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    Mixtures of bleaching agents
    21.
    发明授权
    Mixtures of bleaching agents 有权
    漂白剂的混合物

    公开(公告)号：US07504372B2

    公开(公告)日：2009-03-17

    申请号：US11662305

    申请日：2005-09-03

    Applicant: Gerd Reinhardt ,  Georg Borchers

    Inventor： Gerd Reinhardt ,  Georg Borchers

    IPC: C11D10/00

    CPC classification number: C11D3/3935 ,  C11D3/3917 ,  C11D3/392 ,  C11D3/3945

    Abstract: What are claimed are synergistically active bleach mixtures consisting ofa) a compound of the formula (1) in which n is 3, 4 or 5, and b) tetraacetylethylenediamine and/or 1,5-diacetyl-2,4-dioxo-1,3,5-hexa-hydrotriazine.

    Abstract translation: 所要求的是协同活性漂白混合物，其由a）式（1）的化合物组成，其中n为3,4或5，b）四乙酰基乙二胺和/或1,5-二乙酰基-2,4-二氧代-1 ，3,5-hexa-hydrotriazine。

    Use of transition metal complexes as bleach catalysts in laundry detergents and cleaning compositions
    22.
    发明授权
    Use of transition metal complexes as bleach catalysts in laundry detergents and cleaning compositions 失效
    过渡金属配合物作为漂白催化剂在衣物洗涤剂和清洁组合物中的应用

    公开(公告)号：US07205267B2

    公开(公告)日：2007-04-17

    申请号：US11041468

    申请日：2005-01-24

    Applicant: Gerd Reinhardt ,  Ekaterina Jonas

    Inventor： Gerd Reinhardt ,  Ekaterina Jonas

    IPC: C11D3/26 ,  C11D3/28 ,  C11D3/39 ,  C11D3/395

    CPC classification number: C11D3/168 ,  C11D3/3932

    Abstract: The use is claimed of transition metal complexes of the formula (I) [M(L)Yn]Xm  (I) where M is a metal atom from the group of Mn and Fe, L is a ligand of the general formula (II) or (III) where R1, R2, R3 and R4 are the same or different and are each H, C1–C8-alkyl or C6–C12-alkaryl; X and Y are each an uncharged or anionic ligand from the group of CH3CN, chloride, bromide, nitrate, perchlorate, sulfate, citrate, hexafluorophosphate, trifluoromethanesulfonate, tetrafluoroborate, tetraphenylborate or an anion of organic acids having C1–C22 carbon atoms, n and m are each a number from 0 to 4 as bleach catalysts in laundry detergents and cleaning compositions.

    Abstract translation: 要求使用下式的过渡金属络合物

    Process for the preparation of acyloxybenzenesulfonic acids and their salts
    28.
    发明授权
    Process for the preparation of acyloxybenzenesulfonic acids and their salts 失效
    制备乙酰苯二酚酸及其盐的方法

    公开(公告)号：US5100588A

    公开(公告)日：1992-03-31

    申请号：US154057

    申请日：1988-02-09

    Applicant: Fritz-Feo Grabley ,  Gerd Reinhardt ,  Roland Steinl

    Inventor： Fritz-Feo Grabley ,  Gerd Reinhardt ,  Roland Steinl

    IPC: C07C309/42 ,  C07C20060101 ,  C07C67/00 ,  C07C301/00 ,  C07C303/02 ,  C07C303/04 ,  C07C303/06 ,  C07C303/14 ,  C07C303/30 ,  C07C303/32 ,  C07C309/58 ,  C11D1/22 ,  C11D3/34

    CPC classification number: C07C309/00

    Abstract: The process for the preparation of acyloxybenzenesulfonic acids of the general formula ##STR1## in which R denotes a (C.sub.1 -C.sub.17)-alkyl or (C.sub.2 -C.sub.17)-alkenyl radical, or alkali metal, alkaline earth metal or ammonium salts thereof, is carried out in the following stages: (a) sulfonation of phenol, (b) heat treatment of the phenolsulfonic acid formed as the intermediate product, (c) esterification of the phenolsulfonic acid and, if appropriate, (d) neutralization of the resulting (C.sub.2 -C.sub.18)-acyloxybenzenesulfonic acid. As a result of the incorporation of stage (b), the process affords products in which the proportion of the 1,4-isomer compared with the 1,2-isomer is markedly increased, as a result of which these products can be used, in particular, as perborate activators in detergents.

    Abstract translation: 其中R表示（C1-C17） - 烷基或（C2-C17） - 烯基或其碱金属，碱土金属或铵盐的通式为“IMAGE”的酰氧基苯磺酸的制备方法为 在以下阶段进行：（a）苯酚的磺化，（b）作为中间产物形成的酚磺酸的热处理，（c）苯酚磺酸的酯化，如果合适的话，（d）中和所得的（ C2-C18） - 酰氧基苯磺酸。 作为阶段（b）的结合，该方法提供了与1,2-异构体相比的1,4-异构体的比例显着增加的产物，由此可以使用这些产物， 特别是作为洗涤剂中的过硼酸盐活化剂。

    Bleach catalyst compounds, method for the production thereof and use thereof
    29.
    发明授权
    Bleach catalyst compounds, method for the production thereof and use thereof 有权
    漂白催化剂化合物，其制备方法和用途

    公开(公告)号：US08889611B2

    公开(公告)日：2014-11-18

    申请号：US13513729

    申请日：2010-11-30

    Applicant: Gerd Reinhardt ,  Michael Best

    Inventor： Gerd Reinhardt ,  Michael Best

    IPC: C11D7/26 ,  C11D7/32 ,  C11D7/54 ,  C07F13/00 ,  C11D17/06 ,  C11D17/00 ,  C11D3/16 ,  C11D3/39 ,  D21C9/10 ,  D21C9/16

