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21.发明授权Method for producing self-assembled objects comprising fullerene nanotubes and compositions thereof 有权包含富勒烯纳米管的自组装物体的制造方法及其组合物公开(公告)号：US07419651B2
公开(公告)日：2008-09-02
申请号：US11507965
申请日：2006-08-22
申请人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Ken Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
发明人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Ken Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
CPC分类号： G11C13/025 , B01J19/081 , B01J19/087 , B01J19/10 , B01J19/121 , B01J19/126 , B01J19/129 , B01J21/185 , B01J23/74 , B01J23/755 , B01J23/8913 , B01J37/0238 , B01J37/349 , B01J2219/00078 , B01J2219/0892 , B82B3/00 , C01B32/152 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/12 , D01F9/127 , D21H27/00 , G11B9/1418 , G11B9/1445 , G11B9/1472 , G11B9/149 , G11C13/0014 , G11C13/0019 , G11C2213/16 , G11C2213/71 , G11C2213/81 , H01G9/2059 , H01L31/0352 , H01L31/06 , H01L31/18 , H01M4/133 , H01M4/525 , H01M4/583 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E10/542 , Y02E60/122 , Y02P70/521 , Y02P70/54 , Y10S977/70 , Y10S977/742 , Y10S977/745 , Y10S977/748 , Y10S977/75 , Y10S977/753 , Y10S977/789 , Y10S977/842 , Y10S977/843 , Y10S977/845 , Y10S977/847 , Y10S977/848 , Y10S977/849 , Y10S977/882 , Y10S977/948 , Y10T428/24058 , Y10T428/2918 , Y10T428/292 , Y10T428/30
摘要： This invention relates generally to a method for producing self-assembled objects comprising fullerene nanotubes and compositions thereof. In one embodiment, the present invention involves a three-dimensional structure of derivatized fullerene nanotubes that spontaneously form. It includes several components having multiple derivatives brought together to assemble into the three-dimensional structure. In another embodiment, objects may be obtained by bonding functionally-specific agents (FSAs) to groups of nanotubes, enabling them to form into structures. The bond selectivity of FSAs allow selected nanotubes of a particular size or kind to assemble together and inhibit the assembling of unselected nanotubes that may also be present.
摘要翻译： 本发明一般涉及一种生产包含富勒烯纳米管及其组合物的自组装物体的方法。 在一个实施方案中，本发明涉及自发形成的衍生的富勒烯纳米管的三维结构。 它包括具有多个衍生物的几个组件组合在一起以组装成三维结构。 在另一个实施方案中，可以通过将功能特异性试剂（FSA）结合到纳米管组获得目标，使得它们能够形成结构。 FSAs的键选择性允许特定尺寸或种类的所选纳米管组装在一起并且抑制也可能存在的未选择的纳米管的组装。
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22.发明授权公开(公告)号：US07048999B2
公开(公告)日：2006-05-23
申请号：US10033228
申请日：2001-12-28
申请人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
发明人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
IPC分类号： D01F9/12
CPC分类号： G11C13/025 , B01J19/081 , B01J19/087 , B01J19/10 , B01J19/121 , B01J19/126 , B01J19/129 , B01J21/185 , B01J23/74 , B01J23/755 , B01J23/8913 , B01J37/0238 , B01J37/349 , B01J2219/00078 , B01J2219/0892 , B82B3/00 , C01B32/152 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/12 , D01F9/127 , D21H27/00 , G11B9/1418 , G11B9/1445 , G11B9/1472 , G11B9/149 , G11C13/0014 , G11C13/0019 , G11C2213/16 , G11C2213/71 , G11C2213/81 , H01G9/2059 , H01L31/0352 , H01L31/06 , H01L31/18 , H01M4/133 , H01M4/525 , H01M4/583 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E10/542 , Y02E60/122 , Y02P70/521 , Y02P70/54 , Y10S977/70 , Y10S977/742 , Y10S977/745 , Y10S977/748 , Y10S977/75 , Y10S977/753 , Y10S977/789 , Y10S977/842 , Y10S977/843 , Y10S977/845 , Y10S977/847 , Y10S977/848 , Y10S977/849 , Y10S977/882 , Y10S977/948 , Y10T428/24058 , Y10T428/2918 , Y10T428/292 , Y10T428/30
摘要： This invention relates generally to a method for producing self-assembled objects comprising single-wall carbon nanotubes (SWNTs) and compositions thereof. In one embodiment, the present invention involves a three-dimensional structure of derivatized single-wall nanotube molecules that spontaneously form. It includes several component molecule having multiple derivatives brought together to assemble into the three-dimensional structure. In another embodiment, objects may be obtained by bonding functionally-specific agents (FSAs) groups of nanotubes into geometric structures. The bond selectivity of FSAs allow selected nanotubes of a particular size or kind to assemble together and inhibit the assembling of unselected nanotubes that may also be present.
