Biocidal polymers and polymer dispersions, processes for their
preparation and their use
    11.
    发明授权
    Biocidal polymers and polymer dispersions, processes for their preparation and their use 失效
    杀生物聚合物和聚合物分散体,其制备方法及其用途

    公开(公告)号:US5252321A

    公开(公告)日:1993-10-12

    申请号:US994138

    申请日:1992-12-21

    CPC分类号: C08F246/00 A01N47/18

    摘要: Preparation of biocidal polymers and copolymers based on free radical-polymerizable and copolymerizable ethylenically unsaturated monomers containing monomer units composed of BCM salts of ethylenically unsaturated carboxylic acids, sulfonic acids or phosphonic acids, solutions thereof and preferably aqueous dispersions thereof. Processes for their preparation and their use as fungicidal and algicidal impregnating agents, paints and finishing agents for scumbles and dispersion paints providing protection against blue staining on wood, for synthetic resin renderings, for exposed concrete paints and for textile finishing agents.

    摘要翻译: 制备基于可自由基聚合和可共聚的烯属不饱和单体的杀生物聚合物和共聚物,其含有由烯键式不饱和羧酸,磺酸或膦酸的BCM盐,其溶液和优选其水分散体组成的单体单元。 它们的制备方法及其作为杀真菌剂和杀藻剂浸渍剂,涂料和整理剂的用途,用于提供防止木材上的蓝色染色,用于合成树脂效果,用于暴露的混凝土涂料和纺织品整理剂的防污染和分散涂料。

    Chemical process for the preparation of pharmaceutically active compounds
    13.
    发明授权
    Chemical process for the preparation of pharmaceutically active compounds 失效
    用于制备药物活性化合物的化学方法

    公开(公告)号:US5023337A

    公开(公告)日:1991-06-11

    申请号:US469749

    申请日:1990-01-19

    IPC分类号: C07D235/32

    CPC分类号: C07D235/32

    摘要: The present invention is directed to the preparation of benzimidazole derivatives of the formula (I), ##STR1## wherein A=stands for S, SO or SO.sub.2,R.sup.1 =stands for C.sub.1-4 alkyl group,R.sup.2 =stands for C.sub.1-4 alkyl, C.sub.3-7 cycloalkyl or C.sub.6-10 aryl or aralkyl,comprising reacting a sulphochloride of the formula (II) ##STR2## with an alkyl aluminum compound of the formula (III).R.sub.n.sup.2 AlClhd (3-n) (III)The reaction is performed in one step.

    摘要翻译: 本发明涉及制备式(I)的苯并咪唑衍生物,其中A = S,SO或SO 2,R 1 = C 1-4烷基,R 2代表C 1 1-4烷基,C 3-7环烷基或C 6-10芳基或芳烷基,其包括使式(II)的二氯化亚氨基与式(III)的烷基铝化合物反应。 Rn2AlClhd(3-n)(III)反应在一个步骤中进行。

    Substituted benzimidazole fungicide
    14.
    发明授权
    Substituted benzimidazole fungicide 失效
    取代的苯并咪唑杀真菌剂

    公开(公告)号:US4857541A

    公开(公告)日:1989-08-15

    申请号:US894029

    申请日:1986-08-07

    申请人: Mikio Chiba

    发明人: Mikio Chiba

    IPC分类号: C07D235/32 A01N47/38

    CPC分类号: A01N47/38

    摘要: A fungicide which is particularly effective against benomyl resistant fungi is selected from the group of fungicides represented by the formula: ##STR1## wherein R is C.sub.n H.sub.2n+1 and n is 1, 2, 3 or 6 or R is phenyl. The method comprises applying as a suspension an effective amount of the one or more fungicides selected from the formula to benomyl resistant fungi, such as benomyl resistant isolates of Botrytis cinerea.

