nickel carbonyl gas decomposes on the foam structure to form a nickel plated foam structure. The nickel plated foam structure is then sintered leaving an open-cell nickel network to form the nickel foam. The open-cells of the nickel foam comprise substantially hollow wires having a substantially uniform transverse cross-section. The nickel foam is further characterized by the conductivity through the nickel foam multiplied by a factor of 3.4 being equal to or greater than the theoretical conductivity of nickel.
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14.发明授权Process for metal recovery by solvent extraction from CaSO.sub.4 containing sulfate solutions 失效通过溶剂萃取从含CaSO 4的硫酸盐溶液中回收金属的方法
公开(公告)号：US4610861A
公开(公告)日：1986-09-09
申请号：US767096
申请日：1985-08-19
申请人： Juraj Babjak
发明人： Juraj Babjak
CPC分类号： C01G51/003 , B01D11/0434 , C22B3/0066 , C22B3/0077 , Y02P10/234
摘要： A multistage countercurrent solvent extraction process for removing cobalt from an aqueous sulfate solutions containing saturation amounts of calcium using an organic soluble phosphinic acid as the extractant preferably characterized by control of pH in various stages of the process to minimize scaling of gypsum in the extraction equipment.
摘要翻译： 使用有机可溶性次膦酸作为萃取剂从含有饱和量的钙的硫酸盐水溶液中除去钴的多级逆流溶剂萃取方法优选地特征在于控制在该方法的各个阶段中的pH以最小化萃取设备中石膏的结垢。
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15.发明授权
公开(公告)号：US4320099A
公开(公告)日：1982-03-16
申请号：US172670
申请日：1980-07-28
申请人： Juraj Babjak
发明人： Juraj Babjak
CPC分类号： C01G51/10 , C01G53/003 , C22B3/42 , Y02P10/234
摘要： By contacting an aqueous cobaltous sulfate solution with an ion-exchange resin having bis--(2-picolyl)amine functional groups nickel is removed down to very low levels.
摘要翻译： 通过使硫酸钴水溶液与具有双（2-吡啶甲基）胺官能团的离子交换树脂接触，将镍除去至非常低的水平。
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公开(公告)号：US07033555B2
公开(公告)日：2006-04-25
申请号：US10430154
申请日：2003-05-06
IPC分类号： C01D15/00
CPC分类号： C01G45/1228 , C01G51/42 , C01G51/50 , C01G53/42 , C01G53/50 , C01P2002/72 , C01P2002/76 , C01P2006/40 , H01M4/505 , H01M4/525
摘要： A low temperature contaminant limiting process for lithiating hydroxides and forming lithiated metal oxides of suitable crystalinity in-situ. M(OH)2 is added to an aqueous solution of LiOH. An oxidant is introduced into the solution which is heated below about 150° C. and, if necessary, agitated. M may be selected from cobalt, nickel and manganese. The resultant LiMO2 becomes crystallized in-situ and is subsequently removed.
摘要翻译： 用于锂化氢氧化物的低温污染物限制方法，并原位形成适当结晶度的锂化金属氧化物。 向LiOH的水溶液中加入M（OH）2 N。 将氧化剂引入溶液中，该溶液被加热至低于约150℃，如果需要，将其搅拌。 M可以选自钴，镍和锰。 所得LiMO 2 N 2原位结晶并随后除去。
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公开(公告)号：US5545392A
公开(公告)日：1996-08-13
申请号：US402368
申请日：1995-03-13
申请人： Juraj Babjak , Victor A. Ettel
发明人： Juraj Babjak , Victor A. Ettel
IPC分类号： C01G20060101 , C01G53/04 , C01B13/14
CPC分类号： C01G53/04 , C01P2006/12 , C01P2006/80
摘要： The invention provides a method of producing nickel hydroxide from elemental metal. Elemental nickel is first introduced into an aqueous ammonia or ammonia/ammonium salt solution capable of dissolving nickel. The potential, as measured by a standard calomel electrode, is allowed to reach a negative or reducing level. Oxygen is added to the aqueous solution at a rate that maintains the negative potential to facilitate the conversion of elemental nickel to nickel hydroxide. Nickel hydroxide may be readily precipitated from the aqueous solution.
摘要翻译： 本发明提供从元素金属制造氢氧化镍的方法。 首先将元素镍引入能够溶解镍的氨水或氨/铵盐溶液中。 由标准甘汞电极测量的电位被允许达到负的或降低的水平。 将氧气以维持负电位的速率加入到水溶液中，以促进元素镍转化为氢氧化镍。 氢氧化镍可能容易从水溶液中沉淀出来。
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公开(公告)号：US5447707A
公开(公告)日：1995-09-05
申请号：US196769
申请日：1994-02-10
申请人： Juraj Babjak , Victor A. Ettel , Stephen J. Baksa
发明人： Juraj Babjak , Victor A. Ettel , Stephen J. Baksa
CPC分类号： C01G53/04 , H01M4/52 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/80
摘要： A process for producing nickel hydroxide from nickel powders, in which the feed nickel powder is directly converted in an aqueous solution containing nitrate and particulate nickel at least at room temperature and a pH in excess of about 6 into nickel hydroxide of a high density. Nickel powders of high surface area, e.g. 0.4 m.sup.2 /g or higher, typically produced by the thermal decomposition of nickel carbonyl, are particularly suitable as feed materials for this process.
摘要翻译： 一种从镍粉生产氢氧化镍的方法，其中将进料镍粉末至少在室温下直接转化成含有硝酸盐和颗粒状镍的水溶液，并将pH超过约6转化成高密度氢氧化镍。 高表面积的镍粉，例如 通常通过羰基镍热分解产生的0.4m 2 / g或更高，特别适用于该方法的进料。
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公开(公告)号：US5145716A
公开(公告)日：1992-09-08
申请号：US560859
申请日：1990-07-27
CPC分类号： C23C16/16 , C23C16/481
摘要： The invention provides an apparatus for metal plating a substrate. The apparatus includes a chamber adapted to receive metal carbonyl gas. The chamber includes an infrared transparent window. The infrared transparent window has a cooling passage filled with liquid coolant. The liquid coolant has a temperature below which decomposition of the metal carbonyl gas occurs. The liquid coolant prevents decomposition of the metal carbonyl gas on the infrared transparent window. The liquid coolant also is substantially infrared transparent for allowing infrared radiation through the infrared transparent window and cooling passage into the chamber. An infrared radiation source sends infrared radiation into the chamber through the infrared transparent window and cooling passage to heat the substrate to a temperature at which decomposition of the metal carbonyl gas occurs.
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公开(公告)号：US4764353A
公开(公告)日：1988-08-16
申请号：US380075
申请日：1982-05-20
申请人： Juraj Babjak , Eberhard Krause
发明人： Juraj Babjak , Eberhard Krause
CPC分类号： C22B60/0234 , C22B60/0208
摘要： Uranium is leached from water slurries of uranium ore by incorporating a mixture of sulfur dioxide and air therein to provide the oxidizing and acidifying requirements to accomplish leaching.
摘要翻译： 通过在其中混合二氧化硫和空气来将铀从铀矿石的水浆中浸出以提供氧化和酸化的要求以完成浸出。
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