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公开(公告)号：US11938416B2
公开(公告)日：2024-03-26
申请号：US16982796
申请日：2019-11-01
发明人： Zhijun Li , Cheng Wu , Yumin Zhang , Yubo Li
CPC分类号： B01D11/0449 , B01D11/0457 , B01D11/0492 , B01D17/045
摘要： Disclosed in the present invention is a polyether polyol refining method, comprising (1) neutralising or diluting crude polyether polyol to obtain a mixed solution; (2) flowing the mixed solution through a hydrophilic medium to aggregate same into a first density phase liquid and a second density phase liquid, the first density phase liquid being an aqueous solution containing alkaline metal ions and/or alkaline earth metal ions, and the second density phase liquid being polyether polyol; and (3) allowing the first density phase liquid to settle and separating same from the second density phase liquid to obtain refined polyether polyol. In the present refining method, using the hydrophilic medium for one-step removal of the alkaline ions and water in the polyether polyol simplifies the treatment steps, increases treatment efficiency, and can prevent polyether polyol loss; the obtained polyether polyol has low alkaline ion content and little odour. Also disclosed in the present invention is a polyether polyol refining apparatus, comprising a mixing unit and a separating unit, and being capable of refining polyether polyol with low alkaline ion content and little odour.
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公开(公告)号：US20230191280A1
公开(公告)日：2023-06-22
申请号：US17760027
申请日：2022-07-12
申请人： CHEMTOR, LP
发明人： Rana MOHAMED
CPC分类号： B01D11/0496 , C11B3/006 , B01D11/0449 , B01F33/30 , B01F2101/2204
摘要： The present disclosure relates to the design of structural features that enable the facile and reproducible fabrication of a microfluidic reactor that eliminates the problem of scaling factors in turn enabling the broad integration of microchannel reactors to industrial scale production. The process is highlighted via the effective and successful scale up of a purification process for the removal of a variety of different classes of impurities from crude vegetable oils mixtures into feedstocks that can be directly integrated into the hydrotreatment vegetable oil hydrogenation process for mass production of synthetic diesel derived from renewable sources.
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公开(公告)号：US20170014733A1
公开(公告)日：2017-01-19
申请号：US15277533
申请日：2016-09-27
申请人： Chemtor, LP
发明人： John Lee Massingill
IPC分类号： B01D11/04 , C22B3/26 , C07C29/76 , C07F9/09 , C07D207/06 , C07C67/56 , C07D333/76 , C02F1/26 , C07C51/47
CPC分类号： B01D11/0449 , B01D11/04 , C02F1/26 , C02F2101/103 , C02F2101/20 , C02F2101/308 , C02F2101/34 , C02F2103/10 , C02F2103/24 , C02F2103/30 , C02F2103/325 , C02F2103/343 , C07C29/76 , C07C51/47 , C07C67/56 , C07D207/06 , C07D333/76 , C07F9/09 , C22B3/0005 , Y02P10/234
摘要： Processes are provided which utilize fiber conduit reactors/contactors to effect extraction from a fluid stream, particularly a fermentation broth, a waste stream of a fermentation process, a fluid comprising a dye, or a fluid comprising a pharmaceutical compound. In particular, methods are provided which include introducing a first stream comprising an extractant and a second stream which is substantially immiscible with the first stream into a conduit reactor proximate a plurality of fibers. The streams are introduced into the conduit reactor such that they are in contact with each other and the extractant of the first stream interacts with the second stream to extract a fermentation product, a fermentation byproduct, a dye or a pharmaceutical compound from the second stream into the first stream. The method further includes receiving the first and second streams in collection vessel/s and withdrawing separately the first and second streams from collection vessel/s.
摘要翻译： 提供了使用纤维导管反应器/接触器来实现从流体流，特别是发酵液，发酵过程的废物流，包含染料的流体或包含药物化合物的流体中提取的方法。 特别地，提供了包括将包含萃取剂的第一流和与第一流基本上不混溶的第二流引入靠近多个纤维的导管反应器中的方法。 将流引入导管反应器中使得它们彼此接触，并且第一物流的提取物与第二物流相互作用以将发酵产物，发酵副产物，染料或药物化合物从第二流提取成 第一流。 该方法还包括在收集容器中接收第一和第二流，并将第一和第二流分别从收集容器中取出。
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公开(公告)号：US20150105529A1
公开(公告)日：2015-04-16
申请号：US14400050
申请日：2013-05-22
发明人： Robert Fosdick , Gary Wieber
IPC分类号： C08G77/34
CPC分类号： C08G77/34 , B01D11/0449 , B01D2011/005
摘要： A process is disclosed for preparing silicone resins having improved product purity. The process involves flowing a first liquid containing a silicone resin and an impurity through a fiber bundle, wherein the first liquid and second liquid are substantially immiscible.