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公开(公告)号：US06936233B2
公开(公告)日：2005-08-30
申请号：US10032933
申请日：2001-12-28
申请人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
发明人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
IPC分类号： B01J8/06 , B01J19/08 , B01J19/10 , B01J19/12 , B01L7/00 , B82B3/00 , C01B31/02 , D01F9/12 , D01F9/127 , G01Q70/06 , G01Q70/12 , G11B9/00 , G11C13/02 , H01G9/20 , H01L31/0352 , H01L31/06 , H01L31/18 , H01M4/133 , H01M4/52 , H01M4/525 , H01M4/58 , H01M4/583 , H01M4/587 , H01M4/62 , H01M10/0525 , H01M10/36
CPC分类号： G11C13/025 , B01J19/081 , B01J19/087 , B01J19/10 , B01J19/121 , B01J19/126 , B01J19/129 , B01J21/185 , B01J23/74 , B01J23/755 , B01J23/8913 , B01J37/0238 , B01J37/349 , B01J2219/00078 , B01J2219/0892 , B82B3/00 , C01B32/152 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/12 , D01F9/127 , D21H27/00 , G11B9/1418 , G11B9/1445 , G11B9/1472 , G11B9/149 , G11C13/0014 , G11C13/0019 , G11C2213/16 , G11C2213/71 , G11C2213/81 , H01G9/2059 , H01L31/0352 , H01L31/06 , H01L31/18 , H01M4/133 , H01M4/525 , H01M4/583 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E10/542 , Y02E60/122 , Y02P70/521 , Y02P70/54 , Y10S977/70 , Y10S977/742 , Y10S977/745 , Y10S977/748 , Y10S977/75 , Y10S977/753 , Y10S977/789 , Y10S977/842 , Y10S977/843 , Y10S977/845 , Y10S977/847 , Y10S977/848 , Y10S977/849 , Y10S977/882 , Y10S977/948 , Y10T428/24058 , Y10T428/2918 , Y10T428/292 , Y10T428/30
摘要： This invention relates generally to a single-wall carbon nanotube (SWNT) purification process and more particularly to a purification process that comprises heating the SWNT-containing felt under oxidizing conditions to remove the amorphous carbon deposits and other contaminating materials. In a preferred mode of this purification procedure, the felt is heated in an aqueous solution of an inorganic oxidant, such as nitric acid, a mixture of hydrogen peroxide and sulfuric acid, or a potassium permanganate. Preferably, SWNT-containing felts are refluxed in an aqueous solution of an oxidizing acid at a concentration high enough to etch away amorphous carbon deposits within a practical time frame, but not so high that the single-wall carbon nanotube material will be etched to a significant degree. When material having a high proportion of SWNT is purified, the preparation produced will be enriched in single-wall nanotubes, so that the SWNT are substantially free of other material.
