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    Maleic acid based copolymer and its production process and use
    21.
    发明授权
    Maleic acid based copolymer and its production process and use 失效
    马来酸共聚物及其制备方法及用途

    公开(公告)号：US5733857A

    公开(公告)日：1998-03-31

    申请号：US277528

    申请日：1994-07-19

    申请人： Shigeru Yamaguchi ,  Keishi Tsuboi ,  Yoshio Irie

    发明人： Shigeru Yamaguchi ,  Keishi Tsuboi ,  Yoshio Irie

    IPC分类号： C02F1/56 ,  C08F222/02 ,  C09D17/00 ,  C11D3/37 ,  C11D17/04 ,  C11D17/06 ,  D06L1/12 ,  D06L3/02 ,  D06M15/263 ,  D06P1/52 ,  C08F222/06

    CPC分类号： C11D17/041 ,  C02F1/56 ,  C08F222/02 ,  C09D17/004 ,  C11D17/065 ,  C11D3/3757 ,  D06L1/12 ,  D06L3/021 ,  D06M15/263 ,  D06P1/5257 ,  Y10S516/06

    摘要： A maleic acid-based copolymer is provided which has a weight-average molecular weight of 1,000 to 100,000, a calcium ion-capturability of 300 mgCaCO.sub.3 /g or higher calculated as calcium carbonate, and a clay-dispersibility of 1.2 or higher. Another maleic acid-based copolymer is also provided which has a level of adsorption to clay within the range of 20 to 90% and a calcium ion-stabilization degree constant of 4.0 or larger. These copolymers are obtainable by a process including the steps of: charging maleic acid and/or its salt (A) into a reaction vessel, in such a manner that the concentration of the (A) will be 35% by weight or higher; adding hydrogen peroxide into the vessel after the charging step, in such a manner that the amount of hydrogen peroxide is within the range of 3 to 20% by weight of the (A); and adding a water-soluble ethylenically unsaturated monomer (B) into the vessel after the charging step and within 30 to 500 minutes after initiation of a reaction, in such a manner that the ratio (A)/(B) is within the range of 95/5 to 5/95 in mol ratio, wherein the adding of the monomer (B) is completed 10 to 300 minutes later than completion of the step of adding hydrogen peroxide. The copolymers are used for detergent compositions, inorganic pigment-dispersing agents, water-treating agents and fiber-treating agents.

    摘要翻译： 提供了一种马来酸基共聚物，其重均分子量为1,000至100,000，钙离子捕获性为300mgCaCO 3 / g或更高，以碳酸钙计算，粘土分散性为1.2或更高。 还提供另一种马来酸基共聚物，其具有在20至90％范围内对粘土的吸附水平和4.0或更大的钙离子稳定度常数。 这些共聚物可以通过以下步骤获得：包括以下步骤：将马来酸和/或其盐（A）装入反应容器中，使得（A）的浓度为35重量％以上; 在充电步骤之后，将过氧化氢加入到容器中，使得过氧化氢的量在（A）的3至20重量％的范围内; 在充电步骤之后并在反应开始后的30〜500分钟内向容器中加入水溶性烯属不饱和单体（B），使得（A）/（B）的比例在 95/5〜5/95摩尔比，其中，单体（B）的添加比完成加入过氧化氢步骤后10〜300分钟完成。 共聚物用于洗涤剂组合物，无机颜料分散剂，水处理剂和纤维处理剂。

    Method for drying granular water-containing gel-like cross-linked polymer
    24.
    发明授权
    Method for drying granular water-containing gel-like cross-linked polymer 有权
    颗粒状含水凝胶状交联聚合物的干燥方法

    公开(公告)号：US08875415B2

    公开(公告)日：2014-11-04

    申请号：US13583144

    申请日：2011-03-07

    申请人： Yoshio Irie

    发明人： Yoshio Irie

    IPC分类号： C08F6/06 ,  C08F6/00 ,  B01J2/26 ,  C08L33/02 ,  C08F22/02 ,  B01D1/24 ,  A61L15/22 ,  A61L15/60 ,  C08J3/12

    CPC分类号： C08F6/008 ,  A61L15/22 ,  A61L15/60 ,  B01D1/24 ,  B01J2/26 ,  C08F22/02 ,  C08J3/12 ,  C08J2300/14 ,  C08L33/02 ,  C08L33/06

