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    Process for producing 1-benzyl-4-[(5,6-dimethoxy-1-indanon)-2-yl]methylpiperidine or hydrochloride thereof
    41.
    发明授权
    Process for producing 1-benzyl-4-[(5,6-dimethoxy-1-indanon)-2-yl]methylpiperidine or hydrochloride thereof 失效
    1-苄基-4 - [（5,6-二甲氧基-1-茚满酮）-2-基]甲基哌啶或其盐酸盐的制备方法

    公开(公告)号：US07332606B2

    公开(公告)日：2008-02-19

    申请号：US11546444

    申请日：2006-10-12

    Applicant: Akio Imai

    Inventor： Akio Imai

    IPC: C07D211/02 ,  C07D211/14

    CPC classification number: C07D211/32

    Abstract: 1-Benzyl-4-[(5,6-dimethoxy-1-indanon)-2-yl]methylpiperidine or hydrochloride thereof, which is useful as a drug, can be produced in high purity by safer and easier operations suitable for industrial production by subjecting 1-benzyl-4-[(5,6-dimethoxy-1-indanon)-2-ylidene]methyl-piperidine or a solvate thereof to catalytic hydrogenation in the presence of a palladium-alumina catalyst and if necessary, converting the thus obtained compound to its hydrochloride.

    Abstract translation: 可用作药物的1-苄基-4 - [（5,6-二甲氧基-1-茚满酮）-2-基]甲基哌啶或其盐酸盐可以通过适合于工业生产的更安全和更容易的操作而以高纯度制备 通过在钯 - 氧化铝催化剂的存在下使1-苄基-4 - [（5,6-二甲氧基-1-茚满酮）-2-亚基]甲基 - 哌啶或其溶剂合物进行催化氢化，如果需要， 从而得到化合物至其盐酸盐。

    α-Olefin polymerization catalyst and process for producing α-olefin polymer
    42.
    发明授权
    α-Olefin polymerization catalyst and process for producing α-olefin polymer 失效
    α-烯烃聚合催化剂和生产α-烯烃聚合物的方法

    公开(公告)号：US06838412B2

    公开(公告)日：2005-01-04

    申请号：US10282181

    申请日：2002-10-29

    Applicant: Makoto Satoh ,  Yasuki Fujiwara ,  Akio Imai

    Inventor： Makoto Satoh ,  Yasuki Fujiwara ,  Akio Imai

    IPC: C08F4/658 ,  C08F4/60 ,  C08F4/642 ,  C08F10/00 ,  C08F4/02

    CPC classification number: C08F10/00 ,  C08F4/6565

    Abstract: An α-olefin polymerization catalyst comprising (A) a solid catalyst component containing a titanium compound obtained by treating a solid product having a titanium content of 1.5% by weight or less obtained by reducing Ti(OR1)aX4-n (R1 represents a hydrocarbon group having 1 to 20 carbon atoms, X represents a halogen atom and a represents a number satisfying 0

    Abstract translation: 一种α-烯烃聚合催化剂，其包含（A）含有钛化合物的固体催化剂组分，所述钛化合物通过处理通过还原Ti（OR 1）aX 4-n（R 2）获得的钛含量为1.5重量％以下的固体产物 在具有Si-O键的有机硅化合物的存在下，使用有机镁化合物与式（1）表示碳原子数1〜20的烃基，X表示卤素原子，a表示满足0

    .alpha.-olefin polymerization catalyst and process for producing .alpha.-olefin polymer
    43.
    发明授权
    .alpha.-olefin polymerization catalyst and process for producing .alpha.-olefin polymer 失效
    α-烯烃聚合催化剂和α-烯烃聚合物的制备方法