摘要翻译： 本发明一般涉及单壁碳纳米管（SWNT）纯化方法，更具体地涉及一种净化方法，其包括在氧化条件下加热含SWNT的毡以除去无定形碳沉积物和其它污染物质。 在该纯化方法的优选方式中，将毡在无机氧化剂如硝酸，过氧化氢和硫酸的混合物或高锰酸钾的水溶液中加热。 优选地，含SWNT的毡在氧化酸的水溶液中以足够高的浓度回流，以在实用的时间框架内去除非晶碳沉积物，但不要太高，使得单壁碳纳米管材料将被蚀刻到 重要程度 当具有高比例的SWNT的材料被纯化时，所制备的制剂将富集在单壁纳米管中，使得SWNT基本上不含其它材料。
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公开(公告)号：US06683783B1
公开(公告)日：2004-01-27
申请号：US09380545
申请日：1999-12-22
申请人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Ken Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
发明人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Ken Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
IPC分类号： D01F912
CPC分类号： G11C13/025 , B01J19/081 , B01J19/087 , B01J19/10 , B01J19/121 , B01J19/126 , B01J19/129 , B01J21/185 , B01J23/74 , B01J23/755 , B01J23/8913 , B01J37/0238 , B01J37/349 , B01J2219/00078 , B01J2219/0892 , B82B3/00 , C01B32/152 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/12 , D01F9/127 , D21H27/00 , G11B9/1418 , G11B9/1445 , G11B9/1472 , G11B9/149 , G11C13/0014 , G11C13/0019 , G11C2213/16 , G11C2213/71 , G11C2213/81 , H01G9/2059 , H01L31/0352 , H01L31/06 , H01L31/18 , H01M4/133 , H01M4/525 , H01M4/583 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E10/542 , Y02E60/122 , Y02P70/521 , Y02P70/54 , Y10S977/70 , Y10S977/742 , Y10S977/745 , Y10S977/748 , Y10S977/75 , Y10S977/753 , Y10S977/789 , Y10S977/842 , Y10S977/843 , Y10S977/845 , Y10S977/847 , Y10S977/848 , Y10S977/849 , Y10S977/882 , Y10S977/948 , Y10T428/24058 , Y10T428/2918 , Y10T428/292 , Y10T428/30
摘要： A method for purifying a mixture comprising single-wall carbon nanotubes and amorphous carbon contaminate is disclosed. The method includes the steps of heating the mixture under oxidizing conditions sufficient to remove the amorphous carbon, followed by recovering a product comprising at least about 80% by weight of single-wall carbon nanotubes. A method for producing tubular carbon molecules of about 5 to 500 nm in length is also disclosed. The method includes the steps of cutting single-wall nanotube containing-material to form a mixture of tubular carbon molecules having lengths in the range of 5-500 nm and isolating a fraction of the molecules having substantially equal lengths. The nanotubes may be used, singularly or in multiples, in power transmission cables, in solar cells, in batteries, as antennas, as molecular electronics, as probes and manipulators, and in composites.
摘要翻译： 公开了一种纯化包含单壁碳纳米管和无定形碳污染物的混合物的方法。 该方法包括在足以除去无定形碳的氧化条件下加热混合物的步骤，然后回收包含至少约80重量％的单壁碳纳米管的产品。 还公开了一种生产长度为约5至500nm的管状碳分子的方法。 该方法包括以下步骤：切割含有单壁纳米管的材料以形成长度在5-500nm范围内的管状碳分子的混合物，并分离具有基本相等长度的分子的一部分。 纳米管可以在输电电缆，太阳能电池，电池，天线，分子电子学，探头和操纵器以及复合材料中单独或多次使用。
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公开(公告)号：US07510695B2
公开(公告)日：2009-03-31
申请号：US11507924
申请日：2006-08-22
申请人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Ken Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
发明人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Ken Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
