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公开(公告)号：US20090285866A1
公开(公告)日：2009-11-19
申请号：US12119623
申请日：2008-05-13
CPC分类号： A61K8/31 , A61K8/025 , A61K8/0279 , A61K8/735 , A61K8/8152 , A61K8/88 , A61K8/891 , A61K2800/56 , A61K2800/654 , A61Q19/001
摘要： A composition including a film-former and a porous polymeric release system comprising a solvent for the film-former is provided. Also provided is a method of prolonging the physical stability of a film-former on the skin by applying to the skin a self-healing composition containing the film-former and a porous polymeric release system comprising a solvent for the film-former.
摘要翻译： 提供包含成膜剂和包含成膜剂溶剂的多孔聚合物释放体系的组合物。 还提供了一种通过向皮肤施加含有成膜剂的自愈组合物和包含成膜剂的溶剂的多孔聚合物释放体系来延长成膜剂在皮肤上的物理稳定性的方法。
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22.发明授权公开(公告)号：US06387995B1
公开(公告)日：2002-05-14
申请号：US09776516
申请日：2001-02-01
申请人： Milan F. Sojka
发明人： Milan F. Sojka
IPC分类号： C08L3304
CPC分类号： B01J20/30 , B01J20/26 , C08F2/06 , C08F20/04 , C08F220/28 , C08F220/40 , C08F222/1006 , C09K3/32 , C09K8/12 , C09K8/887 , Y10S526/909 , Y10T428/2987
摘要： A process for producing a microporous oil sorbent polymer comprising the steps of: dissolving a polyunsaturated monomer in a silicone organic solvent to provide a monomer mixture containing more than 90% by weight polyunsaturated monomer; polymerizing said monomers by precipitation polymerization, under an inert atmosphere to precipitate microporous, micro-particles in the form of micro-particles, agglomerates and aggregates having a bulk density of about 0.02 gm/cm3 to about 0.01 gm/cm3 and capable of adsorbing at least about 20% by weight organic materials based on the total weight of polymer plus adsorbed organic material.
摘要翻译： 一种制备微孔油吸附剂聚合物的方法，包括以下步骤：将多不饱和单体溶解在有机硅有机溶剂中以提供含有超过90重量％的多不饱和单体的单体混合物;在惰性气氛下通过沉淀聚合将所述单体聚合， 沉淀为微粒形式的微孔微粒，堆积物和聚集体，其堆积密度为约0.02gm / cm 3至约0.01g / cm 3，并且能够基于总量吸附至少约20重量％的有机材料 聚合物加吸附有机材料的重量。
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公开(公告)号：US5834577A
公开(公告)日：1998-11-10
申请号：US891717
申请日：1997-07-11
申请人： Milan F. Sojka
发明人： Milan F. Sojka
IPC分类号： B01J20/26 , B01J20/28 , B01J20/30 , C08F2/06 , C08F2/18 , C08F220/18 , C08F220/20 , C08F220/28 , C08F220/40 , C08F222/10 , C09K3/32 , C08F20/10
CPC分类号： B01J20/26 , B01J20/30 , C08F2/06 , C08F220/18 , C08F220/28 , C08F220/40 , C08F222/1006 , C09K3/32 , Y10T428/2998
摘要： The present invention is directed to a porous copolymer micro-particle having a high oil absorbency. The method of the present invention comprises the steps of: dissolving at least two polyunsaturated monomers in a water-immiscible organic solvent to provide a monomer mixture containing at least about 60%, preferably about 100% by weight polyunsaturated monomers; adding the monomer mixture to an aqueous solution, preferably having an effective amount of a suspension stabilizer dissolved therein, to form an organic/aqueous biphasic liquid system; vigorously agitating the biphasic liquid system at a rate sufficient to cause the water immiscible organic phase to be suspended as micro-droplets in the aqueous phase; continuing vigorous agitating during polymerization of the monomers in the suspended micro-droplets to produce a microporous polymer micro-particle; and separating the microporous polymer micro-particle from the organic solvent to produce a microporous and oil sorbent polymer micro-particle having a mean unit diameter of less than about 25 microns.