    摘要： The present invention is to provide a drying method by which both cost reduction and superior physical properties can be attained in a step which comprises subjecting a water-containing gel-like crosslinked polymer obtained by polymerizing an aqueous monomer solution to fine granulation during or after the polymerization, and drying the resultant particulate water-containing gel-like crosslinked polymer with a through-circulation band dryer. The method has a feature in that the drying conditions over a period from a time of introducing the particulate water-containing gel-like crosslinked polymer into a drying zone of the through-circulation band dryer to a time of reaching a solid content concentration thereof to 80% by weight, satisfy that (1) a difference of temperature between a temperature of hot air blown to a particulate hydrogel layer and a temperature measured after the hot air passes through the particulate hydrogel layer is 20 to 70° C.

    摘要翻译： 本发明提供一种干燥方法，其可以在以下步骤中实现成本降低和物理性能优异的步骤：将含有单体溶液聚合得到的含水凝胶状交联聚合物在 聚合，并用通过循环带式干燥器干燥得到的含颗粒状含水凝胶状交联聚合物。 该方法的特征在于，在将含颗粒状含水凝胶状交联聚合物引入通循环带式干燥机的干燥区域到达固体成分浓度的时间的期间内的干燥条件为 80重量％，满足以下（1）吹送到颗粒状水凝胶层的热空气的温度与热空气通过颗粒状水凝胶层后测量的温度之间的温度差为20〜70℃。

    Water-absorbent composition, process for production thereof, absorbent and absorbing product
    25.
    发明授权
    Water-absorbent composition, process for production thereof, absorbent and absorbing product 有权
    吸水剂组合物，其制造方法，吸收和吸收产品

    公开(公告)号：US07825169B2

    公开(公告)日：2010-11-02

    申请号：US10448456

    申请日：2003-05-30

    申请人： Katsuyuki Wada ,  Hiroko Ueda ,  Kunihiko Ishizaki ,  Yoshio Irie ,  Yasuhisa Nakashima

    发明人： Katsuyuki Wada ,  Hiroko Ueda ,  Kunihiko Ishizaki ,  Yoshio Irie ,  Yasuhisa Nakashima

    IPC分类号： A61L9/013

    CPC分类号： A61L15/60 ,  A61F13/8405 ,  A61L9/01 ,  A61L15/40 ,  B01J20/267 ,  B01J2220/4875

    摘要： A water-absorbent composition includes: a specific plant extract; a water-absorbent resin whose surface portion and/or periphery thereof is treated; and/or a water-absorbent resin having a specific property. Specifically, it is preferable to use a water-absorbent resin having three characteristics: (1) a specific neutralization rate, (2) a specific particle diameter, and (3) a specific plant extract. The water-absorbent composition has a superior deodorant performance and an absorbent characteristic when the water-absorbent composition is used (provided) in an absorbing product such as a paper diaper, thereby providing a superior deodorant performance and a superior absorbent characteristic to the foregoing absorbing product.

    摘要翻译： 吸水组合物包括：特定植物提取物; 其表面部分和/或其周边被处理的吸水性树脂; 和/或具有特定性质的吸水性树脂。 具体而言，优选使用具有三个特征的吸水性树脂：（1）特定中和率，（2）特定粒径，和（3）特定植物提取物。 吸水性组合物在纸尿布等吸收体中使用（设置）吸水性组合物时具有优异的除臭性能和吸收特性，从而为上述吸收性物质提供优异的除臭性能和优异的吸收特性 产品。

    Production method for hydrophilic polymer
    26.
    发明授权
    Production method for hydrophilic polymer 有权
    亲水性聚合物的生产方法