IPC分类号： D01F9/12
CPC分类号： G11C13/025 , B01J19/081 , B01J19/087 , B01J19/10 , B01J19/121 , B01J19/126 , B01J19/129 , B01J21/185 , B01J23/74 , B01J23/755 , B01J23/8913 , B01J37/0238 , B01J37/349 , B01J2219/00078 , B01J2219/0892 , B82B3/00 , C01B32/152 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/12 , D01F9/127 , D21H27/00 , G11B9/1418 , G11B9/1445 , G11B9/1472 , G11B9/149 , G11C13/0014 , G11C13/0019 , G11C2213/16 , G11C2213/71 , G11C2213/81 , H01G9/2059 , H01L31/0352 , H01L31/06 , H01L31/18 , H01M4/133 , H01M4/525 , H01M4/583 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E10/542 , Y02E60/122 , Y02P70/521 , Y02P70/54 , Y10S977/70 , Y10S977/742 , Y10S977/745 , Y10S977/748 , Y10S977/75 , Y10S977/753 , Y10S977/789 , Y10S977/842 , Y10S977/843 , Y10S977/845 , Y10S977/847 , Y10S977/848 , Y10S977/849 , Y10S977/882 , Y10S977/948 , Y10T428/24058 , Y10T428/2918 , Y10T428/292 , Y10T428/30
摘要： This invention relates generally to forming a patterned array of fullerene nanotubes. In one embodiment, a nanoscale array of microwells is provided on a substrate; a metal catalyst is deposited in each microwells; and a stream of hydrocarbon or CO feedstock gas is directed at the substrate under conditions that effect growth of fullerene nanotubes from each microwell.
摘要翻译： 本发明一般涉及形成富勒烯纳米管的图案化阵列。 在一个实施例中，在衬底上提供纳米尺寸的微孔阵列; 在每个微孔中沉积金属催化剂; 并且在从每个微孔产生富勒烯纳米管的生长的条件下，将烃或CO原料气流引向基材。
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公开(公告)号：US20080311025A1
公开(公告)日：2008-12-18
申请号：US11507924
申请日：2006-08-22
申请人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
发明人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
IPC分类号： D01F9/12
CPC分类号： G11C13/025 , B01J19/081 , B01J19/087 , B01J19/10 , B01J19/121 , B01J19/126 , B01J19/129 , B01J21/185 , B01J23/74 , B01J23/755 , B01J23/8913 , B01J37/0238 , B01J37/349 , B01J2219/00078 , B01J2219/0892 , B82B3/00 , C01B32/152 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/12 , D01F9/127 , D21H27/00 , G11B9/1418 , G11B9/1445 , G11B9/1472 , G11B9/149 , G11C13/0014 , G11C13/0019 , G11C2213/16 , G11C2213/71 , G11C2213/81 , H01G9/2059 , H01L31/0352 , H01L31/06 , H01L31/18 , H01M4/133 , H01M4/525 , H01M4/583 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E10/542 , Y02E60/122 , Y02P70/521 , Y02P70/54 , Y10S977/70 , Y10S977/742 , Y10S977/745 , Y10S977/748 , Y10S977/75 , Y10S977/753 , Y10S977/789 , Y10S977/842 , Y10S977/843 , Y10S977/845 , Y10S977/847 , Y10S977/848 , Y10S977/849 , Y10S977/882 , Y10S977/948 , Y10T428/24058 , Y10T428/2918 , Y10T428/292 , Y10T428/30
摘要： This invention relates generally to forming a patterned array of fullerene nanotubes. In one embodiment, a nanoscale array of microwells is provided on a substrate; a metal catalyst is deposited in each microwells; and a stream of hydrocarbon or CO feedstock gas is directed at the substrate under conditions that effect growth of fullerene nanotubes from each microwell.
