公开(公告)号：US20050089457A1

公开(公告)日：2005-04-28

申请号：US10503532

申请日：2003-01-30

申请人： Michel Devic ,  Philippe Bonnet ,  Eric Lacroix

发明人： Michel Devic ,  Philippe Bonnet ,  Eric Lacroix

IPC分类号： B01J19/00 ,  B01J10/00 ,  B01J14/00 ,  B01J19/02 ,  B01J19/18 ,  C07B61/00 ,  C07C17/20 ,  C07C19/08 ,  F28D1/00

CPC分类号： B01J19/18 ,  B01J10/00 ,  B01J14/00 ,  B01J19/02 ,  B01J2219/00076 ,  B01J2219/00135 ,  B01J2219/0245

摘要： The present invention relates to a reactor suitable for liquid-phase fluorination and provided, as heating means, with at least one element fixed to the cover so as to be immersed to the bottom of the vessel, characterized in that the parts of said reactor that are liable to be in contact with the reaction medium, other than the heating element, are coated with a tetrafluoroethylene/hexafluoropropylene copolymer and in that the part of the heating element liable to be in contact with the reaction medium is made of silicon carbide.

公开(公告)号：US06447743B1

公开(公告)日：2002-09-10

申请号：US09601967

申请日：2000-08-09

申请人： Michel Devic ,  Lionel Delais

发明人： Michel Devic ,  Lionel Delais

IPC分类号： C01B1501

CPC分类号： B01J19/006 ,  B01J10/002 ,  B01J12/00 ,  B01J19/0066 ,  B01J19/1881 ,  B01J2219/00083 ,  B01J2219/00103 ,  B01J2219/00162 ,  B01J2219/00164 ,  C01B15/029

摘要： A catalytic process and a device for preparing, in absolute safely, aqueous hydrogen peroxide solutions at high concentration levels directly from hydrogen and oxygen; more particularly, a method whereby hydrogen and oxygen are injected, into the aqueous medium in proportions corresponding to the flammability range of the hydrogen-oxygen mixture, and are present in proportions outside the flammability range in the continuous gas phase. The invention also concerns a device for implementing the method.

摘要翻译： 催化方法和用于以绝对安全的方式从氢和氧直接制备高浓度水溶液的过氧化氢水溶液; 更具体地说，以与氧 - 氢混合物的可燃性范围相对应的比例将氢和氧注入到水介质中的方法，并且以连续气相中的可燃性范围外的比例存在。 本发明还涉及一种用于实现该方法的装置。

公开(公告)号：US5480788A

公开(公告)日：1996-01-02

申请号：US277948

申请日：1994-07-19

申请人： Michel Devic

发明人： Michel Devic

IPC分类号： A23B7/06 ,  A23B7/157 ,  A23L1/10 ,  A23L1/185 ,  A23L1/214 ,  A23L1/277 ,  A23L1/308 ,  A23L1/36 ,  C12P3/00 ,  A21D2/04 ,  D21C1/00

CPC分类号： C12Y111/01006 ,  A23B7/06 ,  A23B7/157 ,  A23L19/10 ,  A23L25/30 ,  A23L33/22 ,  A23L5/49 ,  A23L7/115 ,  A23L7/20

摘要： A variety of plant materials adopted for processing into, e.g., low-calorie vegetable fibers and dietary flours, are bleached by (1) soaking a plant material having a moisture content of up to 50% at a temperature ranging from 20.degree. to 100.degree. C. with an aqueous solution containing an alkaline agent and more than 100 g/l of hydrogen peroxide, and having a pH of at least 8.5, such that the aqueous solution is completely absorbed by the plant material without establishing any liquid phase; (2) heating the soaked plant material at a temperature ranging from 40.degree. to 100.degree. C. for a period of time sufficient to effect the bleaching, and washing the bleached plant material with water and drying it.

