Method of monitoring and controlling activity involving a fuel composition
    21.
    发明申请
    Method of monitoring and controlling activity involving a fuel composition 审中-公开
    监测和控制涉及燃料组成的活动的方法

    公开(公告)号:US20140229010A1

    公开(公告)日:2014-08-14

    申请号:US14120068

    申请日:2014-04-22

    CPC classification number: G01N33/22

    Abstract: The method and apparatus are used to determine class, grade and properties of fuel samples, regardless of ambient, instrument, or sample temperature, using mathematical correlations between fuel class, grade and properties and their spectra developed from a database of samples with measured properties and spectra. The ability to measure a fuel sample using the present method and apparatus is useful in identifying unknown fuel samples, determining suitability in equipment, and monitoring and controlling fuel processes, such as blending operations, distillation, and synthesis.

    Abstract translation: 该方法和设备用于确定燃料样品的等级,等级和性能,无论环境,仪器或样品温度如何,使用燃料类别,等级和性质之间的数学相关性以及从具有测量性质的样品数据库开发的光谱,以及 光谱。 使用本方法和装置测量燃料样品的能力可用于识别未知燃料样品,确定设备的适用性,以及监测和控制燃料过程,例如混合操作,蒸馏和合成。

    Analysis method effected with rapid analyte chemical separation and quick detection
    22.
    发明授权
    Analysis method effected with rapid analyte chemical separation and quick detection 有权
    快速分析化学分离快速检测分析方法

    公开(公告)号:US08012763B2

    公开(公告)日:2011-09-06

    申请号:US12322158

    申请日:2009-01-29

    Abstract: A stationary medium is employed both to separate chemicals from a sample solution and also to generate surface-enhanced Raman scattering, so that spectral analysis of the separated analyte chemical can be performed. Applied driving force causes the sample to flow into the stationary medium and to distribute therethrough, thereby causing rapid separation of the analyte chemical, and surface-enhanced Raman scattered radiation is quickly detected, at a plurality of locations along a flow path defined by the stationary medium, for ultimate analysis.

    Abstract translation: 既采用固定介质将样品溶液中的化学物质分开,也可产生表面增强的拉曼散射,从而可以进行分离的分析物化学品的光谱分析。 施加的驱动力使得样品流入固定介质并分布在其中,从而导致分析物化学物质的快速分离,并且在沿着由静止物定义的流动路径的多个位置处快速检测到表面增强的拉曼散射辐射 中等,用于最终分析。

    Process control method for manufacturing polyolefin
    26.
    发明授权
    Process control method for manufacturing polyolefin 失效
    制造聚烯烃的工艺控制方法

    公开(公告)号:US5151474A

    公开(公告)日:1992-09-29

    申请号:US481020

    申请日:1990-02-16

    CPC classification number: B01J19/0006 C08F10/00 C08F2400/02

    Abstract: A process control method for controlling a polyolefin polymerization process, such as a solution polyethylene process, which includes five steps. The first step is to flow a stream of a solvent into a polyolefin reactor, such as flowing a stream of heptane solvent into the reactor at essentially a constant rate. The second step is to add a principal monomer to the stream of solvent, such as by adding ethylene at a controllable rate to the stream of solvent. The third step is to add a co-monomer to the stream of solvent, such as by adding 1-octene at a controllable rate to the stream of solvent. The fourth step is to determine the concentration of the principal monomer and the concentration of the co-monomer in the stream of solvent by high resolution multi-wavelength vibrational spectroscopy analysis, such as by Fourier transform infrared spectroscopy system having a spectral resolution of 4 wavenumbers which analyzes at 1909 wavenumbers for ethylene, at 1829 wavenumbers for 1-octene and at 2120 wavenumbers for a reference signal. The fifth step is to control the rate of addition of the principal monomer, the rate of addition of the comonomer or preferably the rate of addition of both the principal monomer and the co-monomer according to the determination of the fourth step to obtain the desired concentration of ethylene and 1-octene in the solvent so that, for example, the density of the polyolefin product can be controlled.

    Abstract translation: 用于控制聚烯烃聚合方法的过程控制方法,例如溶液聚乙烯方法,其包括五个步骤。 第一步是将溶剂流流入聚烯烃反应器中,例如以基本恒定的速率将庚烷溶剂流输入反应器。 第二步是将主要单体加入到溶剂流中,例如通过以可控速率向溶剂流中加入乙烯。 第三步是向溶剂流中加入共聚单体,例如通过以可控的速率向溶剂流中加入1-辛烯。 第四步是通过高分辨率多波长振动光谱分析来确定主要单体的浓度和溶剂流中共聚单体的浓度,例如通过具有4个波数的光谱分辨率的傅里叶变换红外光谱系统 其分析了1909年的乙烯波数,1829波数的1-辛烯和2120波数的参考信号。 第五步是根据第四步的测定来控制主要单体的加入速率,共聚单体的加入速率或优选加入主单体和共聚单体的速率以获得所需的 乙烯和1-辛烯在溶剂中的浓度使得例如可以控制聚烯烃产品的密度。

    Analysis method effected with rapid analyte chemical separation and quick detection
    27.
    发明申请
    Analysis method effected with rapid analyte chemical separation and quick detection 有权
    快速分析化学分离快速检测分析方法

    公开(公告)号:US20090168059A1

    公开(公告)日:2009-07-02

    申请号:US12322158

    申请日:2009-01-29

    Abstract: A stationary medium is employed both to separate chemicals from a sample solution and also to generate surface-enhanced Raman scattering, so that spectral analysis of the separated analyte chemical can be performed. Applied driving force causes the sample to flow into the stationary medium and to distribute therethrough, thereby causing rapid separation of the analyte chemical, and surface-enhanced Raman scattered radiation is quickly detected, at a plurality of locations along a flow path defined by the stationary medium, for ultimate analysis.

    Abstract translation: 既采用固定介质将样品溶液中的化学物质分开,也可产生表面增强的拉曼散射,从而可以进行分离的分析物化学品的光谱分析。 施加的驱动力使得样品流入固定介质并分布在其中,从而导致分析物化学物质的快速分离,并且在沿着由静止物定义的流动路径的多个位置处快速检测到表面增强的拉曼散射辐射 中等,用于最终分析。

    Method for quantitative surface-enhanced raman spectroscopy using a chemical reference
    30.
    发明申请
    Method for quantitative surface-enhanced raman spectroscopy using a chemical reference 审中-公开
    使用化学参考的定量表面增强拉曼光谱法的方法

    公开(公告)号:US20050266583A1

    公开(公告)日:2005-12-01

    申请号:US10854134

    申请日:2004-05-26

    CPC classification number: G01N21/658 G01N21/278

    Abstract: A method for obtaining quantitative surface-enhanced Raman (SER) spectra that corrects for deficiencies of, and variations in, the materials and devices employed, especially the SER-active media utilized, employs a reference chemical, having an effective surface-enhanced Raman factor, of known concentration within the same SER experimental field of view as the analyte chemical being measured. Knowledge of the relative amounts of SER-scattering for the reference chemical and analyte chemical allows calculating the concentration of the latter to a high degree of accuracy and precision.

    Abstract translation: 获得定量表面增强拉曼(SER)光谱的方法,其校正所用材料和装置的缺陷和变化,特别是所用的SER活性介质,采用具有有效表面增强拉曼因子的参考化学品 在与测量的分析物质相同的SER实验视野内具有已知浓度。 了解参考化学品和分析物化学品的SER散射的相对量,可以高精度和精确地计算后者的浓度。

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