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    FLUOROADAMANTANE DERIVATIVE
    32.
    发明申请
    FLUOROADAMANTANE DERIVATIVE 失效
    荧光素衍生物

    公开(公告)号：US20070129566A1

    公开(公告)日：2007-06-07

    申请号：US11567391

    申请日：2006-12-06

    申请人： Shu-zhong WANG ,  Taiki Hoshino ,  Kimiaki Kashiwagi ,  Takashi Okazoe ,  Eisuke Murotani ,  Masahiro Ito ,  Kunio Watanabe

    发明人： Shu-zhong WANG ,  Taiki Hoshino ,  Kimiaki Kashiwagi ,  Takashi Okazoe ,  Eisuke Murotani ,  Masahiro Ito ,  Kunio Watanabe

    IPC分类号： C07C69/52

    CPC分类号： C07C69/653 ,  C07C29/095 ,  C07C35/52 ,  C07C67/14 ,  C07C67/287 ,  C07C2603/74 ,  C07C69/708

    摘要： Adamantane derivates which can be material compounds of a polymer excellent in etching resistance and having improved transmittance to light having a short wavelength, are produced by an economically advantageous process from readily available materials. A compound (10) is subjected to esterification reaction with a compound (11) to obtain a compound (12), which is subjected to fluorination in a liquid phase to obtain a compound (13), which is then subjected to hydrolysis or alcoholysis to obtain a compound (2), which is then reacted with a compound (15) thereby to obtain a compound (1). Here, A to J are —CFH— or —CF2—; RF is a perfluoroalkyl group or the like; X10 is F or the like; Y2 is H or OH; Y3 is H or RFCOO—; Y4 is H, F or RFCOO—; Y5 is H, F, RFCOO— or OH; Y0 is H, F, —OCOCR1═CH2 or OH: R1 is a hydrogen atom, a methyl group or the like; and X11 is OH or a halogen atom:

    摘要翻译： 金刚烷衍生物可以通过从容易获得的材料的经济上有利的方法产生耐蚀性优异且具有改善的具有短波长的光的透射率的聚合物的材料化合物。 化合物（10）与化合物（11）进行酯化反应，得到化合物（12），将其进行液相氟化，得到化合物（13），然后进行水解或醇解 得到化合物（2），然后与化合物（15）反应，得到化合物（1）。 这里，A至J为-CFH-或-CF 2 - RF是全氟烷基等; X 10是F等; Y 2是H或OH; Y 3是H或R 0 COO-; Y 4是H，F或R“COO-; H 5是H，F，R F CO或O-; Y 0是H，F，-OCOCR 1 -CH 2或OH：R 1是氢原子 ，甲基等; 并且X 11是OH或卤素原子：

    Fluoroadamantane derivative
    33.
    发明授权
    Fluoroadamantane derivative 失效
    氟金刚烷衍生物

    公开(公告)号：US07511177B2

    公开(公告)日：2009-03-31

    申请号：US12020863

    申请日：2008-01-28

    申请人： Shu-zhong Wang ,  Taiki Hoshino ,  Kimiaki Kashiwagi ,  Takashi Okazoe ,  Eisuke Murotani ,  Masahiro Ito ,  Kunio Watanabe

    发明人： Shu-zhong Wang ,  Taiki Hoshino ,  Kimiaki Kashiwagi ,  Takashi Okazoe ,  Eisuke Murotani ,  Masahiro Ito ,  Kunio Watanabe

    IPC分类号： C07C35/22

    CPC分类号： C07C69/653 ,  C07C29/095 ,  C07C35/52 ,  C07C67/14 ,  C07C67/287 ,  C07C2603/74 ,  C07C69/708

    摘要： Adamantane derivates which can be material compounds of a polymer excellent in etching resistance and having improved transmittance to light having a short wavelength, are produced by an economically advantageous process from readily available materials.A compound (10) is subjected to esterification reaction with a compound (11) to obtain a compound (12), which is subjected to fluorination in a liquid phase to obtain a compound (13), which is then subjected to hydrolysis or alcoholysis to obtain a compound (2), which is then reacted with a compound (15) thereby to obtain a compound (1). Here, A to J are —CFH— or —CF2—; RF is a perfluoroalkyl group or the like; X10 is F or the like; Y2 is H or OH; Y3 is H or RFCOO—; Y4 is H, F or RFCOO—; Y5 is H, F, RFCOO— or OH; Y0 is H, F, —OCOCR1═CH2 or OH: R1 is a hydrogen atom, a methyl group or the like; and X11 is OH or a halogen atom:

    摘要翻译： 金刚烷衍生物可以通过从容易获得的材料的经济上有利的方法产生耐蚀性优异且具有改善的具有短波长的光的透射率的聚合物的材料化合物。 化合物（10）与化合物（11）进行酯化反应，得到化合物（12），将其进行液相氟化，得到化合物（13），然后进行水解或醇解 得到化合物（2），然后与化合物（15）反应，得到化合物（1）。 这里，A至J为-CFH-或-CF2-; RF是全氟烷基等; X10为F等; Y2是H或OH; Y3为H或RFCOO-; Y4是H，F或RFCOO-; Y5为H，F，RFCOO-或OH; Y0是H，F，-OCOCR1-CH2或OH：R1是氢原子，甲基等; X 11为OH或卤原子：

    Fluorinated adamantane derivative
    34.
    发明授权
    Fluorinated adamantane derivative 失效
    氟化金刚烷衍生物

    公开(公告)号：US07425646B2

    公开(公告)日：2008-09-16

    申请号：US11611183

    申请日：2006-12-15

    申请人： Kazuya Oharu ,  Takashi Okazoe ,  Eisuke Murotani ,  Kunio Watanabe ,  Masahiro Ito

    发明人： Kazuya Oharu ,  Takashi Okazoe ,  Eisuke Murotani ,  Kunio Watanabe ,  Masahiro Ito

    IPC分类号： C07C69/63

    CPC分类号： C07C61/15 ,  C07C51/58 ,  C07C2603/74

    摘要： A compound represented by the formula AF(—COF)n, provided that AF and n have the following meanings.AF: a fluorinated adamantane residue which is an n-valent group having an n number of hydrogen atoms removed from adamantane (provided that when n is at least 2, the removed hydrogen atoms are hydrogen atoms bonded to different carbon atoms), wherein at least one of the remaining hydrogen atoms is substituted by a fluorine atom, and the remaining hydrogen atoms may be substituted by a C1-6 alkyl group or fluoroalkyl group, and n: an integer of from 1 to 4, provided the when n is 1, AF has at least one hydrogen atom.

    摘要翻译： 由式A -F（ - COF）n N表示的化合物，条件是A和N具有下列含义。 氟化金刚烷残基，其是从金刚烷中除去n个氢原子的n价基团（条件是当n至少为2时，除去的氢原子是与氢原子键合的氢原子 不同的碳原子），其中剩余的氢原子中的至少一个被氟原子取代，剩余的氢原子可以被C 1-6烷基或氟代烷基取代，n ：1〜4的整数，n为1时，A为至少1个氢原子。

    Fluoropolyether compound
    37.
    发明授权
    Fluoropolyether compound 有权
    氟聚醚化合物

    公开(公告)号：US07795375B2

    公开(公告)日：2010-09-14

    申请号：US11483566

    申请日：2006-07-11

    申请人： Daisuke Shirakawa ,  Kazuya Oharu ,  Takashi Okazoe

    发明人： Daisuke Shirakawa ,  Kazuya Oharu ,  Takashi Okazoe

    IPC分类号： C08G65/321

    CPC分类号： C11D1/004 ,  C08G65/323 ,  C08G65/337 ,  C08L71/02 ,  C10M105/54 ,  C10M107/38 ,  C10M2211/0406 ,  C10M2213/043

    摘要： It is to provide a compound which has a low vapor pressure and low viscosity, which is less problematic in deterioration during its use and which is useful as e.g. a lubricant, a surface modifier or a surfactant.A fluoropolyether compound represented by the formula (X—)xY(—Z)z, wherein X is a group represented by the formula HO—(CH2CH2O)a.(CH2CH(OH)CH2O)b—(CH2)c—CF2O(CF2CF2O)d— (wherein “a” is an integer of from 0 to 100, b is an integer of from 0 to 100, c is an integer of from 1 to 100, and d is an integer of from 1 to 200), Z is a group represented by the formula RFO(CF2CF2O)g— (wherein RF is e.g. a C1-20 perfluoroalkyl group having an etheric oxygen atom inserted between carbon-carbon atoms, and g is an integer of from 3 to 200), Y is e.g. a (x+z) valent perfluorinated saturated hydrocarbon group, x is an integer of at least 2, z is an integer of at least 0, and (x+z) is an integer of from 3 to 20.