    Process for the preparation of benzimidazole-thiol
    15.
    发明授权
    Process for the preparation of benzimidazole-thiol 失效
    苯并咪唑硫醇的制备方法

    公开(公告)号:US4675413A

    公开(公告)日:1987-06-23

    申请号:US811246

    申请日:1985-12-19

    IPC分类号: C07D235/32 C07D235/04

    CPC分类号: C07D235/32

    摘要: A new process is disclosed for preparing a compound of the formula (I) ##STR1## wherein R is C.sub.1 to C.sub.5 alkyl; which comprises reducing a compound of the formula (II) ##STR2## or salt thereof wherein A is --SO.sub.2 X, --SOH, --SOA.sup.1, or --SA.sup.1 group,X is chlorine or hydrogen; andA.sup.1 is a group of the Formula ##STR3## with the aid of aluminum activated with a catalytic amount of a metal and/or metal salt in a mixture of water, a mineral acid, and an aliphatic carboxylic acid having 1 to 3 carbon atoms at a temperature of 0.degree. to 100.degree. C., thereafter, optionally, the product is recovered from an acid medium at a pH range of 2 to 3 in crystalline form.

    摘要翻译: 公开了用于制备式(I)化合物的新方法,其中R是C1至C5烷基; 其包括还原式(II)的化合物或其盐,其中A是-SO 2 X,-SOH,-SOA 1或-SA 1基团,X是氯或氢; 并且A1是通过在水,无机酸和具有1至3个碳原子的脂族羧酸的混合物中催化量的金属和/或金属盐活化的铝的助催化剂的组合的“IMAGE” 在0℃至100℃的温度下,然后,任选地,该产物从酸性介质中以2至3的结晶形式从pH值范围内回收。

    Process for preparing substituted urea derivatives
    19.
    发明授权
    Process for preparing substituted urea derivatives 失效
    制备取代脲衍生物的方法

    公开(公告)号:US4435567A

    公开(公告)日:1984-03-06

    申请号:US334470

    申请日:1981-12-28

    摘要: A process for the preparation of substituted urea derivatives, and compositions and concentrates for the same purpose are disclosed. According to the process the substituted urea derivatives of formula (I) ##STR1## wherein R is hydrogen, alkyl, aryl, cycloalkyl or aralkyl, R.sup.1 and R.sup.2 are hydrogen, alkyl, alkenyl, alkinyl, alkoxy, oxyalkyl, cycloalkyl, aralkyl, alkoxycarbonylalkyl, aryl or heteroaryl, or R.sup.1 and R.sup.2 together with the adjacent nitrogen atom may form a saturated or unsaturated heterocycle, or a condensed and/or substituted ring system, and said heterocycle or said condensed and/or substituted ring system may contain also a sulfo group,can be manufactured by reacting an amine of formula (II) ##STR2## with an N-carbamoyl-benzoic acid sulfimide derivative of formula (III) ##STR3## The disclosed N-acylating composition comprises of from 3 to 60% by weight, preferably of from 5 to 50% by weight sulfimide derivative of formula (III), of from 97 to 40% by weight, preferably of from 95 to 50% by weight solvent, and if desired, an organic or inorganic base.The disclosed N-acylating concentrate comprises of from 60 to 95.5% by weight N-acylating agent of formula (III) and of from 4.5 to 40% by weight additives.

    摘要翻译: 公开了用于制备取代的脲衍生物的方法,以及用于相同目的的组合物和浓缩物。 根据该方法,式(I)的取代脲衍生物其中R是氢,烷基,芳基,环烷基或芳烷基,R1和R2是氢,烷基,烯基,炔基,烷氧基,烷氧基,环烷基,芳烷基,烷氧基羰基 ,芳基或杂芳基,或R 1和R 2与相邻的氮原子一起可以形成饱和或不饱和的杂环或稠合和/或取代的环系,并且所述杂环或所述缩合和/或取代的环系可以含有磺基 可以通过使式(II)的胺与式(III)的N-氨基甲酰基 - 苯甲酸硫酰亚胺衍生物反应来制备。所公开的N-酰化组合物包含3至60重量% ,优选为5至50重量%的式(III)的亚磺酰亚胺衍生物,为97至40重量%,优选为95至50重量%的溶剂,如果需要,为有机或无机碱。 所公开的N-酰化浓缩物包含60至95.5重量%的式(III)的N-酰化剂和4.5至40重量%的添加剂。