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    ORGANOPHOSPHONATE OLIGOMERS
    22.
    发明申请
    ORGANOPHOSPHONATE OLIGOMERS 审中-公开
    有机磷酸酯低聚物

    公开(公告)号：US20100267871A1

    公开(公告)日：2010-10-21

    申请号：US12681885

    申请日：2008-10-16

    申请人： Techen Tsao ,  Arthur G. Mack ,  William J. Layman ,  Jeffrey Todd Aplin

    发明人： Techen Tsao ,  Arthur G. Mack ,  William J. Layman ,  Jeffrey Todd Aplin

    IPC分类号： C08K5/52 ,  C07F9/06

    CPC分类号： C07F9/091 ,  C07F9/093 ,  C07F9/4006 ,  C08J9/0038 ,  C08J2375/04 ,  C08K5/521 ,  C08L75/00

    摘要： This invention provides chlorohydrocarbyloxy phosphonate oligomers, organophosphonate oligomers, and processes for the preparation of such oligomers. The chlorohydrocarbyloxy phosphonate oligomers can be represented by the formula (IV) where R1 is a linear or branched hydrocarbylene group or oxygen-containing hydrocarbylene group, which hydrocarbylene group has about two to about twenty carbon atoms, or a hydrocarbylene group having at least one cycloaliphatic or aromatic ring; R2 is an alkyl group or an aromatic group; and n is a number from about 2 to about 20.

    摘要翻译： 本发明提供了氯代氧代膦酸酯低聚物，有机膦酸酯低聚物和制备这种低聚物的方法。 氯代氧代膦酸酯低聚物可以由式（IV）表示，其中R 1是亚烃基具有约2至约20个碳原子的直链或支链亚烃基或含氧亚烃基，或具有至少一个脂环族基团的亚烃基 或芳环; R2是烷基或芳基; n为约2至约20的数。

    Flame Retardant Additive Compositions and Use Thereof
    24.
    发明申请
    Flame Retardant Additive Compositions and Use Thereof 审中-公开
    阻燃添加剂组合物及其用途

    公开(公告)号：US20090143494A1

    公开(公告)日：2009-06-04

    申请号：US12293496

    申请日：2007-04-03

    申请人： Arthur G. Mack ,  Hoover B. Chew

    发明人： Arthur G. Mack ,  Hoover B. Chew

    IPC分类号： C09K21/14 ,  C08J9/02 ,  C09K3/00

    CPC分类号： C09K21/12 ,  C08G18/4607 ,  C08G2101/0008 ,  C08K5/12 ,  C08K5/523 ,  C08K5/5357

    摘要： Improved flame retardant additives are formed from (A) at least one bis(alkanoic acid ester) of a ring-brominated aromatic diester diol; (B) liquid alkylated triphenyl phosphate having an approximate average formula (RxPhO)3P═O) in which each R is, independently, a hydrogen atom or a C14 alkyl group and x is an average number in the range of about 0.2 to 3; and (C) at least one alicyclic phosphonate ester having 1, 2 or 3 phosphorus atoms in the molecule, at least one of which is part of an alicyclic ring system, and having a phosphorus content of at least about 15 wt %. Combinations of these components are well-suited for use in various polymers or resins, especially polyurethanes.

    摘要翻译： 改进的阻燃添加剂由（A）至少一种环 - 溴化芳族二酯二醇的双（链烷酸酯）形成; （B）具有近似平均式（RxPhO）3 P-O）的液体烷基化三苯基磷酸酯，其中每个R独立地是氢原子或C14烷基，x是约0.2-3的平均数; 和（C）至少一种在分子中具有1,2或3个磷原子的脂环族膦酸酯，其中至少一种是脂环族体系的一部分，并且具有至少约15重量％的磷含量。 这些组分的组合非常适用于各种聚合物或树脂，特别是聚氨酯。

    PROCESSING OF SOLID BROMINATED AROMATIC ORGANIC COMPOUNDS CONTAINING OCCLUDED BROMINE
    25.
    发明申请
    PROCESSING OF SOLID BROMINATED AROMATIC ORGANIC COMPOUNDS CONTAINING OCCLUDED BROMINE 失效
    含有固体溴化物的芳香族有机化合物的处理

    公开(公告)号：US20080114195A1

    公开(公告)日：2008-05-15

    申请号：US11840302

    申请日：2007-08-17

    申请人： Saadat Hussain ,  Arthur G. Mack

    发明人： Saadat Hussain ,  Arthur G. Mack

    IPC分类号： C07C25/18 ,  C07C17/23

    CPC分类号： C07C17/38 ,  C07C25/18 ,  C07C41/34 ,  C07C43/29 ,  C09K21/08

    摘要： Solid-state highly brominated compounds such as solid brominated flame retardants with bromine contents of at least about 60 wt % often contain occluded bromine. Because of their high bromine contents, such compounds have relatively low solubility in common organic solvents. Despite this low solubility, the content of occluded bromine in such solid brominated compounds is effectively reduced by agitating a concentrated agitated slurry of the compound in an inert solvent at a suitable temperature for at least about 1 hour. Thereafter, solids with reduced content of occluded bromine are isolated or recovered from the slurry. Novel products having substantially reduced or eliminated occluded bromine contents and other very desirable characteristics are also provided.

