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    Fluorination process and reactor
    51.
    发明授权
    Fluorination process and reactor 有权
    氟化工艺和反应器

    公开(公告)号：US09353029B2

    公开(公告)日：2016-05-31

    申请号：US14206088

    申请日：2014-03-12

    Applicant: Honeywell International, Inc.

    Inventor： Daniel C. Merkel ,  Hsueh Sung Tung ,  Haiyou Wang ,  Haluk Kopkalli ,  Yuon Chiu

    IPC: C07C17/00 ,  C07C17/20 ,  C07C17/25

    CPC classification number: B01J19/24 ,  B01J4/002 ,  C07C17/206 ,  C07C17/25 ,  C07C21/18

    Abstract: The invention relates to a process to prepare tetrahalopropenes, such as 2-chloro-3,3,3-trifluoropropene (1233xf). The process comprises atomizing a feed material, such as 1,1,2,3-tetrachloropropene (1230xa) and the like, and mixing it with superheated HF to form a vaporized composition of feed material and HF with substantially instantaneous contact with a vapor phase fluorination catalyst. The invention extends catalyst life and forestalls catalyst deactivation.

    Abstract translation: 本发明涉及制备四卤代丙烯的方法，例如2-氯-3,3,3-三氟丙烯（1233xf）。 该方法包括将原料如1,1,2,3-四氯丙烯（1230xa）等进行雾化，并与过热HF混合以形成与气相基本上瞬时接触的原料和HF的蒸发组合物 氟化催化剂。 本发明延长了催化剂的寿命并阻止了催化剂的失活。

    Process for producing 2,3,3,3-tetrafluoropropene
    53.
    发明授权
    Process for producing 2,3,3,3-tetrafluoropropene 有权
    制备2,3,3,3-四氟丙烯的方法

    公开(公告)号：US09328043B2

    公开(公告)日：2016-05-03

    申请号：US14382082

    申请日：2013-02-25

    Applicant: HONEYWELL INTERNATIONAL INC.

    Inventor： Haiyou Wang ,  Selma Bektesevic ,  Hsueh S. Tung ,  Haluk Kopkalli ,  Yuon Chiu

    IPC: C07C17/35 ,  C07C17/20 ,  C07C17/38

    CPC classification number: C07C17/35 ,  C07C17/206 ,  C07C17/38 ,  Y02P20/582 ,  C07C21/18

    Abstract: The present invention relates, in part, an improved process for the production of certain hydrofluoroolefins, particularly 2,3,3,3-tetrafluoropropene (1234yf). In certain non-limiting embodiments, the invention relates to methods for improving process efficiency during the fluorination of 1,1,2,3-tetrachloropropene, 2,3,3,3-tetrachloropropene, and/or 1,1,1,2,3-pentachloropropane to 2-chloro-3,3,3-trifluoropropene by separating and recycling unreacted HF, unreacted starting materials, and/or certain process intermediates from the 2-chloro-3,3,3-trifluoropropene product stream.

    Abstract translation: 本发明部分地涉及用于生产某些氢氟烯烃，特别是2,3,3,3-四氟丙烯（1234yf）的改进方法。 在某些非限制性实施方案中，本发明涉及在1,1,2,3-四氯丙烯，2,3,3,3-四氯丙烯和/或1,1,1,2,3-四氯丙烯的氟化期间提高工艺效率的方法 通过从2-氯-3,3,3-三氟丙烯产物流中分离和循环未反应的HF，未反应的起始物质和/或某些过程中间体，将3-五氯丙烷加入到2-氯-3,3,3-三氟丙烯中。

    Process for the manufacture of fluorinated olefins
    57.
    发明授权
    Process for the manufacture of fluorinated olefins 有权
    制造氟化烯烃的方法

    公开(公告)号：US08940948B2

    公开(公告)日：2015-01-27

    申请号：US13944207

    申请日：2013-07-17

    Applicant: Honeywell International Inc.

    Inventor： Haiyou Wang ,  Hsueh Sung Tung

    IPC: C07C17/00 ,  C07C17/10 ,  C07C17/04 ,  C07C17/354 ,  C07C17/357

    CPC classification number: C07C17/04 ,  C07C17/354 ,  C07C17/357 ,  C07C21/18 ,  C07C19/08

    Abstract: Provided are methods for producing fluorinated organic compounds, which preferably comprises converting at least one compound of formula (I) CH2XCHZCF3 to at least one compound of formula (II) CHX═CZCF3 where X and Z are independently H or F, with the proviso that X and Z are not the same. The converting step comprises catalytically reacting at least one compound of formula (I), preferably via dehydrogenation or oxidative dehydrogenation. In another aspect, the inventive method of preparing fluorinated organic compounds comprises converting a reaction stream comprising at least one pentafluoropropene to a product stream comprising at least one pentafluoropropane and at least one compound of formula (I), separating out the compound of formula (I) from the product stream, and converting the compound of formula (I) separated from the product stream to at least one compound of formula (II), wherein the conversion the compound of formula (I) to 3,3,3-trifluoropropyne is substantially limited.