摘要翻译： 公开了一种制备具有提高的产品纯度的硅树脂的方法。 该方法包括使含有硅树脂和杂质的第一液体通过纤维束流动，其中第一液体和第二液体基本上是不混溶的。
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公开(公告)号：US20130082003A1
公开(公告)日：2013-04-04
申请号：US13644430
申请日：2012-10-04
CPC分类号： C02F1/26 , B01D11/0449 , B01D11/0488 , B01D11/0492 , C02F1/265 , C02F2103/08 , C02F2103/365 , C02F2303/18 , Y02W10/37
摘要： Purified water can be obtained via a continuous or semi-continuous process by mixing a liquid composition (e.g., sea water or produced frac water) including water with a directional solvent to selectively dissolve water from the liquid composition into the directional solvent. The concentrated remainder of the liquid composition (e.g., brine) is removed, and the water is precipitated from the directional solvent and removed in a purified form. The solvent is then reused as the process is repeated in a continuous or semi-continuous operation.
摘要翻译： 通过将包括水和液体组合物（例如海水或生产的压裂水）与定向溶剂混合以选择性地将水从液体组合物溶解到定向溶剂中，可以通过连续或半连续方法获得纯化水。 除去液体组合物的浓缩剩余物（例如盐水），并从定向溶剂中沉淀出水并以纯化形式除去。 然后在连续或半连续操作过程中重复使用溶剂。
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公开(公告)号：US20100069686A1
公开(公告)日：2010-03-18
申请号：US12300694
申请日：2008-05-15
申请人： Brian J. Waibel , Val J. Krukonis
发明人： Brian J. Waibel , Val J. Krukonis
CPC分类号： B01D11/0449 , B01D11/0457 , B01D11/0488 , B01D11/0492 , C07C29/86 , Y02P20/544 , Y02P20/57 , C07C31/08
摘要： The present invention provides methods and systems for extracting ethanol from an ethanol-water solution comprising (1) extracting ethanol from an ethanol-water solution with a first solvent comprising an esterified fatty acid, wherein the esterified fatty acid comprises a hydroxylated fatty acid component and an alcohol component such that the alcohol component is a C3-6 alcohol, such that the distribution coefficient for ethanol in the mixture of the ethanol-water solution and the first solvent is at least 0.02 favoring the transfer of ethanol from the ethanol-water solution to the first solvent, thereby extracting the ethanol from the ethanol-water solution into the first solvent, and (2) extracting the ethanol-enriched first solvent with carbon dioxide, such that the carbon dioxide is at a liquid or near supercritical phase, wherein the distribution coefficient for ethanol in a mixture of the first solvent and the carbon dioxide is at least 0.1 favoring the transfer of ethanol from the first solvent to the carbon dioxide.
摘要翻译： 本发明提供从乙醇 - 水溶液中提取乙醇的方法和系统，其包括（1）用乙醇 - 水溶液从含有酯化脂肪酸的第一溶剂中提取乙醇，其中酯化脂肪酸包含羟基化脂肪酸组分和 醇组分使得醇组分为C 3-6醇，使得乙醇 - 水溶液和第一溶剂的混合物中乙醇的分配系数为至少0.02，有利于从乙醇 - 水溶液中转移乙醇 从而将乙醇从乙醇 - 水溶液中提取到第一溶剂中，（2）用二氧化碳萃取富含乙醇的第一溶剂，使得二氧化碳处于液体或接近超临界相，其中 在第一溶剂和二氧化碳的混合物中乙醇的分配系数至少为0.1，有利于乙醇的转移 第一溶剂至二氧化碳。
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7.发明授权Device and method for non-dispersive contacting of liquid—liquid reactive system 有权液 - 液反应体系非分散接触装置及方法公开(公告)号：US07207445B2
公开(公告)日：2007-04-24
申请号：US10813815
申请日：2004-03-31
申请人： Ujjwal Manna , Ram Prakash Verma , Sarvesh Kumar , Sukumar Banik , Arpita Dasgupta , Shankar Khatua
发明人： Ujjwal Manna , Ram Prakash Verma , Sarvesh Kumar , Sukumar Banik , Arpita Dasgupta , Shankar Khatua
CPC分类号： B01D11/0449
摘要： An apparatus for separating impurities from a liquid by a non-dispersive contacting of a liquid—liquid reactive systems, the liquids being immiscible with each other, having a cylindrical column separated into a first stage and a second stage, a plurality of modules of packed metallic fibers mounted in the first stage of the column on a support, a first distributor provided in the first stage of the column for distributing a first liquid located above the support such that the first liquid completely wets the fibers by capillary action and forms a film thereon, a second distributor fitted at a bottom portion of the second stage for distributing a second liquid containing impurities on to the metallic fibers, wherein the second liquid flows concurrently with said first liquid so that the impurities present in the second liquid react with the first liquid and dissolve therein and a separator connected to a bottom of said column separates the first liquid and purified second liquid.