    摘要翻译： 固态高度溴化的化合物，例如溴含量至少约60wt％的固体溴化阻燃剂通常含有阻塞的溴。 由于溴含量高，所以这些化合物在常见的有机溶剂中的溶解度相对较低。 尽管这种低溶解度，但是通过在惰性溶剂中在合适的温度下搅拌化合物的浓缩的搅拌浆料至少约1小时，可以有效地降低这些固体溴化化合物中封闭的溴的含量。 此后，从浆液中分离或回收含有减少的阻塞溴含量的固体。 还提供了具有显着降低或消除了阻塞的溴含量和其它非常理想特性的新产品。

    Efficient methods for making tetrahalophthalate esters having excellent purity
    26.
    发明授权
    Efficient methods for making tetrahalophthalate esters having excellent purity 有权
    制备具有优异纯度的四卤代邻苯二甲酸酯的高效方法

    公开(公告)号：US6150552A

    公开(公告)日：2000-11-21

    申请号：US343316

    申请日：1999-06-30

    申请人： Jeffrey A. Schreier ,  James D. Siebecker ,  Arthur G. Mack

    发明人： Jeffrey A. Schreier ,  James D. Siebecker ,  Arthur G. Mack

    IPC分类号： C07C67/08 ,  C07C67/48 ,  C07C69/76 ,  C08K5/09

    CPC分类号： C07C67/08 ,  C07C67/48

    摘要： Provided are methods for the preparation and purification of alkyl tetrahalophthalate esters by the reaction of a tetrahalophthalic compound with an alkanol in the presence of a titanate catalyst. More particularly, improved methods are provided for making and recovering an ester with little contamination by catalytic metal components and color bodies, and with little acidity, in a high yield from the esterification reaction by pretreating the starting materials to reduce the acidity thereof, reacting the starting materials in the presence of a titanate catalyst, stripping excess alcohol, hydrolyzing the catalyst, and filtering out solids to yield a high purity tetrahalophthalate ester product.

    摘要翻译： 本发明提供了在钛酸酯催化剂存在下通过四卤代邻苯二甲酸化合物与链烷醇的反应来制备和纯化四卤代烷基酯的方法。 更具体地，提供了通过预处理起始原料以降低其酸度，通过酯化反应以高产率从而催化金属组分和着色体几乎没有污染并且几乎没有酸性的酯的制备和回收的改进方法， 在钛酸酯催化剂的存在下起始原料，汽提过量的醇，水解催化剂，过滤出固体，得到高纯度的四卤代邻苯二甲酸酯产物。

    Reduced methyl bromide process for making tetrabromobisphenol-A
    28.
    发明授权
    Reduced methyl bromide process for making tetrabromobisphenol-A 失效
    降低制备四溴双酚A的甲基溴工艺

    公开(公告)号：US5446212A

    公开(公告)日：1995-08-29

    申请号：US302541

    申请日：1994-09-08

    申请人： Dave C. Sanders ,  Arthur G. Mack ,  Larry D. Timberlake

    发明人： Dave C. Sanders ,  Arthur G. Mack ,  Larry D. Timberlake

    IPC分类号： C07C37/62 ,  C07C39/16 ,  C07C39/367

    CPC分类号： C07C37/62

    摘要： A reduced methyl bromide process for making tetrabromobisphenol A in methanol, including: dissolving bisphenol-A in a methanol solvent to form a bisphenol-A methanol solution, adding bromine to the bisphenol-A methanol solution to brominate bisphenol-A and form tetrabromobisphenol A and hydrogen bromide, exposing the bisphenol-A methanol solution to an amount of a hydrogen peroxide agent to reduce the amount of methyl bromide co-product resulting from the bromination of bisphenol-A in methanol by reducing the amount of hydrogen bromide co-product available to react with the methanol, and collecting the resulting tetrabromobisphenol A product thus formed after the bromination is substantially complete.

    摘要翻译： 在甲醇中制备四溴双酚A的还原甲基溴方法，包括：将双酚A溶解在甲醇溶剂中以形成双酚A甲醇溶液，向双酚A甲醇溶液中加入溴以溴化双酚A并形成四溴双酚A和 溴化氢，将双酚A甲醇溶液暴露于一定量的过氧化氢试剂，以减少由甲醇中双酚A溴化而产生的甲基溴共同产物的量，通过减少可用的溴化氢共同产物的量 与甲醇反应，收集溴化后所形成的四溴双酚A产物基本上完成。