摘要:
In a gas chromatograph system having a column with a stationary phase and a carrier gas moving through the column to contact the stationary phase, the system being useful for detecting analytes in a sample, a method and apparatus for predicting the retention times for the analytes under various conditions, the method utilizing the steps of:a) detecting the analytes under a number of sets of given conditions;b) calculating values for various parameters characteristic of the system based on a mathematical model that includes a correction to compensate for the permeability of said column to said carrier gas;c) entering into the model the values for the characteristic parameters and at least one further set of conditions; andd) using the model to predict retention times for conditions other than those of step a;the apparatus composed of a data handling system including a model for predicting retention times at a variety of conditions of operation of the system, the model having a first set of inputs including retention times determined during a number of operating condition sets; and a second input representative of the permeability of the column to the carrier gas, the data handling system possessing a prediction mechanism for putting into the model a set of conditions other than those of a) above and for putting in the set of parameters, and for predicting retention times for those conditions other than those of a).
摘要:
Spectral bands are grouped for data acquisition in a spectrophotometer with a charge-coupled detector having a plurality of pixels. Preliminary data is generated on time-integrated radiation to the pixels for a sample. Maximum permitted exposure times for the pixels are calculated from the data and a predetermined maximum exposure. The maximum times are grouped so that for each group the ratio of the highest to the lowest maximum times is less than 100. A group run time is established for each group nominally less than the lowest maximum time in the group. Subgroups are created and ordered so that accumulated readout times for the pixels are less than wait times established to prevent readout contamination from subsequent charge buildup. The spectrophotometer is further operated on the sample for the run time of each group and subgroup to generate spectral data.
摘要:
A photolithography exposure control system tolerant of noisy pulsed light sources having a controllable variable attenuator. A detector monitors the exposure dose of a light pulse enabling a controller to trigger another light pulse, when a predetermined attenuator is positioned in its path. A high degree of exposure control is achieved with a minimum number of light pulses or shots.
摘要:
A Rowland circle-type polychromator with the Rowland circle arc pivotally connected to the concave grating. Separate adjustments are provides for shifting the spectral lines and focussing. A tie rod is used to adjust the focus of the spectral lines. Dectectors are predeterminedly spaced along the arc to simultaneously detect unique spectral lines for analysis of multiple elements contained in a single sample.
摘要:
An apparatus for monitoring a plasma torch includes a dedicated photometer which produces a signal representative of the temperature of a quartz tube of the torch, which signal can be used to reduce the temperature thereof.
摘要:
An electrode includes a plurality of nested concentric rings forming plenum chambers. Process gas is fed into the plenum chambers through capillary tubes. The gas is then delivered through slits between the rings into a plasma etching reactor.