    CPC classification number: C07F13/005 ,  C11D3/168 ,  C11D3/3932 ,  C11D17/0052 ,  C11D17/06 ,  C11D17/065 ,  D21C9/10 ,  D21C9/163

    Abstract: The invention relates to compounds in solid form, containing a) one or more manganese complex compounds of the general formula (1), where M is independently selected from manganese in the III or IV oxidation state, X is independently a co-ordinating or bridging species selected from H2O, O22−, O2−, O2−, OH−, HO2−, SH−, S2−, SO, Cl−, N3−, SCN−, N3−, RCOO−, NH2− and NR3, where R is a radical selected from H, alkyl and aryl, L are independently organic ligands, each of which contains at least two nitrogen atoms co-ordinated on manganese, z is an integer from −4 to +4, Y is a monovalent or multivalent counter-ion selected from chloride, sulphate, hydrogen sulphate, nitrate and acetate, which leads to charge neutrality of the complex, and q is an integer from 1 to 4, and b) one or more salts of the general formula R′—C6H4—SO3Me, where R′ is CH3 or C2H5 and denotes Me, Na, K, Ca or Mg, characterized in that the molar ratio of the manganese complex compound of the general formula (1) to salt of the general formula R′—C6H4—SO3Me is 1:0.5 to 1:5. The invention also describes a method for producing the compounds and to the use thereof as oxidation catalysts or bleach catalysts, in particular in detergents or cleaning agents.

    Abstract translation: 本发明涉及固体形式的化合物，其包含a）一种或多种通式（1）的锰络合物，其中M独立地选自III或IV氧化态的锰，X独立地为配位或桥接 选自H2O，O22-，O​​2-，O2-，OH-，HO2-，SH-，S2-，SO，Cl-，N3-，SCN-，N3-，RCOO-，NH2-和NR3的物质，其中R 是选自H，烷基和芳基的基团，L独立为有机配体，每个含有至少两个在锰上配位的氮原子，z为-4至+4的整数，Y为单价或多价计数器 其选自氯化物，硫酸盐，硫酸氢盐，硝酸盐和乙酸盐，这导致络合物的电荷中性，q是1至4的整数，b）一种或多种通式R'-C6H4- SO 3 Me，其中R'是CH 3或C 2 H 5，并且表示Me，Na，K，Ca或Mg，其特征在于锰络合物 通式（1）表示的化合物与通式R'-C6H4-SO3Me的盐为1:0.5至1:5。 本发明还描述了一种制备化合物的方法及其用作氧化催化剂或漂白催化剂的用途，特别是在洗涤剂或清洁剂中。

    Method for producing 3,7-diaza-bicyclo[3.3.1]nonane metal complexes
    30.
    发明授权
    Method for producing 3,7-diaza-bicyclo[3.3.1]nonane metal complexes 有权
    制备3,7-二氮杂双环[3.3.1]壬烷金属络合物的方法

    公开(公告)号：US08846921B2

    公开(公告)日：2014-09-30

    申请号：US13877567

    申请日：2011-10-06

    Applicant: Christian Sidot ,  Audrey Caron ,  Miriam Ladwig ,  Gerd Reinhardt

    Inventor： Christian Sidot ,  Audrey Caron ,  Miriam Ladwig ,  Gerd Reinhardt

    IPC: C07F15/02 ,  C07F13/00

    CPC classification number: C07F15/02 ,  C07F13/00 ,  C07F13/005 ,  C07F15/025

    Abstract: The invention relates to a method for producing metal complexes of formula (2) [MaLxXn]Ym (2), where M is a metal from the group consisting of Mn(II), Mn(III), Mn(IV), Fe(II), Fe(III) or Fe(IV), X is a coordinating compound selected from mono-, bi- or tri-charged anions or neutral molecules which can coordinate to a metal in mono-, bi- or tri-dentate form, Y represents a non-coordinating counter-ion which ensures charge equalization of the complex, L represents a ligand of formula (1) or the protonized or de-protonized form thereof, and a, x, n, m, R, R1, R2, R3 and z have the meanings described in claim 1. Said method is characterized in that the reaction of one or more ligands of formula (1) with an iron salt or manganese salt is carried out in an acetone/water mixture in a temperature range from 0 to 50° C. and for this purpose a solution or a suspension of the one or more ligands of formula (1) in acetone is brought in contact with an aqueous metal salt solution of the iron salt or manganese salt in the temperature range in which the reaction takes place.

    Abstract translation: 本发明涉及一种制备式（2）[MaLxXn] Ym（2）的金属配合物的方法，其中M是由Mn（II），Mn（III），Mn（IV），Fe（ II），Fe（III）或Fe（IV），X是选自单，双或三电荷阴离子或中性分子的配位化合物，其可以以单，双或三齿形式与金属配位 ，Y表示非配位抗衡离子，其确保络合物的电荷均衡，L表示式（1）的配体或其质子化或去质子化形式，和a，x，n，m，R，R 1， R2，R3和z具有权利要求1所述的含义。所述方法的特征在于，式（1）的一种或多种配体与铁盐或锰盐的反应在丙酮/水混合物中在温度 范围为0至50℃，为此目的，将式（1）的一种或多种配体在丙酮中的溶液或悬浮液与铁盐水溶液的金属盐溶液接触 r锰盐在发生反应的温度范围内。

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