    公开(公告)号：US6133189A

    公开(公告)日：2000-10-17

    申请号：US660757

    申请日：1996-06-06

    Applicant: Yasuki Fujiwara ,  Makoto Satoh ,  Akio Imai

    Inventor： Yasuki Fujiwara ,  Makoto Satoh ,  Akio Imai

    IPC: C08F4/654 ,  C08F4/60 ,  C08F4/646 ,  C08F10/00 ,  B01J31/00

    CPC classification number: C08F10/00

    Abstract: An .alpha.-olefin polymerization catalyst which comprises:(A) a solid catalyst component containing a tetra-valent titanium obtained by treating a magnesium compound having an Mg--O bond in its molecule with a titanium halide;(B) an organoaluminum compound; and(C) an organosilicon compound represented by the general formula R.sup.1 R.sup.2 Si(OR.sup.3).sub.2wherein R.sup.1 represents a hydrocarbon group having 4 to 30 carbon atoms wherein a carbon bonded directly to Si is a tertiary carbon, R.sup.2 represents a straight chain hydrocarbon group having 2 to 10 carbon atoms and R.sup.3 represents a hydrocarbon group having 1 to 10 carbon atoms, or the general formula R.sup.4 R.sup.5 Si(OR.sup.6).sub.2wherein R.sup.4 and R.sup.5 are hydrocarbon groups having an alicyclic hydrocarbon having 5 carbon atoms as a basic structure, R.sup.4 and R.sup.5 may be the same or different, and R.sup.6 represents a hydrocarbon group having 1 to 10 carbon atoms, and a process for producing .alpha.-olefin with said catalyst.

    Abstract translation: 一种α-烯烃聚合催化剂，其包括：（A）含有通过用卤化钛处理其分子中具有Mg-O键的镁化合物而获得的四价钛的固体催化剂组分; （B）有机铝化合物; 和（C）由通式R 1 R 2 Si（OR 3）2表示的有机硅化合物，其中R 1表示碳原子数4〜30的烃基，其中直接与Si键合的碳为叔碳，R2表示具有2个碳原子的直链烃基 至10个碳原子，R 3表示具有1〜10个碳原子的烃基，或通式R4R5Si（OR6）2，其中R4和R5是具有5个碳原子的脂环族烃基作为碱性结构的烃基，R4和R5可以 相同或不同，R 6表示碳原子数为1〜10的烃基，以及使用该催化剂制造α-烯烃的方法。

    .alpha.-olefin polymerization catalyst and process for producing .alpha.-olefin polymer
    44.
    发明授权
    .alpha.-olefin polymerization catalyst and process for producing .alpha.-olefin polymer 失效
    α-烯烃聚合催化剂和α-烯烃聚合物的制备方法

    公开(公告)号：US6051526A

    公开(公告)日：2000-04-18

    申请号：US665650

    申请日：1996-06-18

    Applicant: Makoto Satoh ,  Yasuki Fujiwara ,  Akio Imai

    Inventor： Makoto Satoh ,  Yasuki Fujiwara ,  Akio Imai

    IPC: C08F4/658 ,  C08F10/00 ,  B01J31/00

    CPC classification number: C08F10/00

    Abstract: An .alpha.-olefin polymerization catalyst which comprises (A) a solid catalyst component obtained by treating a solid product obtained by contacting a compound having an M--O bond (M is the element of the 1st, 2nd, 13th and 14th Groups in the Periodic Table) with an organomagnesium compound in the presence of an electron donor, with an electron donor and successively a halide compound of metal of the 4th to 6th Groups in the Periodic Table, (B) an organoaluminum compound, and (C) an electron donative compound, and a process for producing an .alpha.-olefin polymer polymerizing an .alpha.-olefin with said catalyst.