摘要翻译： 用于加工成例如低热量植物纤维和膳食面粉的各种植物材料通过（1）在20℃至100℃的温度范围内浸湿含水量高达50％的植物材料进行漂白 C.含有碱性试剂和大于100g / l过氧化氢的水溶液，pH值至少为8.5，使得水溶液被植物材料完全吸收而不建立任何液相; （2）在40〜100℃的温度范围内加热浸渍的植物材料一段足以进行漂白的时间，并用水洗涤漂白的植物材料并干燥。

公开(公告)号：US4812206A

公开(公告)日：1989-03-14

申请号：US99762

申请日：1987-09-22

申请人： Michel Devic ,  Robert Angelier

发明人： Michel Devic ,  Robert Angelier

IPC分类号： D21C9/00 ,  D21B1/16 ,  D21C3/22 ,  D21C9/02 ,  D21C9/10 ,  D21C9/16 ,  D21C3/26 ,  D21C3/00

CPC分类号： D21C9/1057

摘要： A process for bleaching a lignocellulosic matter in the form of a mechanical, thermomechanical, chemicomechanical or chemicothermomechanical papermaking pulp, or of wood chips while being converted into one of these pulp types by processing in a machine consisting essentially of two interpenetrating spiral surfaces wound around parallel shafts driven in synchronous rotation in the same direction inside a barrel which encloses them, and determining between upstream and downstream in the direction of forward travel of the matter a series of zones for drawing and braking the matter, which comprises combining a bleaching treatment using a reducing agent and a bleaching treatment using an oxidizing agent, characterized in that, after pretreatment using at least one metal-complexing or sequestering agent, the lignocellulosic matter undergoes a washing operation with an efficiency greater than 96% before undergoing in succession a bleaching treatment using a reducing agent at a pH of between about 8 and 12, a washing operation to remove the reducing agent and a bleaching treatment using an oxidizing agent.

摘要翻译： 一种在机械，机械机械，化学机械或化学机械造纸纸浆或木屑的形式中漂白木质纤维素物质的方法，同时通过在基本上由围绕平行缠绕的两个互穿螺旋表面的机器中加工而转化成这些纸浆类型之一 在围绕它们的桶内以相同的方向同步旋转驱动的轴，以及在物体的向前行进方向上的上游和下游之间确定一系列用于拉制和制动该物质的区域，其包括将使用 还原剂和使用氧化剂的漂白处理，其特征在于，在使用至少一种金属络合或螯合剂进行预处理之后，所述木质纤维素物质经历洗涤操作，其效率大于96％，然后连续进行漂白处理，使用 在pH之间的还原剂 约8和12，用于除去还原剂的洗涤操作和使用氧化剂的漂白处理。

公开(公告)号：US4717451A

公开(公告)日：1988-01-05

申请号：US810405

申请日：1985-12-18

申请人： Michel Devic ,  Jean-Pierre Schirmann

发明人： Michel Devic ,  Jean-Pierre Schirmann

IPC分类号： C07C50/18 ,  C07C45/00 ,  C07C46/00 ,  C07C67/00 ,  D21C3/00 ,  D21C3/20

CPC分类号： C07C46/00

摘要： The process of making a wet or dry dispersion containing anthraquinone suitable for use in the alkaline digestion of wood comprising cyclizing ortho-benzoylbenzoic acid at a temperature of about 150.degree. to 180.degree. C. and at an absolute pressure between about 5 and 40 millibars in the presence of between about 0.05 to 2 parts by weight of sulfuric acid, having a concentration of at least about 95%, per part by weight of ortho-benzoylbenzoic acid to form a reaction mixture containing anthraquinone, bringing the reaction mixture to a pH of at least about 7 by addition thereto at a temperature between about ambient temperature and 100.degree. C. of an aqueous solution of sodium hydroxide or potassium hydroxide containing between about 10% to 40% hydroxide by weight, and then forming a dispersion thereof and using such dispersion in the alkaline digestion of wood.

摘要翻译： 制备适合用于木材碱性消化的含有蒽醌的湿或干分散体的方法，包括在约150-180℃的温度和绝对压力为约5至40毫巴之间环化邻苯甲酰基苯甲酸， 存在约0.05至2重量份的浓度为至少约95重量％的邻苯甲酰基苯甲酸的至少约95重量％的硫酸，以形成含有蒽醌的反应混合物，使反应混合物的pH为 在大约环境温度和100℃之间的温度下加入至少约7的氢氧化钠或氢氧化钾水溶液，其含有约10重量％至40重量％的氢氧化物，然后形成其分散体，并使用它们 分散在木材的碱性消化中。