APPARATUS AND METHODS FOR INORGANIC ELECTROLYTE SYNTHESIS

    公开(公告)号:US20240198419A1

    公开(公告)日:2024-06-20

    申请号:US18556807

    申请日:2022-04-22

    IPC分类号: B22F1/142 B22F9/04 B22F9/20

    摘要: Methods for millling particles include exposing particles to microwave energy during milling. The methods reduce or eliminate the need for pre- and post-processing of reagents and products while minimizing waste associated with the slow kinetics of heat transfer in traditional resistive heating furnaces. Method of synthesizing particles include providing precursor particles, microwave susceptor media, and milling media in a reaction vessel and simultaneously rotating the reaction vessel while exposing the reaction vessel to microwaves. Apparatus for milling particles include a microwave housing defining a microwave enclosure; a microwave generator configured to generate and direct microwaves to the microwave enclosure; and a rotation shaft within the microwave enclosure, the rotation shaft connected or configured to be connected to a motor for rotation, wherein the rotation shaft is configured to be rotatably coupled, within the microwave enclosure, to a processing vessel.

    Method for Preparing Nano-SiO2 Reinforced Aluminum Matrix Composites

    公开(公告)号:US20190185974A1

    公开(公告)日:2019-06-20

    申请号:US16161557

    申请日:2018-10-16

    IPC分类号: C22C32/00

    摘要: A method for preparing nano-SiO2 reinforced aluminum matrix composites, includes the following: Step-1, powder mixing: mixing aluminum matrix powder with nano-SiO2 powder to obtain raw material powder, wherein the aluminum matrix powder has an average particle size between 30 μm to 100 μm, the nano-SiO2 powder has an average particle size between 5 nm to 145 nm, mass percentage of nano-SiO2 in the raw material powder is 0.01% to 5% and the remaining raw material powder is the aluminum matrix powder; Step-2, shaping: press shaping the powder obtained in the Step-1 to obtain base bodies; Step-3, sintering: sintering the base bodies obtained in the Step-2 in an atmosphere of N2 at 550° C. to 660° C., preserving the temperature for a period of 5 min to 60 min, and cooling in a furnace at end of the period under protection of N2 for 0.5 h to 3 h; and Step-4, heat treatment.