    公开(公告)号：US07816445B2

    公开(公告)日：2010-10-19

    申请号：US11638580

    申请日：2006-12-14

    申请人： Yorimichi Dairoku ,  Yoshiro Mitsukami ,  Yoshio Irie ,  Shin-ichi Fujino

    发明人： Yorimichi Dairoku ,  Yoshiro Mitsukami ,  Yoshio Irie ,  Shin-ichi Fujino

    IPC分类号： C08L33/02

    CPC分类号： C08F2/20 ,  C08F2/22 ,  C08F220/06 ,  C08F222/1006 ,  C08J3/245 ,  C08J2333/02

    摘要： The subject invention provides a hydrophilic polymer (water-absorbing resin) which is superior in performance and productivity. According to the production method of the present invention, a hydrophilichigh-molecular-weight compound is dispersed in an aqueous solution containing a hydrophilic monomer. The dispersed hydrophilic high-molecular-weight compound is dissolved by heat of neutralization (heat of hydration) and/or heat of polymerization generated in the process of producing a hydrophilic polymer.

    摘要翻译： 本发明提供了性能和生产率优异的亲水性聚合物（吸水性树脂）。 根据本发明的制造方法，将亲水性高分子量化合物分散在含有亲水性单体的水溶液中。 分散的亲水性高分子量化合物在制备亲水性聚合物的过程中产生的中和热（水合热）和/或聚合热溶解。

    Particulate water absorbent agent and production method thereof, and water absorbent article
    28.
    发明申请
    Particulate water absorbent agent and production method thereof, and water absorbent article 有权
    颗粒状吸水剂及其制造方法和吸水性物品

    公开(公告)号：US20080269372A1

    公开(公告)日：2008-10-30

    申请号：US12078802

    申请日：2008-04-04

    申请人： Yorimichi Dairoku ,  Yoshifumi Adachi ,  Kozo Nogi ,  Hiroki Inoue ,  Katsuyuki Wada ,  Yoshio Irie

    发明人： Yorimichi Dairoku ,  Yoshifumi Adachi ,  Kozo Nogi ,  Hiroki Inoue ,  Katsuyuki Wada ,  Yoshio Irie

    IPC分类号： C08J5/14

    CPC分类号： C08J3/243 ,  A61L15/60 ,  B01J20/26 ,  B01J20/267 ,  B01J2220/68 ,  C08J2300/102

    摘要： A particulate water absorbing agent of the present invention includes a water absorbent resin, having a cross-linking structure, whose surface has been cross-linked by adding a surface treatment agent, wherein: (i) a mass average particle diameter (D50) ranges from 200 to 600 μm and 95 to 100 wt % of a particulate water absorbing agent whose particle diameter ranges from less than 850 μm to not less than 150 μm is contained with respect to 100 wt % of whole the particulate water absorbing agent, and (ii) a logarithmic standard deviation (σζ) of particle size distribution ranges from 0.25 to 0.45, and (iii) a compressibility rate defined by a following equation ranges from 0 to 18%, and (iv) a surface tension of a supernatant liquid obtained in 4 minutes after dispersing 0.5 g of the particulate water absorbing agent in 50 ml of physiological saline whose temperature is 20° C. is 55 mN/m or more, the compressibility rate (%)=(P−A)/P×100 where P represents a tapped bulk density of the particulate water absorbing agent and A represents a loose bulk density of the particulate water absorbing agent.

    摘要翻译： 本发明的颗粒状吸水剂包括具有交联结构的吸水性树脂，其表面通过添加表面处理剂进行交联，其中：（i）质量平均粒径（D50）范围 相对于全部颗粒状吸水剂的100重量％，含有200〜600μm，95〜100wt％粒径范围在850μm〜150μm以下的颗粒状吸水剂，（ ii）粒度分布的对数标准偏差（sigmazeta）范围为0.25〜0.45，（iii）由下式表示的压缩率为0〜18％，（iv）得到的上清液的表面张力 在将0.5g颗粒状吸水剂分散在温度为20℃的50ml生理盐水中的4分钟内，在＆lt;＆lt;直线式说明书=“在线式”末端 =“铅”？>压缩性 y率（％）=（PA）/ P×100 <？在线公式描述=“在线公式”end =“tail”？>其中P表示颗粒状吸水剂的抽头堆积密度，A表示 颗粒状吸水剂的松散堆积密度。