    Abstract translation: 提供了用于制备氟化有机化合物的方法，其优选包括将至少一种式（I）CH 2 XCHZCF 3化合物转化为至少一种式（II）化合物CHX = CZCF3，其中X和Z独立地为H或F，条件是 X和Z不一样。 转化步骤包括使至少一种式（I）化合物催化反应，优选通过脱氢或氧化脱氢。 在另一方面，制备含氟有机化合物的本发明方法包括将包含至少一种五氟丙烯的反应物流转化为包含至少一种五氟丙烷和至少一种式（I）化合物的产物流，将式（I）化合物 ），并将从产物流分离的式（I）化合物转化为至少一种式（II）化合物，其中式（I）化合物与3,3,3-三氟丙炔的转化率为 基本上有限。

    Process for the preparation of 1-chloro-3,3,3-trifluoropropene using a phase transfer catalyst
    58.
    发明授权
    Process for the preparation of 1-chloro-3,3,3-trifluoropropene using a phase transfer catalyst 有权
    使用相转移催化剂制备1-氯-3,3,3-三氟丙烯的方法

    公开(公告)号：US08907146B2

    公开(公告)日：2014-12-09

    申请号：US14168065

    申请日：2014-01-30

    Applicant: Honeywell International Inc.

    Inventor： Hsueh Sung Tung ,  Haiyou Wang ,  Daniel C. Merkel ,  Stephen A. Cottrell ,  Konstantin A. Pokrovski ,  Ian Shankland

    IPC: C07C17/20 ,  C07C17/21

    CPC classification number: C07C17/204 ,  C07C17/206 ,  C07C17/21 ,  C07C17/25 ,  C07C21/18

    Abstract: Disclosed is a process in which the fluorination of an organic reactant comprising 1,1,1,3,3-pentachloropropane (240fa) with anhydrous HF is conducted in the presence of an effective amount of a phase-transfer catalyst which facilitates the reaction between these incompatible reaction components to produce 1-chloro-3,3,3-trifluoro-propene (1233zd). Other organic reactant materials include 1,1,3,3-tetrachloropropene (HCO-1230za), 1,3,3,3-tetrachloropropene (HCO-1230zd), and various mixtures with or without 240fa.

    Abstract translation: 公开了在有效量的相转移催化剂的存在下进行含有1,1,1,3,3-五氯丙烷（240fa）的无水HF的有机反应物的氟化的方法，该相转移催化剂促进了 这些不相容的反应组分产生1-氯-3,3,3-三氟丙烯（1233zd）。 其它有机反应物料包括1,1,3,3-四氯丙烯（HCO-1230za），1,3,3,3-四氯丙烯（HCO-1230zd）以及各种混合物，其中有或没有240fa。

    PROCESS FOR THE PREPARATION OF 1-CHLORO-3,3,3-TRIFLUOROPROPENE USING A PHASE TRANSFER CATALYST
    59.
    发明申请
    PROCESS FOR THE PREPARATION OF 1-CHLORO-3,3,3-TRIFLUOROPROPENE USING A PHASE TRANSFER CATALYST 有权
    使用相转移催化剂制备1-氯-3,3,3-三氟丙烯的方法

    公开(公告)号：US20140221704A1

    公开(公告)日：2014-08-07

    申请号：US14168065

    申请日：2014-01-30

    Applicant: Honeywell International Inc.

    Inventor： Hsueh Sung Tung ,  Haiyou Wang ,  Daniel C. Merkel ,  Stephen A. Cottrell ,  Konstantin A. Pokrovski ,  Ian Shankland

    IPC: C07C17/20

    CPC classification number: C07C17/204 ,  C07C17/206 ,  C07C17/21 ,  C07C17/25 ,  C07C21/18

    Abstract: Disclosed is a process in which the fluorination of an organic reactant comprising 1,1,1,3,3-pentachloropropane (240fa) with anhydrous HF is conducted in the presence of an effective amount of a phase-transfer catalyst which facilitates the reaction between these incompatible reaction components to produce 1-chloro-3,3,3-trifluoro-propene (1233zd). Other organic reactant materials include 1,1,3,3-tetrachloropropene (HCO-1230za), 1,3,3,3-tetrachloropropene (HCO-1230zd), and various mixtures with or without 240fa.

    Abstract translation: 公开了在有效量的相转移催化剂的存在下进行含有1,1,1,3,3-五氯丙烷（240fa）的无水HF的有机反应物的氟化的方法，该相转移催化剂促进了 这些不相容的反应组分产生1-氯-3,3,3-三氟丙烯（1233zd）。 其它有机反应物料包括1,1,3,3-四氯丙烯（HCO-1230za），1,3,3,3-四氯丙烯（HCO-1230zd）以及各种混合物，其中有或没有240fa。

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