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    Integrated Process to Coproduce Trans-1-Chloro-3,3,3-Trifluoropropene, Trans-1,3,3,3-Tetrafluoropropene, and 1,1,1,3,3-Pentafluoropropane
    42.
    发明申请
    Integrated Process to Coproduce Trans-1-Chloro-3,3,3-Trifluoropropene, Trans-1,3,3,3-Tetrafluoropropene, and 1,1,1,3,3-Pentafluoropropane 有权
    共同生产反式-1-氯-3,3,3-三氟丙烯，反式1,3,3,3-四氟丙烯和1,1,1,3,3-五氟丙烷的综合方法

    公开(公告)号：US20120059200A1

    公开(公告)日：2012-03-08

    申请号：US13219831

    申请日：2011-08-29

    Applicant: Konstantin A. Pokrovski ,  Daniel C. Merkel ,  Haiyou Wang ,  Hsueh Sung Tung ,  Ian Shankland

    Inventor： Konstantin A. Pokrovski ,  Daniel C. Merkel ,  Haiyou Wang ,  Hsueh Sung Tung ,  Ian Shankland

    IPC: C07C21/18 ,  C07C19/08

    CPC classification number: C07C17/25 ,  C01B7/0706 ,  C01B7/0712 ,  C07C17/087 ,  C07C17/206 ,  C07C17/383 ,  C07C21/18 ,  Y02P20/125 ,  Y02P20/582 ,  C07C19/08

    Abstract: Disclosed is an integrated manufacturing process to co-produce (E)1-chloro-3,3,3-trifluoropropene, (E)1,3,3,3-tetrafluoropropene, and 1,1,1,3,3-pentafluoro-propane starting from a single chlorinated hydrocarbon feed stock, 240fa. The process includes a combined liquid or vapor phase reaction/purification operation which directly produces (E)1-chloro-3,3,3-trifluoropropene (1233zd(E)) from 240fa. In the second liquid phase fluorination reactor 1233zd(E) is contacted with HF in the presence of catalyst to produce 1,1,1,3,3-pentafluoropropane (245fa) with high conversion and selectivity. A third reactor is used for dehydrofluorination of 245fa to produce (E)1,3,3,3-tetrafluoropropene (1234ze(E)) by contacting in the liquid phase with a caustic solution or in the vapor phase using a dehydrofluorination catalyst. This operation may be followed by one or more purification processes to recover the 1234ze(E) product.

    Abstract translation: 公开了共同生产（E）1-氯-3,3,3-三氟丙烯，（E）1,3,3,3-四氟丙烯和1,1,1,3,3-五氟 丙烷从单一氯化烃原料240fa开始。 该方法包括从240fa直接产生（E）1-氯-3,3,3-三氟丙烯（1233zd（E））的组合的液相或汽相反应/纯化操作。 在第二液相氟化反应器1233zd（E）中，在催化剂存在下与HF接触，得到具有高转化率和选择性的1,1,1,3,3-五氟丙烷（245fa）。 第三反应器用于245fa的脱氟化氢以通过使用脱氟化氢催化剂在液相中与苛性碱溶液接触或以蒸气相接触来制备（E）1,3,3,3-四氟丙烯（1234ze（E））。 该操作之后可以进行一个或多个纯化过程以恢复1234ze（E）产物。

    PROCESS FOR PRODUCING FLUOROPROPENES
    43.
    发明申请
    PROCESS FOR PRODUCING FLUOROPROPENES 有权
    生产氟泛酮的方法

    公开(公告)号：US20120053370A1

    公开(公告)日：2012-03-01

    申请号：US13226019

    申请日：2011-09-06

    Applicant: Daniel C. Merkel ,  Rajiv R. Singh ,  Hsueh Sung Tung

    Inventor： Daniel C. Merkel ,  Rajiv R. Singh ,  Hsueh Sung Tung

    IPC: C07C17/25

    CPC classification number: C07C21/18 ,  C07C17/206 ,  C07C17/25 ,  C07C19/10 ,  C07C19/08

    Abstract: Dehydrohalogenation processes for the preparation of fluoropropenes from corresponding halopropanes, in which the fluoropropenes have the formula CF3CY═CXNHP, wherein X and Y are independently hydrogen or a halogen selected from fluorine, chlorine, bromine and iodine; and N and P are independently integers equal to 0, 1 or 2, provided that (N+P)=2.

    Abstract translation: 用于从相应的卤代丙烷制备氟丙烯的脱卤化氢方法，其中氟丙烯具有式CF 3 C Y = C X N H P，其中X和Y独立地是氢或选自氟，氯，溴和碘的卤素; 并且N和P独立地为等于0,1或2的整数，条件是（N + P）= 2。

    Method for producing 2-chloro-3,3,3,-trifluoropropene (HCFC-1233xf)
    44.
    发明授权
    Method for producing 2-chloro-3,3,3,-trifluoropropene (HCFC-1233xf) 有权
    2-氯-3,3,3-三氟丙烯（HCFC-1233xf）的制备方法

    公开(公告)号：US08119845B2

    公开(公告)日：2012-02-21

    申请号：US12880951

    申请日：2010-09-13

    Applicant: Daniel C. Merkel ,  Hsueh S. Tung

    Inventor： Daniel C. Merkel ,  Hsueh S. Tung

    IPC: C07C17/00

    CPC classification number: C07C17/206 ,  C07C17/06 ,  C07C17/087 ,  C07C17/20 ,  C07C17/25 ,  C07C17/42 ,  C07C21/18

    Abstract: The present invention relates to an improved method for manufacturing 2-chloro-3,3,3,-trifluoropropene (HCFC-1233xf) by reacting 1,1,2,3-tetrachloropropene, 1,1,1,2,3-pentachloropropane, and/or 2,3,3,3-tetrachloropropene with hydrogen fluoride, in a vapor phase reaction vessel in the presence of a vapor phase fluorination catalyst and stabilizer. HCFC-1233xf is an intermediate in the production of 2,3,3,3-tetrafluoropropene (HFO-1234yf) which is a refrigerant with low global warming potential.