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公开(公告)号：US5830967A
公开(公告)日：1998-11-03
申请号：US810268
申请日：1997-03-03
申请人： Milan F. Sojka
发明人： Milan F. Sojka
IPC分类号： B01J20/26 , B01J20/30 , C08F2/00 , C08F2/06 , C08F2/18 , C08F20/04 , C08F220/28 , C08F220/40 , C08F222/10 , C09K3/32 , C09K8/12 , C09K8/88 , C08F20/10
CPC分类号： B01J20/26 , B01J20/30 , C08F2/06 , C08F2/18 , C08F20/04 , C08F220/18 , C08F220/28 , C08F220/40 , C08F222/1006 , C09K3/32 , C09K8/12 , C09K8/887 , Y10T428/2998
摘要： The present invention is directed to a porous polymer micro-particle, in the form of broken spheres, open to a porous oleophilic interior surface area, having a high oil and water absorbency and an apparent bulk density of about 0.02 to about 0.1 grams/cc. The preferred method of the present invention comprises the steps of: dissolving at least one and preferably at least two polyunsaturated monomers along with an effective amount of an organic polymerization initiator in a water-immiscible organic solvent to provide a monomer mixture; adding the monomer mixture to an aqueous solution, preferably having an effective amount of a suspension stabilizer dissolved therein, to form an organic/aqueous biphasic liquid system; vigorously agitating the biphasic liquid system at a rate sufficient to cause the water-immiscible organic phase to be suspended as micro-droplets in the aqueous phase; continuing vigorous agitating during polymerization of the monomers in the suspended micro-droplets to produce a microporous polymer micro-particle; and separating the microporous polymer micro-particle from the organic solvent to produce a microporous and oil sorbent polymer micro-particle having a mean unit diameter of less than about 25 microns and a total sorptive capacity for mineral oil that is at least about 72% by weight, preferably at least about 80% by weight dry polymer basis.
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25.发明授权
公开(公告)号：US5830960A
公开(公告)日：1998-11-03
申请号：US935346
申请日：1997-09-22
申请人： Milan F. Sojka
发明人： Milan F. Sojka
IPC分类号： B01J20/26 , B01J20/30 , C08F2/00 , C08F2/06 , C08F2/14 , C08F20/04 , C08F220/20 , C08F220/28 , C08F220/40 , C08F222/10 , C09K3/32 , C09K8/12 , C09K8/88
CPC分类号： B01J20/30 , B01J20/26 , C08F2/06 , C08F20/04 , C08F220/28 , C08F220/40 , C08F222/1006 , C09K3/32 , C09K8/12 , C09K8/887 , Y10S526/909 , Y10T428/2987
摘要： A process for producing a microporous oil sorbent polymer comprising the steps of: dissolving a polyunsaturated monomer in a silicone organic solvent to provide a monomer mixture containing more than 90% by weight polyunsaturated monomer; polymerizing said monomers by precipitation polymerization, under an inert atmosphere to precipitate microporous, micro-particles in the form of micro-particles, agglomerates and aggregates having a bulk density of about 0.02 gm/cm.sup.3 to about 0.01 gm/cm.sup.3 and capable of adsorbing at least about 20% by weight organic materials based on the total weight of polymer plus adsorbed organic material.
摘要翻译： 一种制备微孔油吸附剂聚合物的方法，包括以下步骤：将多不饱和单体溶解在硅氧烷有机溶剂中，以提供含有超过90重量％的多不饱和单体的单体混合物; 在惰性气氛下通过沉淀聚合使所述单体聚合，以沉积微孔，聚集体和聚集体形式的微孔微粒，其堆积密度为约0.02gm / cm 3至约0.01g / cm 3并能够吸附在 基于聚合物加吸附的有机材料的总重量，至少约20重量％的有机材料。
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26.发明授权
公开(公告)号：US5773546A
公开(公告)日：1998-06-30
申请号：US723866
申请日：1996-09-30
申请人： Anthony S. Tomlin , Milan F. Sojka
发明人： Anthony S. Tomlin , Milan F. Sojka
IPC分类号： C08F2/08 , B01J20/26 , B01J20/30 , C08F2/06 , C08F20/04 , C08F20/06 , C08F20/18 , C08F120/04 , C08F220/04 , C08F220/10 , C09K3/32 , C09K8/12 , C09K8/88 , C08F20/20
摘要： The present invention is directed to an improved process for producing water-soluble and water-insoluble carboxylic acid polymers and copolymers. The process comprises the steps of polymerizing a carboxylic acid monomer, and a polyfunctional cross-linker monomer in a second embodiment, in an effective molar ratio, in a silicone solvent under an inert atmosphere in the presence of an effective amount of an initiator. The preferred copolymer of the second embodiment includes acrylic acid as the carboxylic acid monomer and a lauryl methacrylate and/or stearyl methacrylate as a comonomer. The resulting copolymers have new and unexpected tolerance to salt-containing water when mixed therewith.