    Abstract translation: 一种α-烯烃聚合催化剂，其包含（A）通过处理通过使具有MO键的化合物（M是元素周期表中第1，第2，第13和第14组的元素）获得的固体产物而获得的固体催化剂组分， 在电子给体的存在下与电子给体连续地在周期表中的第4至第6族金属的卤化物化合物，（B）有机铝化合物和（C）给电子化合物， 以及用所述催化剂生产α-烯烃聚合α-烯烃聚合物的方法。

    Catalyst for olefinic hydrocarbon polymerization and process for producing olefinic hydrocarbon polymer
    45.
    发明授权
    Catalyst for olefinic hydrocarbon polymerization and process for producing olefinic hydrocarbon polymer 失效
    烯烃聚合催化剂和生产烯烃聚合物的方法

    公开(公告)号：US5122493A

    公开(公告)日：1992-06-16

    申请号：US675823

    申请日：1991-03-27

    Applicant: Hayato Saba ,  Keisaku Yamamoto ,  Akio Imai ,  Kiyoyuki Sugimori ,  Kizuku Wakatsuki

    Inventor： Hayato Saba ,  Keisaku Yamamoto ,  Akio Imai ,  Kiyoyuki Sugimori ,  Kizuku Wakatsuki

    IPC: C08F4/60 ,  C08F4/68 ,  C08F10/00

    CPC classification number: C08F10/00

    Abstract: An inert hydrocarbon solvent-soluble catalyst for polymerization of olefinic hydrocarbons and a process for producing an olefinic polymer using the same are disclosed, the catalyst being composed of (A) a reaction product obtained by reacting (a) at least one vanadium compound represented by formula:VO(OR).sub.m X.sub.3-mwherein R represents a hydrocarbon group; X represents a halogen atom; and m represents a real number of from 0 to 3, and (b) a dihydroxy hydrocarbon compound constituted of a straight chain hydrocarbon skeleton containing from 2 to 12 carbon atoms and having a hydroxyl group at each of both terminals thereof and at least one hydrocarbon branch bonded to said hydrocarbon skeleton in an inert hydrocarbon solvent at an (a) to (b) molar ratio of from 1:0.5 to 1:1.4 and (B) at least one organoaluminum compound represented by formula:R'.sub.n AlX'.sub.3-nwherein R' represents a hydrocarbon group X' represents a halogen atom; and n represents a real number more than 0 and less than 3. Olefinic hydrocarbon polymers having narrow distributions of molecular weight and composition can be produced with high efficiency and high polymerization activity without being accompanied by obstruction or contamination of equipment due to precipitation of a catalyst.

    Ethylene-.alpha.-olefin copolymer and process for producing the same
    46.
    发明授权
    Ethylene-.alpha.-olefin copolymer and process for producing the same 失效
    乙烯 - （ALPHA） - 烯烃共聚物及其制造方法

    公开(公告)号：US5082908A

    公开(公告)日：1992-01-21

    申请号：US363654

    申请日：1989-06-08

    Applicant: Akio Imai ,  Kiyoyuki Sugimori ,  Keisaku Yamamoto ,  Minoru Takane

    Inventor： Akio Imai ,  Kiyoyuki Sugimori ,  Keisaku Yamamoto ,  Minoru Takane

    IPC: C08F4/68 ,  C08F210/00

    CPC classification number: C08F210/00

    Abstract: An ethylene-.alpha.-olefin copolymer is disclosed, which comprises ethylene and an .alpha.-olefin having from 3 to 10 carbon atoms, has an ethylene/.alpha.-olefin molar ratio of from 88/12 to 98/2, and which has a number average molecular weight of from 35,000 to 80,000 and a weight average molecular weight/number average molecular weight ratio of from 1.8/1 to 3.0/1 as determined by gel permeation chromatography. A process for producing the ethylene-.alpha.-olefin copolymer is also disclosed. The ethylene-.alpha.-olefin copolymer exhibits excellent transparency and excellent low-temperature heat-sealing properties. The process is advantageous from the standpoint of equipment, energy and cost.

