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    CRYSTALLINE FORMS OF 1-(1,2-DIMETHYLPROPYL)-N-ETHYL-5-METHYL-N-PYRIDAZIN-4-YL-PYRAZOLE-4-CARBOXAMIDE
    23.
    发明申请
    CRYSTALLINE FORMS OF 1-(1,2-DIMETHYLPROPYL)-N-ETHYL-5-METHYL-N-PYRIDAZIN-4-YL-PYRAZOLE-4-CARBOXAMIDE 有权

    公开(公告)号：US20220024898A1

    公开(公告)日：2022-01-27

    申请号：US17311403

    申请日：2020-01-10

    Applicant: BASF SE

    Inventor： Joachim Gebhardt ,  Martin Viertelhaus ,  Tiziana Chiodo ,  Michael Rack ,  Eric George Klauber ,  Wen Xu ,  Roland Goetz ,  Florian Vogt ,  Birgit Gockel ,  Sebastian Soergel

    IPC: C07D403/12 ,  A01N43/58 ,  A01P7/04

    Abstract: The present invention relates to a novel crystalline form of 1-(1,2-dimethylpropyl)-N-ethyl-5-methyl-N-pyridazin-4-yl-pyrazole-4-carboxamide recently assigned the common name dimpropyridaz. The invention also relates to the use of the crystalline form B for combating invertebrate pests and to formulations for plant protection which contain the crystalline form B of 1-(1,2-dimethylpropyl)-N-ethyl-5-methyl-N-pyridazin-4-yl-pyrazole-4-carboxamide. The crystalline form B according to the present invention can be identified by powder X-ray diffractometry on the basis of its powder X-ray diffraction diagram, hereinafter also termed powder X-ray diffraction pattern or PXRD pattern, of the polymorph form B recorded using Cu—Kα radiation (1.54178 Å) at 25° C. displays the 3 following reflections, quoted as 2θ values: 20.69±0.10°, 24.15±0.10° and 30.52±0.10°. In addition to these 3 reflections, the polymorph B of the present invention may display in such a PXRD pattern one or more, in particular at least 2, often at least 4, in particular at least 6 or at least 8 reflections and especially all of the reflections quoted hereinafter as 2θ values: 7.99±0.10°, 10.07±0.10°, 12.38±0.10°, 15.31±0.10°, 15.97±0.10°, 16.50±0.10°, 18.03±0.10°, 19.29±0.10°, 20.22±0.0.10°, 20.96±0.10°, 23.40±0.10°, 23.70±0.10°, 26.09±0.10°, 27.26±0.10° and 32.91±0.10°.

    Diaminotriazine derivatives as herbicides
    30.
    发明授权
    Diaminotriazine derivatives as herbicides 有权

    公开(公告)号：US10941122B2

    公开(公告)日：2021-03-09

    申请号：US15302681

    申请日：2015-04-09

    Applicant: BASF SE

    Inventor： Julia Major ,  Florian Vogt ,  Frederick Calo ,  Thomas Seitz ,  Doreen Schachtschabel ,  Trevor William Newton ,  Kristin Hanzlik ,  Johannes Hutzler ,  Klaus Kreuz ,  Stefan Tresch

    IPC: C07D251/18 ,  A01N43/68 ,  C07D251/48

    Abstract: The present invention relates to diaminotriazine compounds of the formula (I) and to their use as herbicides. The present invention also relates to agrochemical compositions for crop protection and to a method for controlling unwanted vegetation. wherein q is 0, 1, 2 or 3 Ra is selected from the group consisting of C1-C6-haloalkoxy, C1-C6-haloalkylthio, (C1-C6-haloalkyl)sulfinyl, (C1-C6-haloalkyl)-carbonyl, etc.; Rb is selected from the group consisting of halogen, OH, CN, amino, NO2, C1-C6-alkyl, C2-C6-alkenyl, C2-C6-alkynyl, C1-C6-alkoxy, etc.; R1 is selected from the group consisting of H, OH, S(O)2NH2, CN, C1-C6-alkyl, C2-C6-alkenyl, C2-C6-alkynyl, (C3-C6-cycloalkyl)-C1-C4-alkyl, etc.; R2 is selected from the group consisting of H, OH, S(O)2NH2, CN, C1-C6-alkyl, C2-C6-alkenyl, C2-C6-alkynyl, (C3-C6-cycloalkyl)-C1-C4-alkyl, etc.; R3 is selected from the group consisting of H, halogen, OH, CN, C1-C6-alkyl, (C1-C6-alkoxy)-C1-C6-alkyl, C3-C6-cycloalkyl, etc.; R4 is H, halogen, CN, C1-C6-alkyl, C1-C6-haloalkyl, C3-C6-cycloalkyl, C3-C6-halocycloalkyl, C1-C6-alkoxy and C1-C6-haloalkoxy; R5 is selected from the group consisting of halogen, CN, C1-C6-alkyl, C2-C6-alkenyl, C3-C6-alkynyl, C3-C6-cycloalkyl, etc.; or R4 and R5 together with the carbon atom to which they are attached form a moiety selected from the group consisting of carbonyl, C3-C6-cycloalkan-1,1-diyl, ipso-C3-C6-cycloalkendiyl, three- to six-membered saturated or partially unsaturated ipso-heterocyclodiyl; including their agriculturally acceptable salts.

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