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公开(公告)号：US06426431B1
公开(公告)日：2002-07-30
申请号：US09643467
申请日：2000-08-22
申请人： Zaida Diaz , Thomas F. Brownscombe
发明人： Zaida Diaz , Thomas F. Brownscombe
IPC分类号： C07L5142
CPC分类号： C07C51/43 , B01J23/002 , B01J23/44 , B01J23/80 , B01J37/088 , C07C51/412 , C07C51/416 , C07C51/42 , C07C51/487 , C08G63/189 , C07C63/38 , C07C63/04
摘要： Disclosed is a method of increasing the yield of 2,6-NDA which comprises: a) Dissolving a disproportionation reaction product containing a dialkali salt of 2,6-NDA in water and filtering off insoluble matter from the resulting solution; b) Precipitating the monoalkali salt of 2,6-NDA (KHNDA) with CO2; c) Suspending said monoalkali salt in water in a weight ratio higher than 8:1, water: monosalt; and d) Heating at a temperature above 100° C. and at a pressure above 100 psig. The improvements in yield are from about 20% to as high as 45%.
摘要翻译： 公开了一种提高2,6-NDA产率的方法，其包括：a）将含有2,6-NDA的二盐的歧化反应产物溶解在水中，并从所得溶液中滤出不溶物; b）沉淀 2,6-NDA（KHNDA）与二氧化碳的单碱性盐; c）以高于8:1的重量比悬浮所述单碱性盐，水：单糖; andd）在高于100℃的温度和高于100psig的压力下加热。产率的提高为约20％至高达45％。
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公开(公告)号：US5510413A
公开(公告)日：1996-04-23
申请号：US811218
申请日：1991-12-20
IPC分类号： C08K3/34
CPC分类号： C08K3/34
摘要： Polymer compositions comprising .alpha.-olefin polymers and a minor proportion of synthetic basic zeolite are stabilized against the harmful effects of corrosion of metal surfaces when processed through mechanical equipment such as molds and extruders where the composition normally contacts metal surfaces.
摘要翻译： 包含α-烯烃聚合物和少量合成碱性沸石的聚合物组合物在通过诸如模具和挤出机的机械设备（其中组合物通常接触金属表面）进行加工时，抵抗了金属表面的腐蚀的有害影响。
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33.发明授权Use of viscosity as an in-line diagnostic for high internal phase emulsion generation 失效使用粘度作为高内相乳液生成的在线诊断
公开(公告)号：US5306734A
公开(公告)日：1994-04-26
申请号：US118541
申请日：1993-09-08
CPC分类号： G01N11/14 , C08F2/32 , C08J9/28 , C08J2201/0504 , G01N2011/147 , Y10S521/917
摘要： A lightweight absorbent foam is produced using a high internal phase emulsion (HIPE), the production of which incorporates the use of capillary viscosity measurements as an in-line diagnostic for HIPE quality. The in-line diagnostics yield measurements of viscosity slope and amplitude. These measurements offer several advantages for monitoring emulsion quality, including stable high resolution measurement of hardware-independent parameters of the whole flow, without the need for sampling.
摘要翻译： 使用高内相乳液（HIPE）生产轻质的吸收性泡沫，其生产包括使用毛细管粘度测量作为HIPE质量的在线诊断。 在线诊断产生粘度斜率和振幅的测量。 这些测量提供了监测乳液质量的几个优点，包括稳定的高分辨率测量整个流程的硬件无关参数，无需采样。
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公开(公告)号：US5264133A
公开(公告)日：1993-11-23
申请号：US957832
申请日：1992-10-08
CPC分类号： C01B19/001 , B01D15/00 , B01J20/186 , C01B19/008 , Y10S210/912
摘要： A process for the removal of soluble selenium from aqueous media comprising contacting the aqueous media with a porous support material having exchanged thereon metal ions selected from transition metal ions, alkali earth metal ions and mixtures thereof.
摘要翻译： 一种从水性介质中除去可溶性硒的方法，包括使含水介质与多孔载体材料接触，所述多孔载体材料上交换有选自过渡金属离子，碱土金属离子及其混合物的金属离子。
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35.发明授权
公开(公告)号：US5252619A
公开(公告)日：1993-10-12
申请号：US17544
申请日：1993-02-16
摘要： In a process for the preparation of a low density porous crosslinked polymeric material by polymerizing a water-in-oil high internal phase emulsion, curing time of the monomers in the emulsion can be reduced without adversely affecting polymer properties or substantially affecting the emulsion by carrying out the curing in multiple-stages. The emulsion is first pre-cured at a temperature less than about 65.degree. C. until the emulsion reaches a Rheometrics dynamic shear modulus of at least about 500 and subsequently curing at a temperature above about 70.degree. C.