    摘要翻译： 本发明提供一种具有低蒸气压和低粘度的化合物，其在使用时的劣化问题较少，可用于例如 润滑剂，表面改性剂或表面活性剂。 由式（X）x Y（-Z）z表示的含氟聚醚化合物，其中X是由式HO-（CH 2 CH 2 O）a。（CH 2 CH（OH）CH 2 O）b - （CH 2）c -CF 2（ CF 2 CF 2 O）d - （其中，“a”为0〜100的整数，b为0〜100的整数，c为1〜100的整数，d为1〜200的整数） Z是由式RFO（CF 2 CF 2 O）g-表示的基团（其中，RF例如是碳原子之间插入醚性氧原子的碳原子数为1-20的全氟烷基，g为3〜200的整数），Y 是例如 （x + z）价全氟饱和烃基，x为至少2的整数，z为至少为0的整数，（x + z）为3至20的整数。

    PERFLUOROPOLYETHER DERIVATIVE
    38.
    发明申请
    PERFLUOROPOLYETHER DERIVATIVE 失效
    全氟代醇衍生物

    公开(公告)号：US20070203366A1

    公开(公告)日：2007-08-30

    申请号：US11742863

    申请日：2007-05-01

    申请人： Daisuke SHIRAKAWA ,  Takashi Okazoe ,  Kazuya Oharu ,  Shu-zhong Wang ,  Koichi Murata ,  Kengo Kawahara

    发明人： Daisuke SHIRAKAWA ,  Takashi Okazoe ,  Kazuya Oharu ,  Shu-zhong Wang ,  Koichi Murata ,  Kengo Kawahara

    IPC分类号： C07C43/12

    CPC分类号： C08G65/007 ,  C10M107/38 ,  C10M2213/043 ,  C10M2213/0606 ,  C10N2240/204

    摘要： A novel perfluoropolyether derivative which is less likely to undergo decomposition, which is free from a problem of deterioration during its use, and which is useful as a lubricating oil or a coating agent, is provided. A compound represented by the following formula (1): HO—(CH2CH2O)r•(CH2CH(OH)CH2O)p—CH2CF2O(CF2CF2O)mCF2CH2O—(CH2CH(OH)CH2O)q•(CH2CH2O)s—H  Formula (1) wherein m represents an integer of from 3 to 200, and each of p, q, r and s which are independent of one another, represents an integer of from 0 to 100, provided that when each of p, q, r and s which are independent of one another, is an integer of at least 1, the arrangement of —(CH2CH2O)— and —(CH2CH(OH)CH2O)— units is not particularly limited, and when one of r and p is an integer of at least 2 and the other is an integer of at least 1, or when one of q and s is an integer of at least 2 and the other is an integer of at least 1, these units may be arranged in a block form or at random.

    摘要翻译： 提供了一种不太可能分解的新型全氟聚醚衍生物，其在使用中没有劣化的问题，并且其可用作润滑油或涂层剂。 由下式（1）表示的化合物：<？in-line-formula description =“In-line formula”end =“lead”？> HO-（CH 2 CH 2 （CH 2 CH（OH）CH 2 O）CH 2 CH（OH）CH 2 CH 2 2 CF 2 O 2（CF 2 CF 2 O）CF 2 O（CF 2 O 2 CF 2） 2 CH 2 CH 2 O - （CH 2 CH 2 OH（CH 2 OH）CH 2 O）q （CH 2 CH 2 CH 2）n -H（式（1））＆lt;线内公式描述=“在线式 “end =”tail“？>其中m表示3〜200的整数，彼此独立的p，q，r和s各自表示0〜100的整数，条件是， 彼此独立的p，q，r和s是至少为1的整数， - （CH 2 CH 2 CH 2 O） - 和 - （CH 2 CH（OH）CH 2 O） - 单元没有特别限制，当r和p中的一个为至少2的整数，另一个为 至少为1的整数，或者q和s之一的整数 至少为2的整数，另一个为至少为1的整数，这些单元可以以块形式或随机排列。

    Fluoropolyether compound
    39.
    发明申请
    Fluoropolyether compound 有权
    氟聚醚化合物