摘要翻译： 本发明一般涉及形成富勒烯纳米管的图案化阵列。 在一个实施例中，在衬底上提供纳米尺寸的微孔阵列; 在每个微孔中沉积金属催化剂; 并且在从每个微孔产生富勒烯纳米管的生长的条件下，将烃或CO原料气流引向基材。
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公开(公告)号：US07390477B2
公开(公告)日：2008-06-24
申请号：US11507971
申请日：2006-08-22
申请人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Ken Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
发明人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Ken Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
IPC分类号： B82B1/00
CPC分类号： G11C13/025 , B01J19/081 , B01J19/087 , B01J19/10 , B01J19/121 , B01J19/126 , B01J19/129 , B01J21/185 , B01J23/74 , B01J23/755 , B01J23/8913 , B01J37/0238 , B01J37/349 , B01J2219/00078 , B01J2219/0892 , B82B3/00 , C01B32/152 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/12 , D01F9/127 , D21H27/00 , G11B9/1418 , G11B9/1445 , G11B9/1472 , G11B9/149 , G11C13/0014 , G11C13/0019 , G11C2213/16 , G11C2213/71 , G11C2213/81 , H01G9/2059 , H01L31/0352 , H01L31/06 , H01L31/18 , H01M4/133 , H01M4/525 , H01M4/583 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E10/542 , Y02E60/122 , Y02P70/521 , Y02P70/54 , Y10S977/70 , Y10S977/742 , Y10S977/745 , Y10S977/748 , Y10S977/75 , Y10S977/753 , Y10S977/789 , Y10S977/842 , Y10S977/843 , Y10S977/845 , Y10S977/847 , Y10S977/848 , Y10S977/849 , Y10S977/882 , Y10S977/948 , Y10T428/24058 , Y10T428/2918 , Y10T428/292 , Y10T428/30
摘要： This invention relates generally to a fullerene nanotube composition. The fullerene nanotubes may be in the form of a felt, such as a bucky paper. Optionally, the fullerene nanotubes may be derivatized with one or more functional groups. Devices employing the fullerene nanotubes of this invention are also disclosed.
摘要翻译： 本发明一般涉及富勒烯纳米管组合物。 富勒烯纳米管可以是毡的形式，例如巴克纸。 任选地，富勒烯纳米管可以用一个或多个官能团衍生化。 还公开了使用本发明的富勒烯纳米管的装置。
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公开(公告)号：US20080089830A1
公开(公告)日：2008-04-17
申请号：US11507971
申请日：2006-08-22
申请人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
发明人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
IPC分类号： B82B3/00
CPC分类号： G11C13/025 , B01J19/081 , B01J19/087 , B01J19/10 , B01J19/121 , B01J19/126 , B01J19/129 , B01J21/185 , B01J23/74 , B01J23/755 , B01J23/8913 , B01J37/0238 , B01J37/349 , B01J2219/00078 , B01J2219/0892 , B82B3/00 , C01B32/152 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/12 , D01F9/127 , D21H27/00 , G11B9/1418 , G11B9/1445 , G11B9/1472 , G11B9/149 , G11C13/0014 , G11C13/0019 , G11C2213/16 , G11C2213/71 , G11C2213/81 , H01G9/2059 , H01L31/0352 , H01L31/06 , H01L31/18 , H01M4/133 , H01M4/525 , H01M4/583 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E10/542 , Y02E60/122 , Y02P70/521 , Y02P70/54 , Y10S977/70 , Y10S977/742 , Y10S977/745 , Y10S977/748 , Y10S977/75 , Y10S977/753 , Y10S977/789 , Y10S977/842 , Y10S977/843 , Y10S977/845 , Y10S977/847 , Y10S977/848 , Y10S977/849 , Y10S977/882 , Y10S977/948 , Y10T428/24058 , Y10T428/2918 , Y10T428/292 , Y10T428/30
摘要： This invention relates generally to a fullerene nanotube composition. The fullerene nanotubes may be in the form of a felt, such as a bucky paper. Optionally, the fullerene nanotubes may be derivatized with one or more functional groups. Devices employing the fullerene nanotubes of this invention are also disclosed.