摘要翻译： 一种用于通过液 - 液反应体系的非分散接触从液体中分离杂质的装置，所述液体彼此不混溶，具有分离成第一级和第二级的圆柱形柱，多个包装模块 金属纤维安装在支柱的第一阶段，第一分配器设置在塔的第一阶段，用于分配位于支撑件上方的第一液体，使得第一液体通过毛细作用完全润湿纤维并形成膜 第二分配器装配在第二级的底部，用于将含有杂质的第二液体分配到金属纤维上，其中第二液体与所述第一液体同时流动，使得存在于第二液体中的杂质与第一液体反应 液体并在其中溶解，并且连接到所述塔底部的分离器分离第一液体和净化的第二液体。
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公开(公告)号：US20020030013A1
公开(公告)日：2002-03-14
申请号：US09754159
申请日：2001-01-04
发明人： Berthold Berend Breman , Jan Visser
IPC分类号： B01D017/02
CPC分类号： B01D11/0449 , B01D11/0457 , Y10S210/05
摘要： Claimed are a process and an apparatus for extracting a component dissolved in a liquid by means of liquid-liquid extraction using an extraction liquid which is immiscible or only partially miscible with the liquid, in which process the extraction liquid is dispersed in the liquid in a dispersion apparatus and then coalesced in a coalescer, after which the extraction liquid, the specific weight of which differs by at least 5% from the specific weight of the liquid to be extracted in which the component to be extracted is to be found, is separated from the liquid by gravity in a phase separator, in which process in order to obtain an efficiency per extraction stage of at least 0.9 at an average residence time of at most 15 seconds in the dispersion apparatus and of at most 300 seconds in the phase separator, at a linear velocity in the coalescer related to its cross-section of at least 30 m/hour: a. the dispersion apparatus used is a centrifugal pump which will give droplets having an average diameter of 5 to 500 nullm, b. the coalescer used is a packed bed of 5-100 cm high composed of dimensionally stable particles wettable by the extraction liquid having an average particle size of 0.05 to 2 mm, and c. the coagulated phase in the phase separator is separated at a linear velocity related to the cross-section of the phase separator of 0.1 to 0.7 times the linear velocity in the coalescer.
摘要翻译： 本发明提供了一种通过使用与液体不混溶或仅部分混溶的萃取液的液 - 液萃取来提取溶解在液体中的组分的方法和装置，在该方法中，萃取液在液体中分散在液体中 分散装置，然后在聚结器中聚结，之后将其比重与要提取的组分的待提取液体的比重相差至少5％的提取液分离， 在相分离器中通过重力从液体中取出液体，其中为了在分散装置中平均停留时间至多为15秒，在相分离器中至多300秒，每个萃取阶段获得至少0.9的效率 在与聚结器相关的线速度至少为30m /小时的横截面上：a。 使用的分散装置是一种离心泵，其将产生平均直径为5至500μm的液滴，b。 所使用的聚结器是由平均粒度为0.05至2mm的提取液可湿性的尺寸稳定的颗粒组成的5-100cm高的填充床，c。 相分离器中的凝固相以与分离器的横截面相关的线速度分离成聚结器中的线速度的0.1至0.7倍。
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公开(公告)号：US4258010A
公开(公告)日：1981-03-24
申请号：US849448
申请日：1977-11-07
申请人： Laszlo Rozsa , Lajos Meszaros , Ferenc Mogyorodi
发明人： Laszlo Rozsa , Lajos Meszaros , Ferenc Mogyorodi
IPC分类号： B01D11/04
CPC分类号： B01D11/0449 , C07C68/08
摘要： Apparatus for solvent extraction of a mother liquor with a solvent that is immiscible with and has a different specific gravity than the mother liquor, is disclosed. Means are provided for introducing into an extraction chamber, the solvent, the mother liquor and a carrier gas. Such means simultaneously serve to atomize the solvent and the mother liquor and disperse same in the carrier gas whereby upon introduction a cloud phase is produced in the chamber.The introducing and simultaneously atomizing is carried out through one and the same spray nozzle. Condensation means are arranged in the extraction chamber and function to terminate the cloud phase and produce a condensed extracted mother liquor phase and a condensed solvent phase containing the substance to be extracted. Means are provided for separating the condensed extracted mother liquor phase from the condensed solvent phase on the basis of the different specific gravities of same.
摘要翻译： 公开了一种用与母液不混溶且具有不同比重的溶剂溶剂萃取母液的设备。 提供用于将萃取室，溶剂，母液和载气引入的装置。 这种装置同时用于雾化溶剂和母液并将其分散在载体气体中，由此在引入时在室中产生云相。 引入并同时雾化通过同一个喷嘴进行。 在提取室中设置冷凝装置，并且起作用以终止浊相，并产生冷凝的提取母液相和含有待提取物质的冷凝溶剂相。 提供了用于根据不同的比重将浓缩的萃取母液相与冷凝的溶剂相分离的方法。
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公开(公告)号：US3207691A
公开(公告)日：1965-09-21
申请号：US23038562
申请日：1962-10-15
申请人： SHELL OIL CO
发明人： MES PIETER A
CPC分类号： B01D11/0449 , B01D11/043 , C10G17/06 , C10G21/00
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