    公开(公告)号：US20060252910A1

    公开(公告)日：2006-11-09

    申请号：US11483566

    申请日：2006-07-11

    申请人： Daisuke Shirakawa ,  Kazuya Oharu ,  Takashi Okazoe

    发明人： Daisuke Shirakawa ,  Kazuya Oharu ,  Takashi Okazoe

    IPC分类号： C08G65/321

    CPC分类号： C11D1/004 ,  C08G65/323 ,  C08G65/337 ,  C08L71/02 ,  C10M105/54 ,  C10M107/38 ,  C10M2211/0406 ,  C10M2213/043

    摘要： It is to provide a compound which has a low vapor pressure and low viscosity, which is less problematic in deterioration during its use and which is useful as e.g. a lubricant, a surface modifier or a surfactant. A fluoropolyether compound represented by the formula (X—)xY(-Z)z, wherein X is a group represented by the formula HO—(CH2CH2O)a.(CH2CH(OH) CH2O)b—(CH2)c—CF2O(CF2CF2O)d— (wherein “a” is an integer of from 0 to 100, b is an integer of from 0 to 100, c is an integer of from 1 to 100, and d is an integer of from 1 to 200), Z is a group represented by the formula RFO(CF2CF2O)g— (wherein RF is e.g. a C120 perfluoroalkyl group having an etheric oxygen atom inserted between carbon-carbon atoms, and g is an integer of from 3 to 200), Y is e.g. a (x+z) valent perfluorinated saturated hydrocarbon group, x is an integer of at least 2, z is an integer of at least 0, and (x+z) is an integer of from 3 to 20.

    摘要翻译： 本发明提供一种具有低蒸气压和低粘度的化合物，其在使用时的劣化问题较少，可用于例如 润滑剂，表面改性剂或表面活性剂。 由式（X-）x Y（-Z）z Z表示的含氟聚醚化合物，其中X是由式HO-（CH 2） （CH 2 CH（OH）CH 2 O）（CH 2 CH（OH）CH 2 O） （CH 2）2 - （CH 2）2 - （CH 2 CH 2） （其中“a”为0至100的整数，b为0至100的整数，c为1至1的整数） 100，d为1〜200的整数），Z为下式表示的基团R（O）2 CF 2 （其中RF是例如碳原子之间插入醚性氧原子的C 120全氟烷基，g是3〜 200），Y是例如 （x + z）价全氟饱和烃基，x为至少2的整数，z为至少为0的整数，（x + z）为3至20的整数。

    Perfluoropolyether derivative
    40.
    发明申请
    Perfluoropolyether derivative 失效
    全氟聚醚衍生物

    公开(公告)号：US20050197408A1

    公开(公告)日：2005-09-08

    申请号：US11107980

    申请日：2005-04-18

    申请人： Daisuke Shirakawa ,  Takashi Okazoe ,  Kazuya Oharu ,  Shu-zhong Wang ,  Koichi Murata ,  Kengo Kawahara

    发明人： Daisuke Shirakawa ,  Takashi Okazoe ,  Kazuya Oharu ,  Shu-zhong Wang ,  Koichi Murata ,  Kengo Kawahara

    IPC分类号： A61K31/08 ,  C08G65/00 ,  C10M107/38

    CPC分类号： C08G65/007 ,  C10M107/38 ,  C10M2213/043 ,  C10M2213/0606 ,  C10N2240/204

    摘要： A novel perfluoropolyether derivative which is less likely to undergo decomposition, which is free from a problem of deterioration during its use, and which is useful as a lubricating oil or a coating agent, is provided. A compound represented by the following formula (1): HO—(CH2CH2O)r.(CH2CH (OH)CH2O)p—CH2CF2O(CF2CF2O)mCF2CH2O——(CH2CH(OH)CH2O)q.(CH2CH2O)s—H  Formula (1) wherein m represents an integer of from 3 to 200, and each of p, q, r and s which are independent of one another, represents an integer of from 0 to 100, provided that when each of p, q, r and s which are independent of one another, is an integer of at least 1, the arrangement of —(CH2CH2O)— and —(CH2CH(OH)CH2O)— units is not particularly limited, and when one of r and p is an integer of at least 2 and the other is an integer of at least 1, or when one of q and s is an integer of at least 2 and the other is an integer of at least 1, these units may be arranged in a block form or at random.

    摘要翻译： 提供了一种不太可能分解的新型全氟聚醚衍生物，其在使用中没有劣化的问题，并且其可用作润滑油或涂层剂。 由下式（1）表示的化合物：<？in-line-formula description =“In-line formula”end =“lead”？> HO-（CH 2 CH 2 （CH 2 CH（OH）CH 2 O）CH 2 CH（OH）CH 2 CH 2 2 CF 2 O 2（CF 2 CF 2 O）CF 2 O（CF 2 O 2 CF 2） 2 CH 2 - （CH 2 CH（OH）CH 2 O）q 其中m表示3〜200的整数，p，q，r和s彼此独立地表示0〜100的整数，条件是每当 彼此独立的p，q，r和s的整数为至少1的整数， - （CH 2 CH 2 CH 2 O）的排列 - 和 - （CH 2 CH（OH）CH 2 O） - 单元没有特别限制，当r和p中的一个为至少2的整数，另一个为 是至少为1的整数，或者q和s之一的整数 是至少为2的整数，另一个是至少为1的整数，这些单元可以以块形式或随机排列。