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    METHOD OF MAKING FLUOROPOLYMERS WITH A POLYIODIDE, COMPOSITIONS AND ARTICLES THEREOF
    43.
    发明申请
    METHOD OF MAKING FLUOROPOLYMERS WITH A POLYIODIDE, COMPOSITIONS AND ARTICLES THEREOF 有权
    制备具有聚酰亚胺，组合物及其制品的氟聚合物的方法

    公开(公告)号：US20150344605A1

    公开(公告)日：2015-12-03

    申请号：US14650091

    申请日：2013-11-27

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Klaus Hintzer ,  Florian D. Jochum ,  Harald Kaspar ,  Kai H. Lochhaas ,  Tilman C. Zipplies

    IPC: C08F214/22

    CPC classification number: C08F214/222 ,  C08F2/16 ,  C08F14/16 ,  C08F14/18 ,  C08F14/26 ,  C08F214/262

    Abstract: Described herein is a method of making a fluoropolymer and fluoropolymers thereof, wherein the method comprises: (a) providing an aqueous solution comprising a water soluble polyiodide salt of Formula (I): M+y[I—I—(I)Jy− wherein M is a cation group having a valence y, y is an integer of at least 1 and n is an integer of at least 1; and (b) initiating polymerization of a monomer in the aqueous solution, wherein the monomer is a fluorinated monomer.

    Abstract translation: 本文描述了制备氟聚合物及其含氟聚合物的方法，其中所述方法包括：（a）提供包含式（I）的水溶性多碘化物盐的水溶液：M + y [I-I-（I） 其中M是具有价数y的阳离子基团，y是至少为1的整数，n是至少为1的整数; 和（b）引发单体在水溶液中的聚合，其中单体是氟化单体。

    HIGHLY FLUORINATED POLYMERS
    44.
    发明申请
    HIGHLY FLUORINATED POLYMERS 有权
    高荧光聚合物

    公开(公告)号：US20150274868A1

    公开(公告)日：2015-10-01

    申请号：US14646980

    申请日：2013-11-21

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Klaus Hintzer ,  Harald Kaspar ,  Herbert Koenigsmann ,  Helmut Traunspurger ,  Tilman C. Zipplies

    IPC: C08F214/26

    CPC classification number: C08L27/18 ,  C08F214/262

    Abstract: A method of making a highly fluorinated polymers and resulting aqueous mixtures. The method comprising polymerizing one or more perfluorinated monomers in an aqueous emulsion polymerization in the presence of a polymerizable fluorinated emulsifier to form a perfluorinated polymer. The polymerizable fluorinated emulsifier has the formula X2C═CX(CF2)m(CH2)n[O—(CX2)p]q—[O—(CX2)r]s—[O—(CX2—CX2)]t—[(O)w—(CX2)u]v—[CH2]z—Y. The method also provides for isolating the highly fluorinated polymer and post-fluorinating the isolated highly fluorinated polymer.

    Abstract translation: 制备高度氟化聚合物和所得含水混合物的方法。 该方法包括在可聚合的氟化乳化剂的存在下在水乳液聚合中聚合一种或多种全氟化单体以形成全氟化聚合物。 可聚合的氟化乳化剂具有式X2C≡CX（CF2）m（CH2）n [O-（CX2）p] q- [O-（CX2）r] s- [O-（CX2-CX2）] t- [ （O）w - （CX2）u] v- [CH2] z-Y。 该方法还提供了分离高度氟化的聚合物和后氟化分离的高度氟化的聚合物。

    METHOD FOR REMOVING PERFLUORINATED ALKANOIC ACIDS
    49.
    发明申请
    METHOD FOR REMOVING PERFLUORINATED ALKANOIC ACIDS 审中-公开

    公开(公告)号：US20190070599A1

    公开(公告)日：2019-03-07

    申请号：US16081808

    申请日：2017-03-02

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Tilman C. Zipplies ,  Klaus Hintzer ,  Helmut Traunspurger ,  Karl D. Weilandt

    IPC: B01J41/05 ,  B01J47/02 ,  C07C51/47

    Abstract: Provided are methods for removing a perfluorinated alkanoic acid from solutions containing the perfluorinated alkanoic acid and a fluorinated alkoxy acid. These methods include contacting the first solution with an anion-exchange resin to produce a second solution and a resultant anion-exchange resin having perfluorinated alkanoic acid adsorbed thereto, wherein the perfluorinated alkanoic acid is present in the first solution at a first concentration and is present in the second solution at a second concentration which is lower than the first concentration, and separating the second solution from the resultant anion-exchange resin.

    FLUORINATED COPOLYMER HAVING SULFONYL PENDANT GROUPS AND METHOD OF MAKING AN IONOMER
    50.
    发明申请
    FLUORINATED COPOLYMER HAVING SULFONYL PENDANT GROUPS AND METHOD OF MAKING AN IONOMER 审中-公开

    公开(公告)号：US20190027769A1

    公开(公告)日：2019-01-24

    申请号：US16082721

    申请日：2017-03-06

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： Gregg D. Dahlke ,  Denis Duchesne ,  Klaus Hintzer ,  Kai Helmut Lochhaas ,  Arne Thaler ,  Tilman C. Zipplies

    IPC: H01M8/1039 ,  H01M4/62 ,  H01M8/1032 ,  C08F214/26

    Abstract: The copolymer includes divalent units represented by formula: (I), one or more independently selected fluorinated divalent units, and —SO2X end groups. In this formula, b is 2 to 8, c is 0 to 2, and e is 1 to 8. In each SO2X, X is independently F, —NZH, —NZSO2(CF2)1−6SO2X′, —NZ[SO2(CF2)aSO2NZ]1−10SO2X′, or —OZ, wherein Z is a hydrogen, an alkali-metal cation or a quaternary ammonium cation, X′ is independently —NZH or —OZ, and each a is independently 1 to 6. The copolymer has an —SO2X equivalent weight of up to 1000. The method includes copolymerizing components including fluorinated olefin and a compound represented by formula CF2═CF—CF2(O—CbF2b)c—O—(CeF2e)—SO2X′, wherein b, c, and e are as defined above. A method of making a membrane using the copolymer or ionomer is also provided. A polymer electrolyte membrane that includes the copolymer or the ionomer and a membrane electrode assembly that includes such a polymer electrolyte membrane are also provided.

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