Method and Device for Removing Contaminants Arising During the Production of Aliphatic Nitrate Esters
    32.
    发明申请
    Method and Device for Removing Contaminants Arising During the Production of Aliphatic Nitrate Esters 审中-公开
    用于去除在脂肪族硝酸酯生产过程中产生的污染物的方法和装置

    公开(公告)号:US20160200663A1

    公开(公告)日:2016-07-14

    申请号:US14912387

    申请日:2014-06-25

    摘要: The invention relates to a method and to a device for removing contaminants arising during the production of aliphatic or alicyclic nitric acid esters, in particular for removing contaminants from nitrated crude nitric acid esters, which nitrated crude nitric acid esters arise during the nitration of monovalent or multivalent aliphatic or alicyclic alcohols capable of nitration, after the separation of the final nitrating acid, and to a production system for nitrating monovalent or multivalent aliphatic alcohols capable of nitration with subsequent purification of the nitrated nitric acid esters.

    摘要翻译: 本发明涉及一种用于去除在制备脂族或脂环族硝酸酯期间产生的污染物的方法和装置,特别是用于从硝化的粗硝酸酯中除去污染物,硝酸化的硝酸酯在硝化单价或 在最终的硝酸分离后能够进行硝化的多价脂肪族或脂环族醇,以及能够硝化硝酸硝酸酯的能够进行硝化的一价或多价脂肪族醇的生产体系​​。

    Method and apparatus for counter current liquid-liquid extraction
    33.
    发明授权
    Method and apparatus for counter current liquid-liquid extraction 失效
    逆流液相萃取的方法和装置

    公开(公告)号:US4879037A

    公开(公告)日:1989-11-07

    申请号:US169498

    申请日:1988-03-17

    摘要: A liquid-liquid extraction device and method for operating the same is disclosed. The device includes first and second conduits in flow communication with each other via a common wall having a large number of perforations. The second conduit includes an outer tube wall having a plurality of perforations leading to the outside of the device. When liquid in the first conduit is subjected to a pressure higher than that of the second conduit, and the pressure of the liquid in the second conduit is higher than that of the ambient pressure, liquid will be allowed to flow from the first conduit via perforations in the common wall into the second conduit so as to intermingle with the liquid in the second conduit. The resultant mixture in the second conduit is then ejected to the outside as a fine liquid jet via the perforations in the outer tube wall. The first and second conduits are constructed of a liquid-tight, elastically resilient material being non-swelling in contact with organic extraction solvents.

    Washing apparatus
    35.
    发明授权

    公开(公告)号:US2755302A

    公开(公告)日:1956-07-17

    申请号:US34199053

    申请日:1953-03-12

    申请人: NITROGLYCERIN AB

    摘要: 731,014. Purifying liquids; gravity-separation apparatus. NITROGLYCERIN AKTIEBOLAGET. April 28, 1953 [April 29, 1952], No. 11664/53. Class 46. The apparatus shown is for washing a liquid such as a nitrated product with another liquid immiscible with it and having a different specific gravity. Washing liquid, such as water, to which an alkali has been added, introduced at 5, and nitroglycerine introduced at 4 are mixed in an injector 3 with the help of compressed air introduced at 6. The mixture passes into a chamber 1 where the air maintains vigorous movement before discharge at 9. The liquid mixture passes between plates 7 forming an angle of between 45 degrees and 60 degrees with the horizontal and spaced apart by a distance small (e.g. 5 mm.) compared with their extent into an intermediate compartment 8 and thence through openings 12 in a wall 10 into a separating chamber 11. From the latter the washing liquid overflows at 16 and the nitroglycerine at 15. The lower end of the separating chamber 11 communicates with an inspection glass 13 ; a layer h e of mixed liquids separating the two liquids may be maintained at the level of this glass by adjusting the height H between the overflow levels 15 and 16, for example with interchangeable nozzles.