    Abstract translation: 本发明涉及一种通过使1,1,2,3-四氯丙烯，1,1,1,2,3-五氯丙烷与1,1,3,3-四氯丙烯反应制备2-氯-3,3,3-三氟丙烯（HCFC-1233xf）的改进方法 ，和/或2,3,3,3-四氯丙烯与氟化氢在气相反应容器中在气相氟化催化剂和稳定剂存在下反应。 HCFC-1233xf是生产2,3,3,3-四氟丙烯（HFO-1234yf）的中间体，它是具有低全球变暖潜能的制冷剂。

    Process for producing fluoropropenes
    47.
    发明授权
    Process for producing fluoropropenes 有权
    制备氟丙烯的方法

    公开(公告)号：US07803973B2

    公开(公告)日：2010-09-28

    申请号：US12104176

    申请日：2008-04-16

    Applicant: Daniel C. Merkel ,  Rajiv R. Singh ,  Hsueh Sung Tung

    Inventor： Daniel C. Merkel ,  Rajiv R. Singh ,  Hsueh Sung Tung

    IPC: C07C17/00

    CPC classification number: C07C21/18 ,  C07C17/206 ,  C07C17/25 ,  C07C19/10 ,  C07C19/08

    Abstract: Dehydrohalogenation processes for the preparation of fluoropropenes from corresponding halopropanes, in which the fluoropropenes have the formula CF3CY═CXNHP, wherein X and Y are independently hydrogen or a halogen selected from fluorine, chlorine, bromine and iodine; and N and P are independently integers equal to 0, 1 or 2, provided that (N+P)=2.

    Abstract translation: 用于从相应的卤代丙烷制备氟丙烯的脱卤化氢方法，其中氟丙烯具有式CF 3 C Y = C X N H P，其中X和Y独立地是氢或选自氟，氯，溴和碘的卤素; 并且N和P独立地为等于0,1或2的整数，条件是（N + P）= 2。

    PROCESSES FOR HYDROFLUORINATION OF 2-CHLORO-3,3,3-TRIFLUOROPROPENE TO 2-CHLORO-1,1,1,2-TETRAFLUOROPROPANE
    50.
    发明申请
    PROCESSES FOR HYDROFLUORINATION OF 2-CHLORO-3,3,3-TRIFLUOROPROPENE TO 2-CHLORO-1,1,1,2-TETRAFLUOROPROPANE 有权
    将2-氯代-3,3,3-三氟苯酚氢化成2-氯-1,1,1,2-四氢呋喃的方法

    公开(公告)号：US20090312585A1

    公开(公告)日：2009-12-17

    申请号：US12484588

    申请日：2009-06-15

    Applicant: Daniel C. Merkel ,  Robert C. Johnson ,  Hsueh Sung Tung

    Inventor： Daniel C. Merkel ,  Robert C. Johnson ,  Hsueh Sung Tung

    IPC: C07C19/08

    CPC classification number: C07C17/087 ,  C07C19/10

    Abstract: A process for making 2-chloro-1,1,1,2-tetrafluoropropane. The process has the step of contacting 2-chloro-3,3,3-trifluoropropene with hydrogen fluoride in the presence of a catalyst having about 25 to about 99.9 mole percent antimony pentachloride and about 0.1 to about 75 mole percent of a metal of a Lewis acid under conditions sufficient to form the 2-chloro-1,1,1,2-tetrafluoropropane. There is a second process for making 2-chloro-1,1,1,2-tetrafluoropropane. The process has the step of hydrofluorinating about 75 to about 99.9 mole percent 2-chloro-3,3,3-trifluoropropene and about 0.1 to about 25 mole percent of one or more other hydrocarbons having at least one chlorine atom in the presence of a catalyst of fluorinated antimony pentachloride under conditions sufficient to form the 2-chloro-1,1,1,2-tetrafluoropropane. There is yet another process for hydrofluorinating 2-chloro-3,3,3-trifluoropropene to 2-chloro-1,1,1,2-tetrafluoropropane. The process has the step of contacting the 2-chloro-3,3,3-trifluoropropene with hydrogen fluoride in the presence of a vapor phase catalyst under conditions sufficient to form the 2-chloro-1,1,1,2-tetrafluoropropane.

    Abstract translation: 制备2-氯-1,1,1,2-四氟丙烷的方法。 该方法具有在催化剂存在下使2-氯-3,3,3-三氟丙烯与氟化氢接触的步骤，该催化剂具有约25至约99.9摩尔％的五氯化锑和约0.1至约75摩尔％的金属 路易斯酸在足以形成2-氯-1,1,1,2-四氟丙烷的条件下进行。 制备2-氯-1,1,1,2-四氟丙烷的第二种方法。 该方法具有在存在下存在下，将约75-约99.9摩尔％的2-氯-3,3,3-三氟丙烯和约0.1-约25摩尔％的一种或多种其它具有至少一个氯原子的烃氢氟化的步骤 在足以形成2-氯-1,1,1,2-四氟丙烷的条件下的氟化五氯化锑催化剂。 还有将2-氯-3,3,3-三氟丙烯氢氟化为2-氯-1,1,1,2-四氟丙烷的另一种方法。 该方法具有在气相催化剂存在下，在足以形成2-氯-1,1,1,2-四氟丙烷的条件下使2-氯-3,3,3-三氟丙烯与氟化氢接触的步骤。

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