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公开(公告)号：US07357906B2
公开(公告)日：2008-04-15
申请号：US11020727
申请日：2004-12-22
申请人： Daniel T. Colbert , Hongjie Dai , Jason H. Hafner , Andrew G. Rinzler , Richard E. Smalley , Jie Liu , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
发明人： Daniel T. Colbert , Hongjie Dai , Jason H. Hafner , Andrew G. Rinzler , Richard E. Smalley , Jie Liu , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
IPC分类号： B82B3/00
CPC分类号： G01Q70/12 , C01B32/152 , C01B32/162 , C01B32/174 , C01B2202/02 , C01B2202/06 , C01B2202/08 , C01B2202/24 , C01B2202/34 , G01Q70/16 , G11B9/1409 , G11B11/007 , G11C13/025 , G11C2213/81 , H01J2201/30469 , Y10S977/70 , Y10S977/75 , Y10S977/789 , Y10S977/843 , Y10S977/845 , Y10T428/249977 , Y10T428/2918
摘要： The invention relates generally to dispersing and fractionating single-wall carbon nanotubes, which can be derivatized to facilitate fractionation, for example, by adding solubilizing moieties to the nanotubes.
摘要翻译： 本发明一般涉及分散和分馏单壁碳纳米管，其可被衍生化以促进分级，例如通过向纳米管中加入增溶部分。
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30.发明授权公开(公告)号：US07087207B2
公开(公告)日：2006-08-08
申请号：US10635976
申请日：2003-08-07
申请人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
发明人： Richard E. Smalley , Daniel T. Colbert , Hongjie Dai , Jie Liu , Andrew G. Rinzler , Jason H. Hafner , Kenneth A. Smith , Ting Guo , Pavel Nikolaev , Andreas Thess
IPC分类号： D01F9/12
CPC分类号： G11C13/025 , B01J19/081 , B01J19/087 , B01J19/10 , B01J19/121 , B01J19/126 , B01J19/129 , B01J21/185 , B01J23/74 , B01J23/755 , B01J23/8913 , B01J37/0238 , B01J37/349 , B01J2219/00078 , B01J2219/0892 , B82B3/00 , C01B32/152 , C01B32/162 , C01B32/17 , C01B2202/02 , D01F9/12 , D01F9/127 , D21H27/00 , G11B9/1418 , G11B9/1445 , G11B9/1472 , G11B9/149 , G11C13/0014 , G11C13/0019 , G11C2213/16 , G11C2213/71 , G11C2213/81 , H01G9/2059 , H01L31/0352 , H01L31/06 , H01L31/18 , H01M4/133 , H01M4/525 , H01M4/583 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E10/542 , Y02E60/122 , Y02P70/521 , Y02P70/54 , Y10S977/70 , Y10S977/742 , Y10S977/745 , Y10S977/748 , Y10S977/75 , Y10S977/753 , Y10S977/789 , Y10S977/842 , Y10S977/843 , Y10S977/845 , Y10S977/847 , Y10S977/848 , Y10S977/849 , Y10S977/882 , Y10S977/948 , Y10T428/24058 , Y10T428/2918 , Y10T428/292 , Y10T428/30
摘要： This invention relates generally to a forming an array of single-wall carbon nanotubes (SWNT) in an electric field and compositions thereof. In one embodiment, a purified bucky paper of single-wall carbon nanotubes is used as the starting material. Upon oxidative treatment of the bucky paper surface, many tube and/or rope ends protrude up from the surface of the paper. Disposing the resulting bucky paper in an electric field results in the protruding tubes and or ropes of single-wall carbon nanotubes aligning in a direction substantially perpendicular to the paper surface. These tubes tend to coalesce to form a molecular array. In another embodiment, a molecular array of SWNTs can be made by “combing” the purified bucky paper starting material with a sharp microscopic tip to align the nanotubes.
摘要翻译： 本发明一般涉及在电场中形成单壁碳纳米管阵列（SWNT）及其组成。 在一个实施方案中，使用单壁碳纳米管的纯化的巴氏纸作为原料。 在对纸张表面进行氧化处理时，许多管和/或绳索端部从纸表面向上突出。 将所得到的负压纸放置在电场中导致单壁碳纳米管的突出管和/或绳索在基本上垂直于纸表面的方向上对齐。 这些管倾向于聚结形成分子阵列。 在另一个实施方案中，SWNT的分子阵列可以通过用精细的微观尖端“精梳”纯化的巴基纸原料来制备纳米管。
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