摘要翻译： 本发明涉及一种生产水溶性和水不溶性羧酸聚合物和共聚物的改进方法。 该方法包括在有效量的引发剂的存在下，在有机摩尔比的硅氧烷溶剂中，在惰性气氛下，在第二个实施方案中聚合羧酸单体和多官能交联剂单体的步骤。 第二实施方案的优选共聚物包括作为羧酸单体的丙烯酸和作为共聚单体的甲基丙烯酸月桂酯和/或甲基丙烯酸硬脂酯。 当与其混合时，所得共聚物对含盐水具有新的和意想不到的耐受性。
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公开(公告)号：US5302379A
公开(公告)日：1994-04-12
申请号：US26706
申请日：1993-03-05
申请人： Milan F. Sojka
发明人： Milan F. Sojka
IPC分类号： A61K8/00 , A61K8/37 , A61K8/89 , A61K8/892 , A61K8/895 , A61K8/91 , A61Q3/00 , A61Q3/02 , C08L83/04 , C08L83/06 , C09D151/00 , C09D151/06 , C09D183/04 , C09D183/06 , A61K7/04
摘要： An improved nail lacquer containing a film forming resin, a plasticizer, and a solvent. The improvement resides in utilizing as the film forming resin a blend of: (i) a graft copolymer having a main backbone chain of acrylic ester units and methacrylic ester units, with the main backbone chain having grafted thereto pendant trialkoxysilyl groups and pendant ethylene glycol dimethacrylate groups; and (ii) a silsesquioxane resin containing RSiO.sub.3/2 units and .tbd.SiOH units in which R is an alkyl group or an aryl group. In an alternate form of the invention, the film forming resin is not a blend, but an improved type of graft copolymer containing, in addition to pendant trialkoxysilyl groups, pendant vinylbenzyl chloride groups.
摘要翻译： 改进的含有成膜树脂，增塑剂和溶剂的指甲油。 改进在于利用成膜树脂的共混物：（i）具有丙烯酸酯单元的主要主链和甲基丙烯酸酯单元的接枝共聚物，主链主链有三烷氧基甲硅烷基侧链和二乙二醇二甲基丙烯酸酯侧链 团体 和（ii）含有RSiO3 / 2单元和（三键）SiOH单元的倍半硅氧烷树脂，其中R是烷基或芳基。 在本发明的替代形式中，成膜树脂不是共混物，而是改进型的接枝共聚物，除了三烷氧基甲硅烷基侧基之外，还含有侧基乙烯基苄基氯基团。
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公开(公告)号：US5157139A
公开(公告)日：1992-10-20
申请号：US770376
申请日：1991-10-03
CPC分类号： C07F7/188
摘要： The present invention relates to a process for preparing clear and colorless alkoxysilane monomers from the reaction of a silazane with an organic alcohol in the presence of an inorganic acid catalyst. The inorganic acid catalyst is present in a critical range from 20 parts per million (ppm) to 300 ppm. Inorganic acid catalysts used within this critical range eliminate the need for a purification step in the process.
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公开(公告)号：US4962170A
公开(公告)日：1990-10-09
申请号：US401582
申请日：1989-08-31
IPC分类号： G02C7/04 , A01N25/00 , A01N25/08 , A01N25/10 , A61K8/04 , A61K8/81 , A61K47/30 , A61K47/32 , A61Q19/00 , B01J20/26 , C08F2/04 , C08F2/06 , C08F8/00 , C08J3/00 , C11D3/37 , G02C13/00
CPC分类号： A61Q19/00 , A61K8/022 , A61K8/0241 , A61K8/8152 , B82Y5/00 , C08F2/06 , C11D3/3757 , A61K2800/413 , A61K2800/56
摘要： A method of forming a highly adsorptive polymer, which includes the steps of: (a) homogeneously mixing a solution of a monomer consisting exclusively of one or more types of polyunsaturated monomer, a monomer solvent, and an initiator, (b) polymerizing the monomers to form a polymer, wherein the monomer solvent is a solvent for the monomers and a non-swelling non-solvent for the polymer, and (c) removing the solvent from the polymer to form a dry powder.
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公开(公告)号：US4962133A
公开(公告)日：1990-10-09
申请号：US402321
申请日：1989-09-05
IPC分类号： C08F2/04 , C08F2/06 , C08F6/06 , C08F6/10 , C08F220/00 , C08F220/10 , C08J9/28
CPC分类号： C08F2/06 , C08J9/286 , Y10S521/921
摘要： A precipitation polymerization process for the production of a macroporous cross-linked copolymer in which there is added to a reactor equipped with a stirrer, at least one monounsaturated monomer and at least one polyunsaturated monomer, dissolving an inorganic polymerization reaction initiator in a homogeneous minimum-boiling binary azeotrope including a solvent and water, and conducting the polymerization in the azeotrope.
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