    Modified diene polymer rubbers
    47.
    发明授权
    Modified diene polymer rubbers 失效
    改性二烯聚合物橡胶

    公开(公告)号：US4885338A

    公开(公告)日：1989-12-05

    申请号：US188326

    申请日：1988-05-04

    Applicant: Hiroyoshi Takao ,  Akio Imai ,  Tomoaki Seki

    Inventor： Hiroyoshi Takao ,  Akio Imai ,  Tomoaki Seki

    IPC: C08C19/42

    CPC classification number: C08C19/42

    Abstract: A process for preparing modified diene polymer rubbers having an increased impact resilience and a reduced hardness at low temperatures and useful as rubber materials for automobile tires and other industries which comprises producing an alkali metal-containing conjugated diene polymer, and reacting the alkali metal-containing polymer with a modifier selected from the group consisting of a nitroalkyl acrylate of the formula: ##STR1## wherein R.sup.1 and R.sup.2 are independently an alkyl group and n is an integer, and a nitroamino compound of the formula: ##STR2## wherein R.sup.3 to R.sup.6 are independently an alkyl group, and m is an integer, said alkali metal-containing diene polymer being prepared by a living anionic polymerization using an alkali metal-based catalyst or by an addition reaction of a diene polymer having conjugated diene units and an alkali metal-based catalyst in a hydrocarbon solvent. The modified diene polymers can be incorporated with usual rubber additives to provide rubber compositions for various purposes, and the cured products show an increased impact resilience and a reduced hardness at low temperatures.

    Process for producing thermoplastic elastomers
    48.
    发明授权
    Process for producing thermoplastic elastomers 失效
    制造热塑性弹性体的方法

    公开(公告)号：US4845173A

    公开(公告)日：1989-07-04

    申请号：US830041

    申请日：1986-02-18

    Applicant: Nobuyuki Yoshida ,  Akio Imai ,  Tomoaki Seki

    Inventor： Nobuyuki Yoshida ,  Akio Imai ,  Tomoaki Seki

    IPC: C08F297/00 ,  C08F297/04

    CPC classification number: C08F297/04

    Abstract: A process for producing a thermoplastic elastomer comprising a block copolymer of the A-B-A' type, wherein A is a monovinyl aromatic hydrocarbon polymer block, B is a conjugated diolefin polymer block, and A' is either the same as A or a polymer block derived from a dialkenyl aromatic hydrocarbon or a dihalogenated hydrocarbon, which process comprises polymerizing a monovinyl aromatic hydrocarbon in a polymerization medium in the presence of an organomonolithium compound as a polymerization initiator, adding a conjugated diolefin to perform block copolymerization, and further adding a monovinyl aromatic hydrocarbon to perform polymerization or in the alternative, adding a dialkenyl aromatic hydrocarbon or a dihalogenated hydrocarbon to perform coupling, wherein the monomer components are used in such amounts that the weight ratio of (A+A') to B ranges from 10/90 to 65/35, and a chained aliphatic hydrocarbon solvent containing from 0.0001 to 0.1 wt % of a Lewis basic compound is used as the polymerization medium, is disclosed. According to the process of the invention, the desired thermoplastic elastomer having good physical properties is readily obtainable with high reproducibility.

    Abstract translation: 一种制备包含ABA'型嵌段共聚物的热塑性弹性体的方法，其中A是单乙烯基芳族烃聚合物嵌段，B是共轭二烯烃聚合物嵌段，A'与A相同或衍生自 二烯基芳烃或二卤代烃，该方法包括在有机锂锂化合物作为聚合引发剂的存在下在聚合介质中聚合单乙烯基芳烃，加入共轭二烯烃进行嵌段共聚，并进一步加入单乙烯基芳烃 进行聚合，或者在替代方案中，加入二烯基芳族烃或二卤代烃进行偶联，其中单体成分的用量使得（A + A'）与B的重量比为10/90〜65 / 35，使用含有0.0001〜0.1重量％路易斯碱性化合物的链状脂肪族烃溶剂 公开了聚合介质。 根据本发明的方法，具有良好物理性能的所需热塑性弹性体可以以高重现性容易地获得。

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