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公开(公告)号:US20200375193A1
公开(公告)日:2020-12-03
申请号:US16999935
申请日:2020-08-21
Applicant: Calix Ltd
Inventor: Mark Sceats , Philip Hodgson
Abstract: A formulation of a pathogen inhibitor or probiotic as a slurry concentrate of a hydrated metal oxide for applications in agriculture, aquaculture, and as an antibiotic in which the bioactivity, when applied by dilution, is controlled by a precursor of Reactive Oxygen Species, and the release rate is controlled by the particle size. The invention may include a means whereby the precursor concentration may be controlled to meet the requirements of the ecosystem, from the maintenance of an aerobic system, to killing pathogenic, anaerobic microbes, or producing sterile ecosystems. In addition, the metal oxide may be selected to provide essential nutrients for growth of the agricultural or aquacultural products.
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公开(公告)号:US20200317549A1
公开(公告)日:2020-10-08
申请号:US16908361
申请日:2020-06-22
Applicant: Calix Ltd
Inventor: Mark Sceats , Adam Vincent
Abstract: A method of manufacture of high-solids hydroxide slurries from caustic calcined carbonate powder is described, whereby the properties of the slurry are its low resistance to shear thinning to facilitate transport, a high stability for transport and storage, ease of reconstitution after long periods of storage, and, as required, a high concentration of chemically reactive species at the particle surface. The method achieves these specifications by mixing caustic calcined carbonate or hydroxide powder with water in an insulated reactor vessel, and agitating the slurry sufficiently such that the hydration reaction causes the water to spontaneously boil, such that the remaining hydration proceeds spontaneously under the fixed conditions of boiling through the water loss. The mixing process is preferably carried out by a shear pump. A viscosity modifier, such as acetic acid, is used to thin the slurry to enable the mixing system to maintain uniform mixing. The reaction is terminated when the boiling has spontaneously ceased and the temperature has spontaneously dropped to a set point though the reactor heat losses, where the processing time is sufficiently long that the slurry meets the desired specifications.
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公开(公告)号:US20190275485A1
公开(公告)日:2019-09-12
申请号:US16345474
申请日:2017-10-27
Applicant: CALIX LTD
Inventor: Mark Sceats , Philip Hodgson , Adam Vincent , Simon Thomsen , Matthew Gill , Daniel Rennie
Abstract: A method and system for producing nano-active powder materials. The method can be used with a reactor system comprising stages in which input particles flow under gravity progressively through stages of the reactor. A powder injector first stage in which ground input precursor powder is injected into the reactor. An externally heated preheater stage may be in the reactor, in which the precursor powder is heated to a temperature of calcination reaction. An externally heated calciner stage in the reactor, in which primary precursor volatile constituents can be rapidly removed calcination reactions as a high purity gas stream to produce the desired nano-active product. A post-processing reactor stage in which there is a change of the gas stream composition to produce the desired hot powder product by virtue of the nano-activity of the first powder material. A powder ejector stage in which the hot powder product is ejected from the reactor.
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公开(公告)号:US20190177194A1
公开(公告)日:2019-06-13
申请号:US16282094
申请日:2019-02-21
Applicant: Calix Ltd
Inventor: Mark Sceats , Adam Vincent
CPC classification number: C02F1/68 , B01J13/0008 , B01J19/1881 , B01J2219/00121 , B01J2219/00168 , B01J2219/00186 , B01J2219/00189 , C01B13/14 , C01F5/16 , C02F1/5236 , C02F1/66 , C02F2101/20 , C02F2103/005 , C02F2303/02 , C02F2303/04 , C04B2/04
Abstract: A method of manufacture of high-solids hydroxide slurries from caustic calcined carbonate powder is described, whereby the properties of the slurry are its low resistance to shear thinning to facilitate transport, a high stability for transport and storage, ease of reconstitution after long periods of storage, and, as required, a high concentration of chemically reactive species at the particle surface. The method achieves these specifications by mixing caustic calcined carbonate or hydroxide powder with water in an insulated reactor vessel, and agitating the slurry sufficiently such that the hydration reaction causes the water to spontaneously boil, such that the remaining hydration proceeds spontaneously under the fixed conditions of boiling through the water loss. The mixing process is preferably carried out by a shear pump. A viscosity modifier, such as acetic acid, is used to thin the slurry to enable the mixing system to maintain uniform mixing. The reaction is terminated when the boiling has spontaneously ceased and the temperature has spontaneously dropped to a set point though the reactor heat losses, where the processing time is sufficiently long that the slurry meets the desired specifications.
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公开(公告)号:US09913475B2
公开(公告)日:2018-03-13
申请号:US15106759
申请日:2014-12-10
Applicant: Calix Ltd
Inventor: Mark Sceats
CPC classification number: A01N59/06 , A01N25/12 , B01J21/10 , B01J35/026 , B01J35/1019 , B82Y40/00 , C01F5/06 , C01P2004/61 , C01P2006/12 , C04B2/102 , C04B2/106 , A01N25/04
Abstract: A process and apparatus for manufacture of oxide products for use as biocide, chemical detoxifying, and catalytic support products, from caustic calcined carbonate powder, preferably from magnesite, dolomite, or hydromagnesite, is described. These oxide particles are characterized by high surface area, high porosity and a high degree of calcination, and the method of manufacture utilizes an indirectly heated counterflow reactor. The oxides may be used as a powder, granules, or formulated into a slurry and used as a spray, emulsion, foam or fog, or the powder product may be directly applied. Also described is the formation of particles with microstructures defined by at least one nano-crystalline structure positioned on the outer surface of the particles.
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