摘要翻译： 在通过聚合油包水高内相乳液制备低密度多孔交联聚合物材料的方法中，可以降低乳液中单体的固化时间，而不会不利地影响聚合物性能或通过携带 在多个阶段进行固化。 首先将乳液在低于约65℃的温度下预固化，直到乳液达到至少约500的Rheometrics动态剪切模量，随后在高于约70℃的温度下固化。
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36.发明授权
公开(公告)号：US5189070A
公开(公告)日：1993-02-23
申请号：US891322
申请日：1992-05-29
IPC分类号： C08F2/24 , C08F2/22 , C08F2/32 , C08F212/00 , C08F212/36 , C08F220/10 , C08F220/18 , C08J9/28
摘要： In a process for the preparation of a low density porous crosslinked polymeric material by polymerizing a water-in-oil high internal phase emulsion, curing time of the monomers in the emulsion can be reduced without adversely affecting polymer properties or substantially affecting the emulsion by carrying out the curing in multiple-stages. The emulsion is first pre-cured at a temperature less than about 65.degree. C. until the emulsion reaches a Rheometrics dymanic shear modulus of at least about 500 and subsequently curing at a temperature above about 70.degree. C.
摘要翻译： 在通过聚合油包水高内相乳液制备低密度多孔交联聚合物材料的方法中，可以降低乳液中单体的固化时间，而不会不利地影响聚合物性能或通过携带 在多个阶段进行固化。 首先将乳液在低于约65℃的温度下预固化，直到乳液达到至少约500的流变测定剪切模量，然后在高于约70℃的温度下固化。
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公开(公告)号：US5053372A
公开(公告)日：1991-10-01
申请号：US387265
申请日：1989-07-31
CPC分类号： B01J29/061 , B01J23/02
摘要： This invention relates to basic compositions comprising a zeolite and an alkaline earth metal compound wherein the sum of the amount of the alkaline earth metal in the compound plus any metal cation exchanged into the zeolite is in excess of that required to provide a fully metal cation-exchanged zeolite. This invention further relates to methods for preparing the instant compositions. In a preferred embodiment the instant compositions are prepared by impregnating a zeolite with a solution of an alkaline earth metal salt wherein said alkaline earth metal impregnated in the zeolite is in excess of that required to provide a fully metal cation-exchanged zeolite, precipitating out an insoluble alkaline earth metal compound within the zeolite by contact with a precipitation agent, and/or drying the resultant impregnated/(precipitated) material and then calcining the resultant composition.
摘要翻译： 本发明涉及包含沸石和碱土金属化合物的碱性组合物，其中化合物中的碱土金属的量加上交换到沸石中的任何金属阳离子的总和超过提供完全金属阳离子 - 交换沸石。 本发明还涉及制备本发明组合物的方法。 在优选的实施方案中，本发明组合物通过用碱土金属盐溶液浸渍沸石来制备，其中浸渍在沸石中的所述碱土金属超过提供完全金属阳离子交换的沸石所需的碱土金属，沉淀出 通过与沉淀剂接触，和/或干燥所得的浸渍/（沉淀）材料，然后煅烧所得组合物，沸石内的不溶性碱土金属化合物在沸石内。
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公开(公告)号：US4379908A
公开(公告)日：1983-04-12
申请号：US355082
申请日：1982-03-05
IPC分类号： C08F283/10 , C08G59/40 , C08G59/68 , C08K3/38 , C08G65/02
CPC分类号： C08G59/68 , C08F283/10 , C08G59/40 , C08K3/38
摘要： The present invention provides an curable composition comprising (1) at least one epoxy compound containing at least one vicinal-epoxy groups, (2) a miscible amount of at least one ethylenically unsaturated monomer and (3) a curing amount of at least one catalyst selected from lithium or Group II metal salts of a non-nucleophilic acid.
摘要翻译： 本发明提供一种可固化组合物，其包含（1）至少一种含有至少一个邻位环氧基的环氧化合物，（2）可混合量的至少一种烯属不饱和单体和（3）固化量的至少一种催化剂 选自非亲核性酸的锂或II族金属盐。
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